data_shelx _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C18 H18 N4 O2 S4' _chemical_formula_weight 450.60 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 12.4489(8) _cell_length_b 14.0742(9) _cell_length_c 12.0688(8) _cell_angle_alpha 90 _cell_angle_beta 93.403(5) _cell_angle_gamma 90 _cell_volume 2110.8(2) _cell_formula_units_Z 4 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 3423 _cell_measurement_theta_min 3.327 _cell_measurement_theta_max 29.007 _exptl_crystal_description cube _exptl_crystal_colour yellow _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.418 _exptl_crystal_F_000 936 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.32 _exptl_crystal_size_mid 0.30 _exptl_crystal_size_min 0.28 _exptl_absorpt_coefficient_mu 0.472 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type EOS,Gemini _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 8234 _diffrn_reflns_av_unetI/netI 0.0392 _diffrn_reflns_av_R_equivalents 0.0192 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 3.327 _diffrn_reflns_theta_max 29.007 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.856 _diffrn_measured_fraction_theta_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.856 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.856 _diffrn_reflns_point_group_measured_fraction_full 0.994 _reflns_number_total 4803 _reflns_number_gt 3423 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0469P)^2^+0.7066P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4803 _refine_ls_number_parameters 253 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0718 _refine_ls_R_factor_gt 0.0456 _refine_ls_wR_factor_ref 0.1134 _refine_ls_wR_factor_gt 0.0999 _refine_ls_goodness_of_fit_ref 1.017 _refine_ls_restrained_S_all 1.017 _refine_ls_shift/su_max 0.009 _refine_ls_shift/su_mean 0.001 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.70991(5) 0.15028(5) 0.55636(5) 0.05029(18) Uani 1 1 d . . . . . S4 S 0.96321(5) 0.12634(5) 0.56514(5) 0.05265(18) Uani 1 1 d . . . . . S3 S 0.76768(5) 0.06198(5) 0.68001(6) 0.05545(19) Uani 1 1 d . . . . . S2 S 0.78552(6) 0.27998(5) 0.74468(5) 0.0590(2) Uani 1 1 d . . . . . N4 N 0.90665(15) -0.03766(13) 0.81541(16) 0.0442(5) Uani 1 1 d . . . . . N3 N 0.96858(15) 0.00706(14) 0.73660(16) 0.0459(5) Uani 1 1 d . . . . . O1 O 0.50338(15) 0.20578(12) 0.31807(15) 0.0617(5) Uani 1 1 d . . . . . H1 H 0.5365 0.2171 0.3774 0.093 Uiso 1 1 calc R U . . . O2 O 0.73139(14) -0.08800(14) 0.91192(16) 0.0653(5) Uani 1 1 d . . . . . H2 H 0.7667 -0.0616 0.8656 0.098 Uiso 1 1 calc R U . . . C13 C 0.91058(18) -0.13014(15) 0.98151(18) 0.0387(5) Uani 1 1 d . . . . . C12 C 0.96166(18) -0.08094(15) 0.89302(19) 0.0415(5) Uani 1 1 d . . . . . H12 H 1.0363 -0.0808 0.8926 0.050 Uiso 1 1 calc R U . . . C8 C 0.71480(18) 0.26600(17) 0.61726(18) 0.0432(5) Uani 1 1 d . . . . . N2 N 0.66945(17) 0.33639(14) 0.56750(16) 0.0501(5) Uani 1 1 d . . . . . C6 C 0.52321(18) 0.37558(17) 0.30250(19) 0.0436(5) Uani 1 1 d . . . . . N1 N 0.61281(16) 0.31185(14) 0.46734(16) 0.0474(5) Uani 1 1 d . . . . . C18 C 0.79851(19) -0.13210(17) 0.9876(2) 0.0465(6) Uani 1 1 d . . . . . C7 C 0.58327(19) 0.38401(17) 0.4086(2) 0.0459(5) Uani 1 1 d . . . . . H7 H 0.6011 0.4444 0.4352 0.055 Uiso 1 1 calc R U . . . C14 C 0.9738(2) -0.17767(17) 1.06347(18) 0.0472(6) Uani 1 1 d . . . . . H14 H 1.0484 -0.1757 1.0617 0.057 Uiso 1 1 calc R U . . . C11 C 0.91052(18) 0.05767(16) 0.66854(19) 0.0424(5) Uani 1 1 d . . . . . C5 C 0.5023(2) 0.45746(19) 0.2390(2) 0.0540(6) Uani 1 1 d . . . . . H5 H 0.5253 0.5163 0.2664 0.065 Uiso 1 1 calc R U . . . C1 C 0.48677(19) 0.28776(18) 0.2608(2) 0.0468(6) Uani 1 1 d . . . . . C15 C 0.9279(2) -0.2274(2) 1.1470(2) 0.0575(7) Uani 1 1 d . . . . . H15 H 0.9710 -0.2596 1.2003 0.069 Uiso 1 1 calc R U . . . C3 C 0.4123(2) 0.3652(3) 0.0969(2) 0.0671(8) Uani 1 1 d . . . . . H3 H 0.3752 0.3616 0.0278 0.081 Uiso 1 1 calc R U . . . C2 C 0.4305(2) 0.2834(2) 0.1580(2) 0.0593(7) Uani 1 1 d . . . . . H2A H 0.4051 0.2254 0.1305 0.071 Uiso 1 1 calc R U . . . C10 C 1.1045(2) 0.1037(2) 0.5882(2) 0.0583(7) Uani 1 1 d . . . . . H10A H 1.1433 0.1383 0.5349 0.087 Uiso 1 1 calc R U . . . H10B H 1.1179 0.0369 0.5802 0.087 Uiso 1 1 calc R U . . . H10C H 1.1280 0.1236 0.6617 0.087 Uiso 1 1 calc R U . . . C16 C 0.8174(2) -0.2290(2) 1.1506(2) 0.0612(7) Uani 1 1 d . . . . . H16 H 0.7860 -0.2629 1.2064 0.073 Uiso 1 1 calc R U . . . C17 C 0.7532(2) -0.1814(2) 1.0729(2) 0.0577(7) Uani 1 1 d . . . . . H17 H 0.6789 -0.1821 1.0773 0.069 Uiso 1 1 calc R U . . . C9 C 0.7656(2) 0.4044(2) 0.7660(2) 0.0699(8) Uani 1 1 d . . . . . H9A H 0.8013 0.4232 0.8352 0.105 Uiso 1 1 calc R U . . . H9B H 0.6900 0.4174 0.7676 0.105 Uiso 1 1 calc R U . . . H9C H 0.7949 0.4394 0.7065 0.105 Uiso 1 1 calc R U . . . C4 C 0.4481(2) 0.4519(2) 0.1365(2) 0.0645(8) Uani 1 1 d . . . . . H4 H 0.4357 0.5065 0.0942 0.077 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0524(4) 0.0450(3) 0.0521(3) 0.0009(3) -0.0079(3) -0.0019(3) S4 0.0533(4) 0.0518(4) 0.0538(4) 0.0134(3) 0.0104(3) -0.0007(3) S3 0.0446(3) 0.0550(4) 0.0669(4) 0.0192(3) 0.0049(3) -0.0005(3) S2 0.0526(4) 0.0729(5) 0.0498(4) -0.0089(3) -0.0112(3) 0.0059(3) N4 0.0433(10) 0.0396(10) 0.0503(11) 0.0055(9) 0.0071(9) -0.0009(9) N3 0.0465(11) 0.0408(10) 0.0512(11) 0.0081(9) 0.0101(9) 0.0007(9) O1 0.0759(13) 0.0470(10) 0.0609(11) 0.0051(9) -0.0058(10) -0.0117(9) O2 0.0423(9) 0.0750(13) 0.0788(13) 0.0290(11) 0.0042(9) 0.0045(9) C13 0.0445(12) 0.0312(11) 0.0402(11) -0.0046(10) 0.0017(10) -0.0005(10) C12 0.0409(12) 0.0355(12) 0.0485(13) -0.0025(10) 0.0064(10) -0.0002(10) C8 0.0392(12) 0.0483(13) 0.0417(12) -0.0036(11) 0.0001(10) -0.0030(11) N2 0.0562(12) 0.0471(12) 0.0461(11) -0.0019(10) -0.0046(9) -0.0021(10) C6 0.0395(12) 0.0462(13) 0.0458(12) 0.0054(11) 0.0071(10) 0.0086(11) N1 0.0526(12) 0.0433(11) 0.0457(11) 0.0023(9) -0.0025(9) -0.0006(10) C18 0.0457(13) 0.0443(13) 0.0497(13) 0.0008(11) 0.0037(11) 0.0016(11) C7 0.0470(13) 0.0398(12) 0.0511(13) 0.0003(11) 0.0041(11) 0.0018(11) C14 0.0484(13) 0.0476(14) 0.0452(12) -0.0035(11) -0.0008(11) 0.0012(11) C11 0.0461(12) 0.0347(11) 0.0468(12) -0.0014(10) 0.0072(10) -0.0009(10) C5 0.0558(14) 0.0504(15) 0.0563(15) 0.0072(12) 0.0066(12) 0.0150(12) C1 0.0407(12) 0.0508(14) 0.0493(13) 0.0042(12) 0.0052(11) 0.0003(11) C15 0.0682(17) 0.0625(17) 0.0410(13) 0.0060(12) -0.0047(12) 0.0035(14) C3 0.0525(16) 0.100(2) 0.0482(14) 0.0077(16) -0.0031(12) 0.0184(17) C2 0.0509(15) 0.0725(19) 0.0543(15) -0.0051(14) 0.0007(12) -0.0004(14) C10 0.0523(15) 0.0577(16) 0.0661(17) 0.0070(14) 0.0140(13) 0.0035(13) C16 0.0713(18) 0.0697(18) 0.0433(13) 0.0075(13) 0.0092(13) -0.0082(16) C17 0.0497(14) 0.0679(17) 0.0565(15) 0.0025(14) 0.0128(12) -0.0033(14) C9 0.0704(19) 0.074(2) 0.0656(17) -0.0230(16) 0.0036(15) -0.0065(16) C4 0.0665(18) 0.0707(19) 0.0566(16) 0.0151(15) 0.0069(14) 0.0285(16) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 C8 1.786(2) . ? S1 S3 2.0399(9) . ? S4 C11 1.737(2) . ? S4 C10 1.793(3) . ? S3 C11 1.793(2) . ? S2 C8 1.737(2) . ? S2 C9 1.789(3) . ? N4 C12 1.281(3) . ? N4 N3 1.408(2) . ? N3 C11 1.278(3) . ? O1 C1 1.355(3) . ? O2 C18 1.351(3) . ? C13 C14 1.398(3) . ? C13 C18 1.402(3) . ? C13 C12 1.451(3) . ? C8 N2 1.273(3) . ? N2 N1 1.406(3) . ? C6 C5 1.400(3) . ? C6 C1 1.400(3) . ? C6 C7 1.449(3) . ? N1 C7 1.280(3) . ? C18 C17 1.389(3) . ? C14 C15 1.379(3) . ? C5 C4 1.376(4) . ? C1 C2 1.389(3) . ? C15 C16 1.379(4) . ? C3 C4 1.376(4) . ? C3 C2 1.379(4) . ? C16 C17 1.371(4) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C8 S1 S3 104.63(8) . . ? C11 S4 C10 101.44(12) . . ? C11 S3 S1 105.80(8) . . ? C8 S2 C9 99.84(13) . . ? C12 N4 N3 114.59(18) . . ? C11 N3 N4 111.83(18) . . ? C14 C13 C18 118.3(2) . . ? C14 C13 C12 119.8(2) . . ? C18 C13 C12 121.9(2) . . ? N4 C12 C13 121.8(2) . . ? N2 C8 S2 121.11(19) . . ? N2 C8 S1 120.80(17) . . ? S2 C8 S1 118.07(14) . . ? C8 N2 N1 113.6(2) . . ? C5 C6 C1 119.0(2) . . ? C5 C6 C7 119.1(2) . . ? C1 C6 C7 122.0(2) . . ? C7 N1 N2 113.2(2) . . ? O2 C18 C17 117.9(2) . . ? O2 C18 C13 122.2(2) . . ? C17 C18 C13 119.8(2) . . ? N1 C7 C6 122.7(2) . . ? C15 C14 C13 121.3(2) . . ? N3 C11 S4 123.25(18) . . ? N3 C11 S3 119.65(17) . . ? S4 C11 S3 117.07(13) . . ? C4 C5 C6 120.7(3) . . ? O1 C1 C2 118.1(2) . . ? O1 C1 C6 122.1(2) . . ? C2 C1 C6 119.7(2) . . ? C16 C15 C14 119.3(2) . . ? C4 C3 C2 121.0(3) . . ? C3 C2 C1 119.9(3) . . ? C17 C16 C15 120.8(2) . . ? C16 C17 C18 120.4(2) . . ? C3 C4 C5 119.6(3) . . ? _refine_diff_density_max 0.292 _refine_diff_density_min -0.188 _refine_diff_density_rms 0.047 _shelxl_version_number 2013-4 _shelx_res_file ; TITL w-sml4fe_a.res in P2(1)/c CELL 0.71073 12.4489 14.0742 12.0688 90.000 93.403 90.000 ZERR 4.00 0.0008 0.0009 0.0008 0.000 0.005 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H N O S UNIT 72 72 16 8 16 MERG 2 ACTA FMAP 2 PLAN 20 BOND L.S. 4 WGHT 0.046900 0.706600 FVAR 5.20065 MOLE 1 S1 5 0.709913 0.150280 0.556359 11.00000 0.05239 0.04505 = 0.05213 0.00092 -0.00788 -0.00189 S4 5 0.963209 0.126340 0.565136 11.00000 0.05326 0.05180 = 0.05376 0.01335 0.01037 -0.00072 S3 5 0.767677 0.061978 0.680009 11.00000 0.04455 0.05505 = 0.06694 0.01921 0.00485 -0.00047 S2 5 0.785519 0.279983 0.744681 11.00000 0.05260 0.07289 = 0.04982 -0.00887 -0.01115 0.00594 N4 3 0.906654 -0.037664 0.815412 11.00000 0.04330 0.03958 = 0.05027 0.00547 0.00711 -0.00087 N3 3 0.968579 0.007059 0.736600 11.00000 0.04647 0.04077 = 0.05123 0.00809 0.01008 0.00072 O1 4 0.503384 0.205782 0.318070 11.00000 0.07590 0.04705 = 0.06092 0.00506 -0.00584 -0.01165 AFIX 83 H1 2 0.536495 0.217121 0.377361 11.00000 -1.50000 AFIX 0 O2 4 0.731391 -0.088005 0.911920 11.00000 0.04233 0.07501 = 0.07875 0.02898 0.00418 0.00445 AFIX 83 H2 2 0.766698 -0.061617 0.865629 11.00000 -1.50000 AFIX 0 C13 1 0.910585 -0.130141 0.981513 11.00000 0.04454 0.03116 = 0.04021 -0.00458 0.00173 -0.00052 C12 1 0.961663 -0.080942 0.893024 11.00000 0.04090 0.03545 = 0.04849 -0.00254 0.00637 -0.00020 AFIX 43 H12 2 1.036345 -0.080819 0.892633 11.00000 -1.20000 AFIX 0 C8 1 0.714801 0.265999 0.617263 11.00000 0.03919 0.04831 = 0.04171 -0.00358 0.00009 -0.00298 N2 3 0.669454 0.336394 0.567497 11.00000 0.05619 0.04714 = 0.04613 -0.00194 -0.00460 -0.00214 C6 1 0.523211 0.375583 0.302500 11.00000 0.03947 0.04624 = 0.04578 0.00536 0.00713 0.00864 N1 3 0.612814 0.311846 0.467342 11.00000 0.05264 0.04334 = 0.04571 0.00232 -0.00251 -0.00059 C18 1 0.798507 -0.132104 0.987556 11.00000 0.04573 0.04427 = 0.04972 0.00076 0.00371 0.00163 C7 1 0.583273 0.384011 0.408615 11.00000 0.04697 0.03978 = 0.05114 0.00029 0.00415 0.00183 AFIX 43 H7 2 0.601098 0.444364 0.435154 11.00000 -1.20000 AFIX 0 C14 1 0.973839 -0.177672 1.063470 11.00000 0.04842 0.04757 = 0.04519 -0.00348 -0.00079 0.00125 AFIX 43 H14 2 1.048386 -0.175701 1.061657 11.00000 -1.20000 AFIX 0 C11 1 0.910521 0.057674 0.668537 11.00000 0.04611 0.03467 = 0.04684 -0.00141 0.00723 -0.00091 C5 1 0.502292 0.457456 0.239030 11.00000 0.05578 0.05041 = 0.05628 0.00721 0.00660 0.01501 AFIX 43 H5 2 0.525287 0.516250 0.266446 11.00000 -1.20000 AFIX 0 C1 1 0.486771 0.287761 0.260767 11.00000 0.04069 0.05078 = 0.04932 0.00423 0.00523 0.00027 C15 1 0.927892 -0.227430 1.146960 11.00000 0.06816 0.06246 = 0.04101 0.00599 -0.00470 0.00354 AFIX 43 H15 2 0.970958 -0.259554 1.200274 11.00000 -1.20000 AFIX 0 C3 1 0.412269 0.365179 0.096858 11.00000 0.05250 0.09994 = 0.04816 0.00770 -0.00312 0.01842 AFIX 43 H3 2 0.375235 0.361638 0.027757 11.00000 -1.20000 AFIX 0 C2 1 0.430463 0.283395 0.158039 11.00000 0.05093 0.07247 = 0.05432 -0.00506 0.00074 -0.00043 AFIX 43 H2A 2 0.405051 0.225361 0.130537 11.00000 -1.20000 AFIX 0 C10 1 1.104522 0.103661 0.588156 11.00000 0.05233 0.05773 = 0.06607 0.00701 0.01399 0.00345 AFIX 33 H10A 2 1.143294 0.138338 0.534869 11.00000 -1.50000 H10B 2 1.117917 0.036907 0.580204 11.00000 -1.50000 H10C 2 1.128005 0.123597 0.661719 11.00000 -1.50000 AFIX 0 C16 1 0.817404 -0.229046 1.150553 11.00000 0.07134 0.06967 = 0.04329 0.00752 0.00920 -0.00824 AFIX 43 H16 2 0.786042 -0.262899 1.206396 11.00000 -1.20000 AFIX 0 C17 1 0.753220 -0.181392 1.072864 11.00000 0.04967 0.06795 = 0.05651 0.00247 0.01278 -0.00329 AFIX 43 H17 2 0.678899 -0.182073 1.077311 11.00000 -1.20000 AFIX 0 C9 1 0.765631 0.404400 0.765988 11.00000 0.07039 0.07375 = 0.06560 -0.02304 0.00361 -0.00650 AFIX 33 H9A 2 0.801324 0.423151 0.835243 11.00000 -1.50000 H9B 2 0.690035 0.417375 0.767634 11.00000 -1.50000 H9C 2 0.794861 0.439429 0.706519 11.00000 -1.50000 AFIX 0 C4 1 0.448060 0.451918 0.136476 11.00000 0.06646 0.07068 = 0.05664 0.01515 0.00693 0.02849 AFIX 43 H4 2 0.435685 0.506509 0.094212 11.00000 -1.20000 AFIX 0 HKLF 4 REM w-sml4fe_a.res in P2(1)/c REM R1 = 0.0456 for 3423 Fo > 4sig(Fo) and 0.0718 for all 4803 data REM 253 parameters refined using 0 restraints END WGHT 0.0461 0.6760 REM Highest difference peak 0.292, deepest hole -0.188, 1-sigma level 0.047 Q1 1 0.7069 0.2105 0.6016 11.00000 0.05 0.29 Q2 1 0.7580 0.1106 0.6221 11.00000 0.05 0.27 Q3 1 0.7633 0.1720 0.5004 11.00000 0.05 0.26 Q4 1 0.7753 0.1242 0.7272 11.00000 0.05 0.26 Q5 1 0.9170 0.0955 0.6142 11.00000 0.05 0.26 Q6 1 0.7933 0.1058 0.7354 11.00000 0.05 0.26 Q7 1 0.8462 0.0447 0.6617 11.00000 0.05 0.25 Q8 1 0.8427 -0.0281 0.8186 11.00000 0.05 0.23 Q9 1 0.7763 -0.1368 1.0406 11.00000 0.05 0.23 Q10 1 0.9247 -0.0965 0.9474 11.00000 0.05 0.22 Q11 1 0.7792 0.2924 0.6653 11.00000 0.05 0.22 Q12 1 1.1418 0.0621 0.5297 11.00000 0.05 0.21 Q13 1 0.5280 0.3950 0.3565 11.00000 0.05 0.20 Q14 1 0.7532 -0.0709 0.9818 11.00000 0.05 0.19 Q15 1 0.4748 0.4088 0.2859 11.00000 0.05 0.19 Q16 1 1.0334 0.0257 0.7000 11.00000 0.05 0.19 Q17 1 0.7530 0.4404 0.6940 11.00000 0.05 0.19 Q18 1 0.9274 -0.0275 0.7692 11.00000 0.05 0.18 Q19 1 0.6318 0.2510 0.4393 11.00000 0.05 0.18 Q20 1 0.7824 0.3412 0.7713 11.00000 0.05 0.18 ; _shelx_res_checksum 53503 _shelx_hkl_file ; 3 0 0 7373.19 260.623 1 -5 0 0 1350.61 136.302 2 5 0 0 1339.93 170.521 1 -5 0 0 1161.60 155.036 1 -6 0 0 154370. 1256.61 2 6 0 0 153223. 1666.25 1 7 0 0 66800.4 1202.98 1 -7 0 0 68650.5 900.017 2 8 0 0-184.940 152.967 1 -8 0 0 121.764 96.4317 2 9 0 0 151.448 147.060 1 -9 0 0 175.303 90.4179 2 -10 0 0 16987.4 531.441 2 10 0 0 17442.9 767.032 1 11 0 0 29082.8 1038.82 1 -11 0 0 26492.6 686.986 2 12 0 0 7514.94 584.129 1 13 0 0 1950.61 341.966 1 14 0 0 212.556 222.157 1 15 0 0 13717.9 899.555 1 16 0 0 11373.0 859.136 1 2 1 0 152026. 1044.41 1 -3 1 0 295838. 1314.71 2 3 1 0 294911. 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109.812 1 2 -4 2 123.480 113.424 3 3 4 2 6367.18 346.575 1 3 -4 2 5889.68 323.350 3 4 4 2 143581. 1725.09 1 4 -4 2 140952. 1609.76 3 5 4 2 617.634 184.675 1 6 4 2 24.1243 141.933 1 7 4 2 3543.80 374.794 1 7 -4 2 3525.85 227.844 2 8 4 2 1605.57 264.567 1 8 -4 2 1653.27 169.200 2 9 4 2 930.448 243.561 1 9 -4 2 1261.79 276.203 1 10 4 2 20908.4 940.033 1 10 -4 2 19052.7 866.728 1 11 -4 2 138.843 201.643 1 11 4 2 530.149 231.896 1 12 -4 2 2825.72 402.773 1 12 4 2 2651.65 417.637 1 13 -4 2 7012.41 616.685 1 13 4 2 6381.31 625.001 1 14 4 2 4135.62 555.804 1 14 -4 2 3928.94 504.454 1 15 4 2 3139.63 535.567 1 15 -4 2 2737.35 455.445 1 16 -4 2 1173.70 356.198 1 16 5 -2 677.147 336.898 1 15 5 -2 1013.01 314.743 1 14 5 -2 1260.62 367.237 1 13 5 -2 11282.1 788.246 1 12 5 -2 8811.39 685.180 1 12 -5 -2 7662.38 519.944 1 11 -5 -2 1073.58 220.050 1 11 5 -2 923.116 310.921 1 10 -5 -2 17770.8 686.693 1 10 5 -2 18254.1 865.735 1 9 5 -2 6997.93 527.928 1 9 -5 -2 7018.14 415.889 1 8 5 -2 1162.97 244.984 1 8 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0 -6 -2 178563. 1379.09 3 1 -6 2 574.294 156.175 3 1 6 2 652.176 139.286 1 2 6 2 207369. 2016.98 1 2 -6 2 207972. 1980.05 3 3 6 2 270.051 159.658 1 3 -6 2 298.183 155.113 3 4 -6 2 69045.9 1229.25 3 4 6 2 70589.4 1331.22 1 5 -6 2 8673.69 466.563 3 5 6 2 9377.10 530.347 1 6 6 2 24859.7 892.910 1 7 6 2-139.664 236.123 1 8 6 2 12022.3 700.872 1 9 6 2 6323.62 567.352 1 10 6 2 4326.78 490.563 1 11 6 2 40.8994 246.831 1 11 -6 2 70.5429 204.522 1 12 6 2 1007.54 283.852 1 12 -6 2 1157.93 313.403 1 13 -6 2 2997.77 453.234 1 13 6 2 3069.43 510.901 1 14 -6 2-144.783 219.597 1 14 6 2 145.720 258.242 1 15 -6 2 483.964 281.581 1 15 7 -2 200.496 259.636 1 14 7 -2 881.860 339.468 1 13 7 -2 2354.48 456.436 1 12 7 -2 988.644 336.462 1 11 7 -2 957.395 292.127 1 10 -7 -2 942.362 193.557 1 10 7 -2 898.273 265.168 1 9 -7 -2 82.7900 121.878 1 9 7 -2 156.995 215.488 1 8 7 -2 24262.1 999.356 1 7 7 -2 18381.4 833.287 1 -6 7 2 11292.2 407.816 3 6 7 -2 10835.3 605.653 1 5 7 -2 12488.5 620.436 1 -5 7 2 11994.9 381.388 3 -5 -7 2 11369.7 599.274 3 -4 7 2 12456.5 356.830 3 -4 -7 2 12229.9 582.963 3 4 -7 -2 11909.2 356.248 3 3 -7 -2 24889.7 498.234 3 -3 -7 2 23587.5 761.195 3 -3 7 2 25134.0 479.986 3 3 -7 -2 23941.4 619.278 1 2 -7 -2 16111.9 408.196 3 2 -7 -2 17337.9 543.715 1 -2 -7 2 16036.1 614.306 3 -1 -7 2-97.7572 193.506 3 1 -7 -2 557.626 107.400 3 0 -7 2 11.3317 132.743 3 0 -7 -2 163.994 94.3406 3 1 7 2 64176.4 1150.58 1 1 -7 2 63155.5 1148.17 3 2 -7 2-24.5506 138.157 3 2 7 2 197.406 145.496 1 3 7 2 14784.7 619.909 1 3 -7 2 14446.9 587.378 3 4 7 2 3564.25 341.692 1 4 -7 2 3403.87 301.100 3 5 7 2 1727.22 276.276 1 5 -7 2 1297.43 217.744 3 6 7 2 3574.26 392.832 1 6 -7 2 3517.34 349.376 3 7 7 2 727.951 285.847 1 8 7 2 942.012 297.531 1 9 7 2 22627.6 1022.39 1 10 7 2 5168.86 535.395 1 11 7 2 203.345 248.595 1 12 -7 2 2748.44 427.245 1 12 7 2 2405.50 444.685 1 13 7 2 4618.12 598.844 1 13 -7 2 4924.48 556.479 1 14 7 2 209.256 282.800 1 14 -7 2 607.938 306.630 1 14 8 -2 1727.85 394.170 1 13 8 -2 797.647 318.265 1 12 8 -2 1602.20 370.774 1 11 8 -2 5002.48 540.510 1 10 -8 -2 6413.86 444.565 1 10 8 -2 6800.40 601.067 1 9 8 -2 271.159 259.375 1 8 8 -2 32651.5 1192.99 1 7 8 -2 47038.3 1349.57 1 -6 8 2 6673.32 324.868 3 6 8 -2 7198.85 533.346 1 -6 -8 2 7113.21 522.435 3 -5 8 2 2777.47 204.199 3 -5 -8 2 2875.40 329.982 3 -4 8 2 5309.80 253.883 3 -4 -8 2 5077.65 411.208 3 4 -8 -2 5315.96 263.256 3 -3 -8 2 29222.1 898.982 3 3 -8 -2 29855.8 601.917 3 -3 8 2 30596.4 586.117 3 -2 -8 2 400.455 165.308 3 2 -8 -2 436.635 99.0473 3 1 -8 -2 21410.1 549.961 3 -1 -8 2 21147.6 736.949 3 0 -8 2 35329.0 922.845 3 0 -8 -2 35602.5 731.758 3 1 8 2-44.9842 127.792 1 -1 -8 -2-81.4547 106.226 3 1 -8 2-192.545 167.215 3 2 -8 2 421.720 167.813 3 2 8 2 470.962 162.621 1 3 -8 2 110.207 147.541 3 3 8 2 114.577 174.285 1 4 -8 2 40555.0 1033.35 3 4 8 2 40831.5 1110.11 1 5 8 2 2714.65 337.380 1 5 -8 2 2497.24 292.424 3 6 -8 2 2621.92 300.729 3 6 8 2 3782.67 408.624 1 7 8 2 6908.48 565.459 1 8 8 2 14791.7 818.777 1 9 8 2 1153.16 304.171 1 10 8 2 187.755 234.929 1 11 8 2 417.444 249.018 1 12 -8 2 3006.78 428.485 1 12 8 2 3104.40 510.165 1 13 8 2 2640.12 481.875 1 13 -8 2 2953.79 458.785 1 14 9 -2 506.439 307.359 1 13 9 -2 222.627 242.431 1 12 9 -2-126.840 293.314 1 11 9 -2 138.721 252.066 1 10 9 -2 5883.45 587.633 1 9 9 -2 1122.59 353.892 1 8 9 -2 3162.90 451.979 1 -8 -9 2 2673.25 421.765 3 7 9 -2 2601.82 407.965 1 -7 -9 2 2036.74 357.086 3 -6 -9 2 145.181 260.429 3 -5 -9 2 2815.91 345.981 3 -5 9 2 2635.96 205.313 3 -4 -9 2 22550.7 859.216 3 -4 9 2 22483.1 558.609 3 4 -9 -2 22486.2 566.601 3 3 -9 -2 2207.82 193.481 3 -3 -9 2 2162.95 303.071 3 2 -9 -2 5972.33 309.319 3 -2 -9 2 5452.73 412.184 3 -1 -9 2 12777.7 610.583 3 1 -9 -2 13365.8 470.468 3 0 -9 2 21039.8 755.717 3 0 -9 -2 21133.5 619.367 3 -1 -9 -2 21951.4 660.399 3 1 -9 2 21901.1 765.249 3 -2 -9 -2 50.3817 143.964 3 2 -9 2 111.711 171.383 3 2 9 2 116.074 149.551 1 3 9 2 35843.9 1058.44 1 3 -9 2 36419.7 1002.38 3 4 9 2 7943.47 540.654 1 4 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58227.3 918.060 3 -2 3 3 57905.4 901.477 2 -1 3 3 34202.3 442.488 1 1 -3 -3 34248.7 442.610 1 -1 -3 3 33985.9 687.037 3 0 -3 -3 310.300 76.7066 1 0 -3 3 336.899 135.189 3 0 3 3 158.727 73.4591 1 1 -3 3 76571.4 1065.03 3 1 3 3 74343.2 918.559 1 -1 -3 -3 73834.7 924.462 1 2 -3 3 2875.05 236.313 3 2 3 3 2955.13 218.798 1 -2 -3 -3 3135.33 221.421 1 3 -3 3 4415.89 302.764 3 3 3 3 4791.32 302.035 1 4 -3 3 71069.2 1197.39 3 4 3 3 72251.8 1209.84 1 5 3 3 37386.2 951.742 1 6 3 3 5623.55 415.195 1 7 3 3 23673.9 864.988 1 7 -3 3 21905.7 440.804 2 8 3 3 3867.88 392.361 1 9 -3 3 2277.72 357.624 1 9 3 3 1934.46 323.048 1 10 3 3 2548.86 378.375 1 10 -3 3 2300.68 357.041 1 11 3 3 13025.8 815.275 1 11 -3 3 13342.7 782.384 1 12 -3 3 2509.94 392.775 1 12 3 3 3182.37 456.786 1 13 3 3 3975.34 533.999 1 13 -3 3 3319.05 462.037 1 14 -3 3 497.059 266.049 1 14 3 3 729.778 345.148 1 15 3 3 600.539 328.272 1 15 -3 3 619.159 313.283 1 16 -3 3 1329.07 373.205 1 15 4 -3 410.888 298.683 1 14 4 -3 6125.62 608.727 1 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3 5899.51 392.631 3 5 4 3 5909.05 410.298 1 6 4 3 9295.41 534.912 1 7 4 3 7470.71 516.351 1 7 -4 3 8457.29 327.083 2 8 4 3 12157.9 671.180 1 8 -4 3 11685.6 386.215 2 9 4 3 2405.85 350.576 1 10 4 3 2449.12 373.089 1 10 -4 3 2087.77 348.203 1 11 4 3 1370.74 343.649 1 11 -4 3 1132.85 275.561 1 12 -4 3 2686.70 428.091 1 12 4 3 3430.57 474.160 1 13 -4 3 415.648 271.035 1 13 4 3-182.569 266.263 1 14 -4 3 805.422 300.784 1 14 4 3 1061.03 355.400 1 15 -4 3 2273.49 444.575 1 15 4 3 2308.82 473.669 1 16 -4 3 483.668 324.071 1 16 5 -3 521.744 337.748 1 15 5 -3 138.652 265.625 1 14 5 -3 893.874 317.391 1 13 5 -3 5545.06 581.457 1 12 5 -3 9727.72 702.278 1 11 5 -3-37.9649 210.844 1 10 5 -3 6366.00 527.226 1 10 -5 -3 5681.67 357.444 1 9 -5 -3 32914.3 798.687 1 9 5 -3 34428.9 1137.59 1 8 -5 -3 37790.6 760.922 1 8 5 -3 39287.3 1138.09 1 -7 5 3 2639.62 205.741 3 7 5 -3 3222.44 348.143 1 7 -5 -3 2954.54 212.747 1 6 5 -3 2545.90 285.426 1 -6 5 3 2903.11 190.068 3 -5 5 3 42399.6 562.469 3 -5 -5 3 43156.8 1038.74 3 -4 5 3 42940.7 428.348 3 -4 -5 3 45245.5 1010.03 3 3 -5 -3 1071.41 100.207 1 -3 -5 3 1079.41 217.635 3 -2 -5 3 108095. 1446.62 3 2 -5 -3 108481. 990.838 1 -1 5 3 119830. 1112.81 1 1 -5 -3 120554. 1141.36 1 1 -5 -3 120758. 771.374 3 -1 -5 3 121468. 1494.31 3 0 5 3 4757.89 257.466 1 0 -5 -3 4778.52 261.263 1 0 -5 3 4414.91 315.416 3 1 5 3 19274.2 547.099 1 -1 -5 -3 19521.9 553.718 1 1 -5 3 17754.4 592.619 3 2 -5 3 99588.9 1406.57 3 2 5 3 103083. 1361.13 1 3 -5 3 21077.0 678.220 3 3 5 3 21759.3 677.702 1 4 5 3 135910. 1791.58 1 4 -5 3 134967. 1758.43 3 5 -5 3 44184.5 1055.64 3 5 5 3 42763.9 1083.93 1 6 5 3 21329.2 813.499 1 7 5 3 28234.4 985.924 1 8 5 3 67870.7 1600.24 1 9 5 3 880.016 250.411 1 10 5 3 56.6629 215.678 1 10 -5 3-103.718 217.626 1 11 -5 3 4617.65 517.929 1 11 5 3 5273.74 565.329 1 12 -5 3 2316.28 401.709 1 12 5 3 1790.98 371.781 1 13 -5 3 313.003 258.610 1 13 5 3-412.644 280.968 1 14 -5 3 717.634 315.965 1 14 5 3 888.685 352.726 1 15 -5 3 408.357 311.965 1 15 6 -3 800.531 349.043 1 14 6 -3 25.1808 246.706 1 13 6 -3 644.014 284.937 1 12 6 -3 2534.94 400.789 1 11 6 -3-110.968 243.905 1 10 6 -3 1586.18 303.611 1 10 -6 -3 1112.32 180.145 1 9 6 -3 22558.6 962.701 1 9 -6 -3 21425.4 641.067 1 8 6 -3 8301.36 571.495 1 8 -6 -3 6946.24 347.763 1 -7 6 3 7258.65 321.375 3 7 6 -3 7231.61 510.300 1 -6 -6 3 14605.5 667.318 3 6 6 -3 15075.2 671.605 1 -6 6 3 15137.9 397.554 3 -5 6 3 356.820 67.1276 3 -5 -6 3 224.038 181.703 3 4 -6 -3 31444.4 571.261 1 -4 6 3 30323.3 386.154 3 -3 -6 3 86720.5 1409.52 3 3 -6 -3 85061.9 961.015 1 2 -6 -3 203626. 1586.35 1 2 -6 -3 202556. 987.705 3 -2 -6 3 200863. 2108.32 3 -1 -6 3 86345.0 1353.68 3 1 -6 -3 89137.6 1128.30 1 1 -6 -3 89591.2 787.239 3 0 6 3 20968.1 572.745 1 0 -6 -3 21599.2 589.029 1 0 -6 3 20258.3 660.975 3 1 -6 3 87072.3 1369.37 3 1 6 3 88880.6 1245.31 1 2 -6 3-55.2754 146.263 3 2 6 3-178.286 153.041 1 3 6 3 10316.5 507.332 1 3 -6 3 9114.57 476.779 3 4 6 3 773.701 237.210 1 4 -6 3 304.181 170.875 3 5 -6 3 46573.8 1113.18 3 5 6 3 48725.6 1207.28 1 6 -6 3 2592.93 298.990 3 6 6 3 3378.68 371.972 1 7 6 3 42537.1 1243.47 1 8 6 3 7760.61 604.879 1 9 6 3 12147.7 760.926 1 10 6 3 864.732 323.043 1 11 -6 3 9490.42 716.887 1 11 6 3 9768.08 746.300 1 12 6 3 1444.20 352.636 1 12 -6 3 881.007 291.140 1 13 6 3 9785.07 826.531 1 13 -6 3 10146.3 789.604 1 14 -6 3 1616.01 385.913 1 14 6 3 2147.69 476.892 1 15 -6 3 5116.80 617.741 1 15 7 -3 782.313 329.207 1 14 7 -3 864.499 315.004 1 13 7 -3 4456.83 544.754 1 12 7 -3 464.781 252.475 1 11 7 -3 2026.56 353.042 1 10 7 -3-317.589 259.920 1 9 -7 -3 3585.78 288.302 1 9 7 -3 4253.17 455.585 1 8 7 -3 1747.12 325.995 1 8 -7 -3 1036.05 168.342 1 7 7 -3 77.6739 201.796 1 -7 -7 3 76.0594 201.657 3 -6 7 3 2086.17 157.313 3 -6 -7 3 1872.36 289.568 3 -5 -7 3 4129.81 378.804 3 -5 7 3 4351.20 189.070 3 4 -7 -3 619.754 115.815 1 -4 7 3 729.137 73.3813 3 -4 -7 3 597.706 194.522 3 3 -7 -3 3168.97 221.467 1 -3 -7 3 2977.37 305.714 3 3 -7 -3 2906.31 134.598 3 2 -7 -3 303.692 62.0143 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352.636 3 -7 -8 3 50501.0 1395.99 3 -6 -8 3 456.288 250.243 3 5 -8 -3 15476.3 500.647 1 -5 8 3 15578.2 367.245 3 -5 -8 3 14940.9 727.047 3 -4 -8 3 7317.44 497.460 3 4 -8 -3 7729.37 367.746 1 3 -8 -3 9398.21 412.249 1 -3 -8 3 8248.75 500.897 3 3 -8 -3 9080.44 277.075 3 -2 -8 3-378.985 232.514 3 2 -8 -3 4.11056 62.2837 3 -1 -8 3 92.1129 186.686 3 1 -8 -3 650.270 114.885 3 0 -8 3 1111.59 245.060 3 0 -8 -3 833.714 131.756 3 1 -8 3 5201.04 388.336 3 1 8 3 5129.62 365.715 1 2 -8 3-91.3401 193.566 3 2 8 3 69.1528 149.071 1 3 -8 3 55229.2 1239.36 3 3 8 3 55868.5 1249.81 1 4 8 3 2351.60 320.994 1 4 -8 3 2408.23 319.488 3 5 -8 3 33039.5 1007.56 3 5 8 3 33924.4 1098.44 1 6 -8 3 66.3299 183.458 3 6 8 3 360.026 229.725 1 7 8 3 21440.6 963.311 1 8 8 3 2385.83 419.491 1 9 8 3 21415.5 1051.27 1 10 8 3 1230.00 343.893 1 11 8 3 1775.74 409.258 1 12 -8 3 148.837 221.442 1 12 8 3 887.610 330.784 1 13 8 3 294.453 325.799 1 13 -8 3-319.490 255.041 1 14 -8 3-21.8003 245.747 1 14 9 -3 130.685 237.270 1 13 9 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471.800 1 11 9 3 2113.88 408.345 1 12 9 3 115.307 243.706 1 13 -9 3 1973.56 396.446 1 14 -9 3 965.015 349.422 1 13 10 -3 541.757 294.101 1 12 10 -3 3173.57 508.174 1 -12 -10 3 3432.72 552.810 3 -11 -10 3 1042.80 370.930 3 -10 -10 3 159.348 271.459 3 -9 -10 3 3906.92 485.952 3 -8 -10 3 8199.97 660.205 3 -7 -10 3 1221.83 317.567 3 -6 -10 3 36.1011 236.506 3 -5 -10 3 39353.3 1237.17 3 4 -10 -3 44.5871 71.3780 3 -4 -10 3-126.059 246.036 3 3 -10 -3 1468.56 154.012 3 -3 -10 3 1298.55 250.004 3 -2 -10 3 1339.12 282.108 3 2 -10 -3 1560.35 164.419 3 1 -10 -3 50350.0 911.095 3 -1 -10 3 50356.3 1292.06 3 0 -10 3 26796.6 944.729 3 0 -10 -3 27862.1 727.316 3 1 -10 3-641.648 285.421 3 -1 -10 -3 52.8990 120.676 3 2 -10 3 5.32479 187.892 3 2 10 3-40.6657 183.302 1 -2 -10 -3-298.923 194.199 3 3 10 3 1455.32 248.403 1 3 -10 3 1932.11 302.319 3 4 10 3 3917.02 408.698 1 4 -10 3 4236.70 408.321 3 5 -10 3 319.619 164.847 3 5 10 3 452.721 228.350 1 6 10 3 7134.55 591.683 1 6 -10 3 7589.57 550.700 3 7 -10 3 1214.83 279.144 3 7 10 3 1110.52 293.548 1 8 10 3 754.183 314.285 1 9 10 3 655.270 320.838 1 10 10 3 3020.68 490.833 1 11 10 3 5972.28 668.112 1 12 10 3-198.121 276.056 1 13 -10 3 134.930 249.723 1 -11 -11 3 1476.40 354.496 3 -10 -11 3 2383.64 431.723 3 -9 -11 3 6811.28 643.683 3 -8 -11 3-300.331 259.745 3 -7 -11 3 1672.24 378.178 3 -6 -11 3 2134.34 360.464 3 -5 -11 3 7748.98 597.048 3 -4 -11 3 3938.47 431.765 3 4 -11 -3 4203.78 249.057 3 -3 -11 3 8055.92 587.165 3 3 -11 -3 8263.19 362.397 3 2 -11 -3 3314.44 255.485 3 -2 -11 3 3283.83 399.909 3 1 -11 -3 3857.60 289.416 3 -1 -11 3 4190.60 451.468 3 0 -11 3 798.825 229.324 3 0 -11 -3 1275.58 200.609 3 1 -11 3 7660.24 536.234 3 -1 -11 -3 8338.19 454.138 3 -2 -11 -3 5783.46 407.523 3 2 -11 3 6266.11 498.906 3 3 11 3 1751.63 307.550 1 3 -11 3 1499.41 264.751 3 -3 -11 -3 1386.72 230.711 3 4 -11 3 1266.08 272.971 3 4 11 3 1568.94 306.121 1 5 11 3 517.394 205.946 1 5 -11 3 1531.98 307.093 3 6 11 3 11681.5 761.358 1 6 -11 3 12187.6 707.155 3 7 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1 9 12 3 881.740 362.713 1 10 12 3 3207.97 547.811 1 -10 -13 3 3231.90 527.406 3 -9 -13 3 928.760 363.941 3 -8 -13 3 365.367 270.670 3 -7 -13 3 1322.82 359.371 3 -6 -13 3 6905.00 647.517 3 -5 -13 3 1162.93 354.152 3 -4 -13 3 447.892 274.805 3 -3 -13 3 8292.51 648.749 3 -2 -13 3 1863.16 351.898 3 1 -13 -3 5981.66 397.502 3 -1 -13 3 6395.86 561.434 3 0 -13 3 1448.28 294.812 3 0 -13 -3 1257.07 208.357 3 1 -13 3-337.689 252.382 3 -1 -13 -3 121.843 155.349 3 2 -13 3 296.408 216.276 3 -2 -13 -3 493.825 169.786 3 3 -13 3 4920.06 490.204 3 -3 -13 -3 5282.33 454.220 3 4 -13 3-207.352 213.551 3 -4 -13 -3 22.1513 190.184 3 5 -13 3 32.0920 192.510 3 -5 -13 -3-112.057 206.432 3 6 13 3 2685.52 416.983 1 -6 -13 -3 2970.60 395.783 3 6 -13 3 3365.70 423.731 3 7 13 3-180.725 250.839 1 7 -13 3 382.055 238.891 3 8 13 3 1103.76 391.129 1 9 13 3 3110.43 531.879 1 -9 -14 3 454.677 325.174 3 -8 -14 3 588.113 336.639 3 -7 -14 3 7375.22 704.028 3 -6 -14 3 937.212 359.911 3 -5 -14 3 1720.28 391.233 3 -4 -14 3 179.964 282.683 3 -3 -14 3 18632.9 987.781 3 -2 -14 3 12550.2 801.418 3 -1 -14 3-154.429 247.390 3 0 -14 3 1916.18 360.677 3 0 -14 -3 2388.82 290.760 3 -1 -14 -3 4418.88 393.704 3 1 -14 3 4653.58 491.292 3 2 -14 3 2861.73 413.691 3 -2 -14 -3 2619.69 326.301 3 3 -14 3 754.346 283.869 3 -3 -14 -3 273.913 196.618 3 -4 -14 -3 36.6893 184.039 3 4 -14 3-129.128 227.210 3 5 -14 3 1505.11 306.985 3 -5 -14 -3 1810.67 319.155 3 6 -14 3 290.017 248.955 3 6 14 3-72.4094 225.398 1 -6 -14 -3 431.312 267.696 3 7 -14 3 240.279 211.619 3 -7 -14 -3 979.715 298.852 3 7 14 3 1219.82 380.521 1 8 14 3 132.664 254.413 1 -8 -14 -3 563.838 315.624 3 9 14 3 649.640 322.892 1 -8 -15 3 411.099 308.405 3 -7 -15 3-100.095 256.257 3 -6 -15 3 2679.55 471.314 3 -5 -15 3-162.666 245.528 3 -4 -15 3 3671.85 493.755 3 -3 -15 3 230.221 231.754 3 -2 -15 3 135.010 226.215 3 -1 -15 3 1504.90 333.490 3 0 -15 3 8624.44 676.333 3 1 -15 3 685.678 279.224 3 2 -15 3 3122.58 457.687 3 -2 -15 -3 2675.59 369.546 3 -3 -15 -3 6383.65 541.002 3 3 -15 3 5245.55 529.396 3 -4 -15 -3 2143.62 342.227 3 4 -15 3 2016.43 359.000 3 5 -15 3 220.392 259.616 3 -5 -15 -3 468.138 271.802 3 6 -15 3 3581.18 468.442 3 -6 -15 -3 2390.56 409.264 3 -7 -15 -3 4678.05 547.714 3 7 -15 3 4243.23 508.554 3 -8 -15 -3 25.5748 234.204 3 -9 -15 -3-382.695 301.442 3 -6 -16 3 370.471 281.921 3 -5 -16 3 1079.13 341.230 3 -4 -16 3-565.648 321.616 3 -3 -16 3-123.090 254.067 3 -2 -16 3-152.796 252.762 3 -1 -16 3 30.0575 218.832 3 0 -16 3 635.229 295.652 3 1 -16 3 5379.11 584.244 3 2 -16 3 3078.53 463.066 3 3 -16 3 401.914 252.016 3 4 -16 3 157.125 225.260 3 -4 -16 -3 531.480 257.068 3 5 -16 3 1098.72 329.632 3 -5 -16 -3 1221.88 335.621 3 -6 -16 -3 863.457 313.886 3 -7 -16 -3 1019.25 347.092 3 -8 -16 -3-9.21783 250.631 3 -5 -17 3 244.155 256.748 3 -4 -17 3 323.247 267.899 3 -3 -17 3 3163.58 500.064 3 -2 -17 3 1652.96 403.171 3 -1 -17 3 864.560 332.806 3 0 -17 3 1645.06 377.493 3 1 -17 3 5067.52 578.072 3 2 -17 3 2571.60 449.004 3 3 -17 3 810.574 321.099 3 -3 -18 3 642.294 330.307 3 -2 -18 3 5242.05 623.484 3 -1 -18 3 138.614 245.791 3 0 -18 3 282.218 280.468 3 1 -18 3 719.997 321.013 3 2 -18 3 1225.59 370.045 3 -13 0 4 2360.23 362.173 2 12 0 -4 14684.6 717.459 1 -12 0 4 13551.0 719.856 2 11 0 -4 24440.2 870.204 1 -11 0 4 24086.8 912.412 2 10 0 -4 16038.8 658.589 1 -10 0 4 15759.8 725.125 2 9 0 -4 769.034 171.523 1 -9 0 4 1045.18 251.384 2 -8 0 4 7307.28 486.790 2 8 0 -4 6251.71 362.221 1 -8 0 4 6482.04 347.811 1 -7 0 4 422154. 2458.06 1 7 0 -4 418399. 2605.62 1 6 0 -4 142218. 1386.15 1 -6 0 4 145563. 1314.90 1 -5 0 4 2239.32 161.000 1 -4 0 4 42393.3 596.823 1 -4 0 4 42641.8 721.840 3 -3 0 4 53329.6 754.176 3 -3 0 4 53778.5 630.710 1 2 0 -4 2811.23 175.861 3 -2 0 4 2809.62 179.536 3 -1 0 4 6188.84 261.400 3 1 0 -4 5935.96 251.142 3 0 0 4 215.620 104.013 3 0 0 -4 90.1060 73.8640 3 1 0 4 1867.74 174.798 3 -1 0 -4 1891.00 170.881 3 2 0 4 110758. 1290.92 3 3 0 4 43350.4 494.453 2 5 0 4 32009.1 899.103 1 6 0 4 1050.08 206.398 1 7 0 4 1723.76 267.365 1 8 0 4 65595.6 1502.91 1 9 0 4 10913.5 655.563 1 10 0 4 8043.63 600.505 1 11 0 4 231.023 248.915 1 12 0 4 301.822 243.888 1 13 0 4-137.389 274.109 1 14 0 4 419.349 246.048 1 15 0 4-343.309 311.691 1 13 1 -4 10449.8 668.210 1 -13 1 4 9821.64 637.220 2 -13 -1 4 9763.69 636.804 2 -12 -1 4 6623.17 527.513 2 -12 1 4 6670.07 510.775 2 12 1 -4 7497.96 539.421 1 12 -1 -4 6974.73 477.272 1 -11 -1 4 207.091 226.088 2 -11 1 4 248.140 200.843 2 11 1 -4 350.868 190.270 1 11 -1 -4 47.3137 166.649 1 10 1 -4 12837.7 609.792 1 10 -1 -4 12982.9 567.218 1 -10 1 4 13101.5 654.182 2 9 -1 -4 31973.8 815.699 1 9 1 -4 31445.4 883.784 1 -9 1 4 31372.8 971.272 2 -8 1 4 13433.6 644.505 2 8 1 -4 13832.8 552.772 1 8 -1 -4 13223.5 483.372 1 -7 1 4 1284.54 330.365 2 -7 1 4 1432.01 155.370 1 7 -1 -4 122.071 101.962 1 -7 -1 4 630.310 149.794 1 7 1 -4 281.424 159.016 1 6 -1 -4 149144. 1254.25 1 -6 1 4 154703. 1881.41 2 -6 -1 4 152841. 1520.92 1 6 1 -4 148034. 1545.16 1 -6 1 4 149617. 1190.98 1 -5 -1 4 49294.5 908.012 3 -5 1 4 51584.8 1044.58 2 -5 -1 4 47565.8 788.757 1 -5 1 4 49186.5 582.590 1 -4 -1 4 117.109 106.969 3 -4 1 4-43.6094 160.082 2 -4 1 4 88.4626 41.4997 1 -4 -1 4 7.48871 65.0962 1 -4 1 4 190.662 78.0956 3 -3 1 4 2841.60 160.195 3 -3 1 4 2880.05 260.280 2 -3 -1 4 2763.70 175.544 1 -3 -1 4 2859.51 207.381 3 -3 1 4 2706.45 111.663 1 2 1 -4 16958.7 454.105 3 -2 1 4 16664.3 361.155 3 -2 -1 4 17402.7 462.910 3 2 -1 -4 16989.0 355.379 3 -2 1 4 16737.1 517.378 2 1 -1 -4 112002. 954.059 3 -1 1 4 112437. 1235.12 2 -1 1 4 114419. 961.454 3 1 1 -4 113906. 1171.24 3 -1 -1 4 113494. 1174.33 3 0 1 4 190961. 1495.88 2 0 -1 4 194109. 1580.71 3 0 1 4 195803. 1357.74 3 0 1 -4 192371. 1575.95 3 0 -1 -4 192837. 1374.95 3 1 -1 4 104244. 1211.94 3 -1 -1 -4 103634. 1112.53 3 1 1 4 103045. 1000.81 2 -2 -1 -4 754.508 121.674 3 2 -1 4 895.044 156.773 3 2 1 4 929.315 152.272 1 2 1 4 760.340 96.6770 2 3 -1 4 19012.3 595.464 3 3 1 4 18865.4 592.781 1 4 1 4 133832. 1672.41 1 5 1 4 212472. 2274.08 1 6 1 4 234.600 154.263 1 6 -1 4 265.724 168.697 1 7 -1 4 5703.69 455.191 1 7 1 4 5571.34 437.608 1 8 -1 4 696.012 260.037 1 8 1 4 1074.63 257.707 1 9 1 4 12885.4 726.122 1 9 -1 4 13361.0 737.420 1 10 -1 4 87.9531 208.929 1 10 1 4 4.35317 228.734 1 11 -1 4 29.7109 223.122 1 11 1 4 10.0991 232.595 1 12 1 4 788.408 314.084 1 12 -1 4 1787.45 384.547 1 13 1 4 92.0435 247.594 1 13 -1 4 124.331 239.145 1 14 1 4 9.44863 291.951 1 14 -1 4-277.566 309.158 1 15 1 4 53.5257 267.607 1 15 -1 4 91.1906 250.937 1 -13 -2 4-37.5413 239.195 2 -13 2 4 526.075 218.952 2 -12 -2 4 306.144 236.707 2 12 2 -4 747.355 238.992 1 -12 2 4-2.29380 227.948 2 -11 2 4-39.7795 208.751 2 11 2 -4 209.569 190.092 1 11 -2 -4-119.840 164.887 1 -10 2 4 3544.81 349.543 2 10 2 -4 3462.58 352.169 1 10 -2 -4 3634.29 290.582 1 -9 2 4 1430.44 263.897 2 9 2 -4 1723.58 262.941 1 9 -2 -4 1259.83 177.211 1 -8 2 4 157.433 197.177 2 8 2 -4-11.1658 147.150 1 8 -2 -4-76.7798 101.854 1 7 2 -4 9625.89 460.809 1 7 -2 -4 10128.2 340.100 1 -7 2 4 9809.96 513.330 2 6 2 -4 3334.63 257.042 1 6 -2 -4 3386.84 168.191 1 -6 2 4 3593.59 322.684 2 -5 -2 4 5437.51 336.788 3 -5 -2 4 5522.70 308.773 1 -5 2 4 5160.54 361.798 2 -4 -2 4 3733.73 240.225 1 -4 -2 4 3872.86 264.834 3 -4 2 4 3724.71 176.033 3 -4 2 4 3831.24 299.499 2 -3 -2 4 5443.57 276.023 1 -3 2 4 5539.93 184.415 3 -3 -2 4 5411.25 297.894 3 -3 2 4 5496.13 327.618 2 -2 2 4 4489.37 155.547 3 -2 2 4 4197.74 276.999 2 -2 -2 4 4412.67 269.452 3 2 -2 -4 4450.53 152.418 3 2 2 -4 4778.36 273.514 3 -2 2 4 4192.39 119.343 1 1 -2 -4 82039.2 722.901 3 -1 -2 4 81927.5 1080.07 3 -1 2 4 80661.6 719.349 1 -1 2 4 79879.5 1063.57 2 -1 2 4 82529.2 705.684 3 0 -2 -4 5240.27 215.719 3 0 -2 4 5320.57 301.024 3 0 2 4 5251.03 266.462 2 0 2 4 5346.76 234.240 1 -1 -2 -4 40744.9 671.220 3 -1 -2 -4 41538.5 682.235 2 1 2 4 40754.0 657.048 2 1 2 4 41023.0 714.240 1 1 -2 4 40870.4 815.563 3 -2 -2 -4 81639.5 1074.72 3 -2 -2 -4 80116.5 876.215 2 2 -2 4 79592.5 1185.50 3 2 2 4 81085.8 1103.32 1 -3 -2 -4 125316. 996.311 2 3 -2 4 128163. 1585.02 3 3 2 4 127623. 1521.05 1 4 2 4 13921.2 551.784 1 5 2 4 98662.4 1554.65 1 6 2 4 12461.8 609.072 1 6 -2 4 9903.73 201.545 2 7 2 4 25077.8 911.742 1 8 -2 4 3640.07 430.647 1 8 2 4 2781.21 348.116 1 9 2 4 27609.4 1064.15 1 9 -2 4 31957.1 1119.59 1 10 2 4 12596.0 773.319 1 10 -2 4 13236.7 782.815 1 11 -2 4 2252.92 383.631 1 11 2 4 2530.26 402.171 1 12 2 4 3796.71 509.243 1 12 -2 4 3137.41 470.065 1 13 -2 4 1709.21 393.407 1 13 2 4 1679.65 390.800 1 14 2 4 2114.08 442.799 1 14 -2 4 1706.57 395.622 1 15 -2 4 92.3844 261.469 1 15 2 4 220.543 277.981 1 14 3 -4 2722.83 402.747 1 13 3 -4 4130.38 470.336 1 -12 3 4 4036.77 391.736 2 12 3 -4 5396.88 489.350 1 -11 3 4 489.807 195.617 2 11 3 -4 1088.62 257.695 1 10 -3 -4 6225.99 368.892 1 10 3 -4 6262.76 491.036 1 -10 3 4 6177.32 466.059 2 -9 3 4 447.386 213.957 2 9 -3 -4 387.774 113.878 1 8 -3 -4 5302.16 271.783 1 8 3 -4 5613.43 414.702 1 -8 3 4 5451.28 430.448 2 7 3 -4 39833.7 985.338 1 7 -3 -4 39158.2 609.499 1 -7 3 4 38844.3 1016.52 2 6 3 -4 25104.0 733.652 1 -6 -3 4 25750.2 781.971 3 -6 3 4 26336.7 797.194 2 6 -3 -4 24867.6 379.495 1 -5 -3 4 4748.34 331.099 3 -5 3 4 5476.75 374.929 2 -4 3 4 46770.3 491.159 3 -4 -3 4 47703.7 962.820 3 -4 3 4 49112.7 996.495 2 -3 -3 4 68157.6 1096.32 3 -3 -3 4 68047.4 1054.02 1 -3 3 4 70900.0 1148.59 2 -2 -3 4 6073.90 336.954 3 -2 3 4 5959.76 334.958 2 -2 3 4 5786.53 144.641 1 -1 3 4 1034.43 167.060 2 1 -3 -4 908.863 75.3320 3 -1 -3 4 917.713 166.718 3 -1 3 4 1059.17 97.4740 1 0 -3 -4 5299.79 207.339 3 0 -3 4 5916.78 332.060 3 0 3 4 5136.33 226.396 1 1 -3 4 37641.5 824.537 3 1 3 4 37993.9 701.434 1 -1 -3 -4 38553.0 704.670 2 -1 -3 -4 38113.7 720.351 1 2 -3 4 66264.3 1123.97 3 2 3 4 63666.7 1004.71 1 -2 -3 -4 66314.1 872.950 2 -2 -3 -4 65215.0 1044.02 1 3 3 4 87802.8 1282.47 1 -3 -3 -4 88563.0 944.078 2 3 -3 4 89621.5 1368.09 3 4 -3 4 25871.5 779.650 3 4 3 4 24615.6 737.617 1 -4 -3 -4 25348.7 471.155 2 5 3 4 839.575 182.227 1 -5 -3 -4 1258.50 105.193 2 6 3 4 68166.3 1418.40 1 -6 -3 -4 65196.4 615.487 2 7 3 4 17746.5 789.035 1 7 -3 4 15274.5 335.102 2 8 3 4 35861.1 1155.57 1 9 -3 4 42025.0 1295.25 1 9 3 4 39722.0 1274.98 1 10 -3 4 1565.30 338.261 1 10 3 4 897.319 269.846 1 11 3 4 725.770 297.675 1 11 -3 4 668.346 284.025 1 12 3 4 13219.5 883.790 1 12 -3 4 15023.0 902.796 1 13 3 4 9040.81 772.717 1 13 -3 4 9733.62 763.045 1 14 3 4-26.4054 259.702 1 14 -3 4 274.477 246.081 1 15 -3 4 1121.02 356.619 1 14 4 -4 85.4032 222.558 1 13 4 -4 3548.58 459.446 1 12 4 -4 734.598 226.217 1 11 4 -4-284.555 215.153 1 10 4 -4 494.783 210.487 1 10 -4 -4 168.431 108.138 1 9 4 -4 18978.5 814.705 1 9 -4 -4 17586.7 517.705 1 8 4 -4 31223.8 988.604 1 8 -4 -4 31777.8 605.484 1 -8 4 4 32095.6 960.065 2 7 4 -4 57040.1 1237.29 1 7 -4 -4 54860.3 662.506 1 -7 4 4 58800.4 1238.33 2 -6 4 4 14893.6 620.069 2 6 -4 -4 13641.4 250.589 1 -6 -4 4 14376.7 624.658 3 -5 -4 4 63840.3 1229.58 3 -5 4 4 65541.5 1224.54 2 -4 -4 4 109030. 1533.20 3 -4 4 4 110871. 1520.52 2 -3 -4 4 4182.03 300.724 3 -2 -4 4 20884.2 646.052 3 -2 4 4 20514.0 332.615 1 2 -4 -4 20295.6 337.411 1 -1 -4 4 21781.3 653.560 3 -1 4 4 21803.9 425.261 1 1 -4 -4 21354.9 308.607 3 1 -4 -4 20700.1 429.314 1 0 -4 4 2368.74 243.570 3 0 4 4 2295.36 175.806 1 0 -4 -4 2360.21 175.178 1 1 -4 4 28783.2 759.133 3 1 4 4 27011.1 626.014 1 -1 -4 -4 28635.0 663.754 2 -1 -4 -4 26998.4 635.897 1 2 -4 4 9881.22 465.809 3 2 4 4 9220.58 409.433 1 -2 -4 -4 10057.7 379.620 2 3 4 4 20335.8 652.098 1 3 -4 4 21233.5 699.873 3 4 4 4 17914.6 656.977 1 4 -4 4 17513.2 667.559 3 5 4 4 125.199 152.778 1 5 -4 4 237.386 144.665 3 6 4 4 1490.30 269.246 1 7 4 4 64747.1 1508.25 1 8 4 4 1416.70 273.214 1 9 4 4 3042.50 382.274 1 10 4 4-83.9639 250.421 1 10 -4 4 121.221 228.486 1 11 4 4 31574.1 1280.03 1 11 -4 4 31227.8 1230.58 1 12 4 4 67.0108 221.942 1 12 -4 4 120.758 241.867 1 13 4 4-246.383 285.752 1 13 -4 4 3.03107 223.978 1 14 -4 4-13.5156 225.735 1 14 4 4 301.463 281.402 1 15 -4 4 540.847 326.135 1 15 5 -4 3115.04 477.723 1 14 5 -4-109.018 239.140 1 13 5 -4 2494.07 395.443 1 12 5 -4 3671.62 457.002 1 11 5 -4 2568.62 375.646 1 10 5 -4-53.7795 204.483 1 9 5 -4 7001.13 522.924 1 9 -5 -4 5810.38 292.362 1 8 -5 -4 521.311 98.5133 1 8 5 -4 829.493 226.740 1 -7 -5 4 14788.5 706.235 3 7 -5 -4 14569.9 337.788 1 -7 5 4 14213.5 405.203 3 -6 5 4 49575.5 628.654 3 -6 -5 4 49834.5 1199.72 3 6 -5 -4 47703.4 490.626 1 -5 -5 4 39083.4 1021.20 3 -5 5 4 35194.0 382.160 3 -4 -5 4 43562.3 1037.44 3 3 -5 -4 462.023 63.2203 1 -3 -5 4 273.732 157.768 3 -2 -5 4 62412.5 1164.45 3 2 -5 -4 60575.0 699.643 1 -1 -5 4 6677.52 399.643 3 -1 5 4 6250.34 265.600 1 1 -5 -4 6092.66 266.260 1 0 5 4 306790. 2032.67 1 0 -5 -4 311162. 2071.63 1 0 -5 4 314708. 2592.14 3 1 5 4 19647.3 571.757 1 -1 -5 -4 19731.0 580.364 1 1 -5 4 20167.9 683.284 3 2 -5 4 1597.57 239.010 3 2 5 4 1805.13 217.356 1 3 -5 4 18999.9 687.291 3 3 5 4 19514.7 659.294 1 4 -5 4 308.970 171.577 3 4 5 4 212.827 130.995 1 5 5 4 4845.36 394.780 1 5 -5 4 4647.21 381.732 3 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6 4 78045.1 1013.10 1 1 -6 -4 77323.7 681.104 3 1 -6 -4 77170.2 1035.91 1 0 6 4 46821.3 852.241 1 0 -6 4 45566.4 1045.99 3 0 -6 -4 48243.3 896.660 1 1 -6 4 189154. 2161.18 3 1 6 4 192736. 1874.85 1 2 6 4 13219.2 548.656 1 2 -6 4 12771.2 587.459 3 3 6 4 5718.29 383.355 1 3 -6 4 5318.22 394.514 3 4 -6 4 25384.5 855.811 3 4 6 4 25524.4 840.495 1 5 6 4 7585.50 505.567 1 5 -6 4 7648.99 497.599 3 6 6 4 7933.82 539.332 1 6 -6 4 7792.48 524.978 3 7 6 4 4536.37 436.903 1 8 6 4 360.095 203.824 1 9 6 4 5442.14 537.721 1 10 6 4 978.112 296.223 1 11 -6 4 1964.97 380.826 1 11 6 4 2942.82 471.459 1 12 -6 4 0.92540 222.636 1 12 6 4 184.761 240.135 1 13 -6 4 636.179 297.518 1 13 6 4 759.577 309.198 1 14 -6 4 355.611 285.564 1 15 -6 4 279.123 281.897 1 15 7 -4 1249.58 378.434 1 14 7 -4 2068.06 415.753 1 13 7 -4-12.1315 228.536 1 12 7 -4 205.843 230.850 1 11 7 -4 51.6257 230.340 1 10 7 -4-187.150 243.333 1 -10 -7 4-159.718 225.012 3 -9 -7 4 797.497 271.353 3 8 -7 -4 68.9315 73.7917 1 -8 -7 4 285.209 201.863 3 -7 -7 4 11855.4 668.846 3 7 -7 -4 10766.1 346.947 1 -6 7 4 5774.08 176.055 3 6 -7 -4 6034.11 246.853 1 -6 -7 4 6376.74 480.403 3 5 -7 -4 4576.86 217.185 1 -5 -7 4 4229.32 397.359 3 -4 -7 4 13575.1 648.287 3 4 -7 -4 12842.5 378.378 1 3 -7 -4 4713.16 249.746 1 -3 -7 4 5496.47 434.416 3 2 -7 -4 39662.9 418.660 3 -2 -7 4 41263.1 1062.81 3 -1 -7 4 75699.7 1414.55 3 1 -7 -4 77039.8 771.872 3 1 -7 -4 77740.1 1140.40 1 0 -7 4 133876. 1870.22 3 0 7 4 135639. 1568.83 1 1 7 4 39942.4 911.444 1 1 -7 4 40504.0 1058.84 3 2 -7 4 406.535 222.774 3 2 7 4 138.847 150.908 1 3 -7 4 6186.03 449.414 3 3 7 4 6166.60 429.897 1 4 -7 4 8493.68 544.677 3 4 7 4 8871.38 535.977 1 5 -7 4 899.645 248.327 3 5 7 4 1086.17 277.661 1 6 7 4 21304.8 898.530 1 6 -7 4 19754.2 825.449 3 7 7 4 4125.51 455.010 1 8 7 4 9672.92 666.241 1 9 7 4 96.5766 251.878 1 10 7 4 3356.62 478.021 1 11 7 4 1003.82 357.822 1 12 7 4 57.6445 281.696 1 12 -7 4-84.1866 220.496 1 13 -7 4 91.5300 234.312 1 13 7 4 674.638 340.595 1 14 -7 4 1395.11 361.465 1 14 8 -4 1139.53 337.883 1 13 8 -4 415.806 288.701 1 -13 -8 4 765.112 341.868 3 12 8 -4 1168.20 356.849 1 -12 -8 4 1160.33 330.036 3 11 8 -4 1232.25 315.159 1 -11 -8 4 1450.28 355.102 3 -10 -8 4 2701.45 419.531 3 -9 -8 4 1242.58 332.726 3 -8 -8 4 1091.74 297.489 3 -7 -8 4 4764.73 475.605 3 -6 -8 4 11628.5 674.506 3 5 -8 -4 17176.5 480.759 1 -5 -8 4 16892.3 780.603 3 -4 -8 4 144.461 166.450 3 4 -8 -4 723.745 118.856 1 -3 -8 4 4887.02 409.064 3 3 -8 -4 5159.48 294.802 1 2 -8 -4 1411.08 104.134 3 2 -8 -4 1485.05 175.555 1 1 -8 -4-24.3853 80.8063 3 -1 -8 4 100.789 184.429 3 0 -8 4 4724.78 426.771 3 0 8 4 3551.60 288.144 1 0 -8 -4 4157.54 245.622 3 1 8 4 65268.9 1239.88 1 1 -8 4 65139.5 1394.93 3 2 -8 4 1213.42 247.280 3 2 8 4 912.176 199.918 1 3 8 4 6031.76 448.494 1 3 -8 4 5372.04 438.005 3 4 -8 4 15309.6 719.824 3 4 8 4 14844.3 706.634 1 5 8 4 22711.1 903.737 1 5 -8 4 20897.8 870.656 3 6 -8 4 5388.32 476.606 3 6 8 4 5206.08 500.883 1 7 -8 4 1690.99 317.529 3 7 8 4 2222.08 393.857 1 8 8 4 151.091 226.908 1 9 8 4 21612.4 1060.45 1 10 8 4 247.432 303.184 1 11 8 4 1863.73 398.948 1 12 8 4 2771.11 481.712 1 13 -8 4-129.910 270.950 1 13 8 4-465.271 332.650 1 14 -8 4-377.177 308.656 1 -13 -9 4 550.143 334.655 3 -12 -9 4 4956.94 599.439 3 -11 -9 4 2365.01 433.706 3 -10 -9 4 627.556 310.256 3 -9 -9 4 82.0664 245.657 3 -8 -9 4 1317.81 333.286 3 -7 -9 4 4244.52 466.786 3 -6 -9 4 6159.85 517.856 3 -5 -9 4 288.282 239.680 3 -4 -9 4 2889.05 351.632 3 -3 -9 4 21550.5 869.736 3 3 -9 -4 21335.9 351.961 3 -2 -9 4 9143.12 565.089 3 2 -9 -4 9550.67 296.993 3 1 -9 -4 2469.63 183.519 3 -1 -9 4 2049.96 290.469 3 0 -9 -4 39780.7 769.417 3 0 -9 4 40520.9 1146.43 3 1 -9 4 21527.4 849.345 3 1 9 4 22426.2 773.785 1 2 9 4 2284.25 291.713 1 2 -9 4 1766.50 283.478 3 3 -9 4 10285.8 611.988 3 3 9 4 10695.2 592.648 1 4 9 4 7472.53 527.517 1 4 -9 4 6372.66 510.384 3 5 9 4 8447.02 589.708 1 5 -9 4 8992.85 592.301 3 6 9 4 1821.78 346.737 1 6 -9 4 1340.26 289.336 3 7 -9 4-242.238 230.316 3 7 9 4 143.447 261.967 1 8 9 4 924.169 315.614 1 9 9 4 2009.37 399.004 1 10 9 4 778.753 346.111 1 11 9 4 469.925 303.928 1 12 9 4 972.140 331.228 1 13 -9 4-174.002 263.941 1 14 -9 4-179.126 299.698 1 -12 -10 4 740.454 337.031 3 -11 -10 4 1747.60 420.572 3 -10 -10 4 4234.12 541.430 3 -9 -10 4 1387.40 341.081 3 -8 -10 4 7606.15 648.271 3 -7 -10 4-13.6218 233.557 3 -6 -10 4 9328.30 659.559 3 -5 -10 4 1306.00 272.100 3 -4 -10 4 24355.5 976.094 3 -3 -10 4 968.536 290.098 3 3 -10 -4 750.309 88.8548 3 2 -10 -4 5714.29 261.927 3 -2 -10 4 5542.89 482.398 3 -1 -10 4 7384.93 540.815 3 1 -10 -4 7135.31 326.875 3 0 -10 -4 4180.84 278.859 3 0 -10 4 4385.15 423.713 3 1 10 4 1840.90 255.869 1 1 -10 4 1362.61 228.766 3 -1 -10 -4 1742.23 199.955 3 2 -10 4 4917.72 437.856 3 2 10 4 3931.35 377.499 1 3 10 4 113.327 179.188 1 3 -10 4 168.059 198.001 3 4 10 4 9105.92 613.941 1 4 -10 4 9066.12 613.819 3 5 10 4 7659.77 589.294 1 5 -10 4 7234.46 559.346 3 6 -10 4 6952.80 553.471 3 6 10 4 6133.05 553.946 1 7 -10 4 5450.83 526.592 3 7 10 4 5394.51 552.758 1 8 10 4 7898.30 680.774 1 9 10 4 5215.34 615.407 1 10 10 4 499.065 257.848 1 11 10 4 4405.42 600.368 1 13 -10 4 1004.02 335.897 1 -11 -11 4 461.872 334.058 3 -10 -11 4 428.948 286.635 3 -9 -11 4 1543.18 383.539 3 -8 -11 4 1433.72 344.844 3 -7 -11 4 13581.0 839.865 3 -6 -11 4 128.332 229.153 3 -5 -11 4 2086.38 342.608 3 -4 -11 4 7725.90 602.108 3 -3 -11 4 12365.5 744.106 3 2 -11 -4 12510.4 419.637 3 -2 -11 4 12984.8 742.333 3 -1 -11 4 11700.5 689.415 3 1 -11 -4 10625.4 422.419 3 0 -11 -4 2108.44 224.763 3 0 -11 4 1674.98 301.124 3 1 -11 4 1371.56 272.213 3 -1 -11 -4 1908.24 231.475 3 2 -11 4 4988.58 467.312 3 2 11 4 4326.20 406.274 1 -2 -11 -4 4497.23 354.173 3 3 11 4 4971.67 469.923 1 3 -11 4 5402.65 488.060 3 4 11 4 9074.12 627.624 1 4 -11 4 9024.98 634.154 3 5 11 4 1246.58 319.062 1 5 -11 4 924.341 271.198 3 6 -11 4 1472.36 341.321 3 6 11 4 1481.10 345.125 1 7 11 4 10669.4 778.162 1 7 -11 4 9705.95 709.165 3 8 11 4 9762.16 774.457 1 9 11 4 720.933 317.954 1 10 11 4 2330.62 454.752 1 11 11 4 3325.54 549.156 1 -10 -12 4 1579.85 391.029 3 -9 -12 4 8607.66 772.695 3 -8 -12 4 1062.10 371.275 3 -7 -12 4 11992.5 840.797 3 -6 -12 4 238.543 262.075 3 -5 -12 4 10290.7 742.720 3 -4 -12 4 371.376 312.259 3 -3 -12 4 13585.0 794.481 3 -2 -12 4 5702.62 522.158 3 -1 -12 4 1713.00 317.173 3 1 -12 -4 1728.80 198.294 3 0 -12 4 1675.05 319.236 3 0 -12 -4 2059.89 226.191 3 1 -12 4-126.213 242.334 3 -1 -12 -4 259.580 142.132 3 2 -12 4 1460.10 308.737 3 -2 -12 -4 1232.89 213.787 3 3 12 4 282.838 197.939 1 3 -12 4 903.117 255.564 3 -3 -12 -4 604.441 191.738 3 4 -12 4 2874.22 395.055 3 4 12 4 2803.78 381.231 1 5 -12 4 2591.62 387.787 3 5 12 4 1847.07 335.960 1 6 -12 4 4266.01 473.778 3 6 12 4 4387.64 531.202 1 7 -12 4 664.924 300.973 3 7 12 4 780.416 328.330 1 8 -12 4 1645.47 375.389 3 8 12 4 1025.78 356.231 1 9 12 4 2071.83 454.457 1 10 12 4 1226.45 390.931 1 -9 -13 4 9427.59 814.543 3 -8 -13 4 476.529 320.526 3 -7 -13 4 2105.84 448.097 3 -6 -13 4 2207.01 417.921 3 -5 -13 4 1769.04 379.935 3 -4 -13 4 296.743 234.138 3 -3 -13 4 647.110 294.092 3 -2 -13 4 5559.63 548.191 3 -1 -13 4 393.877 243.392 3 0 -13 4 236.774 224.848 3 -1 -13 -4 1490.98 224.135 3 1 -13 4 1375.45 324.926 3 -2 -13 -4 22679.7 825.369 3 2 -13 4 22273.3 1023.49 3 3 -13 4 3217.61 441.252 3 -3 -13 -4 2982.88 337.968 3 4 -13 4 5105.47 512.400 3 4 13 4 3854.79 447.728 1 -4 -13 -4 5150.00 457.423 3 5 -13 4 59.7438 201.742 3 -5 -13 -4 257.147 204.410 3 5 13 4-49.3494 276.473 1 6 13 4 3530.28 479.056 1 6 -13 4 4533.23 519.247 3 7 -13 4 126.099 207.074 3 7 13 4 155.999 271.856 1 8 13 4 656.725 355.581 1 8 -13 4 515.450 283.920 3 9 13 4 2594.44 500.194 1 -8 -14 4 3807.16 554.679 3 -7 -14 4 575.707 306.774 3 -6 -14 4 2567.91 465.189 3 -5 -14 4 1732.82 398.282 3 -4 -14 4 89.5421 221.870 3 -3 -14 4 1279.86 343.221 3 -2 -14 4 148.717 226.001 3 -1 -14 4 518.830 251.860 3 0 -14 4 2018.43 353.585 3 1 -14 4 180.961 263.015 3 -2 -14 -4 10111.2 583.331 3 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2 -6 -4 5 25699.7 852.233 3 -6 4 5 25603.9 455.986 3 -6 4 5 26466.3 873.459 2 -5 4 5 35310.9 413.863 3 -5 -4 5 37273.9 979.229 3 -5 4 5 37429.8 1012.80 2 -4 -4 5 52671.6 1120.61 3 -4 4 5 54827.3 1154.31 2 -3 -4 5 6161.06 390.735 3 -3 4 5 6238.99 400.276 2 -2 -4 5 21288.2 689.456 3 -2 4 5 21547.5 365.576 1 -2 4 5 20716.0 652.516 2 -1 -4 5 91716.9 1412.63 3 1 -4 -5 90896.4 776.966 3 -1 4 5 91525.2 923.695 1 0 -4 -5 45051.1 665.316 3 0 -4 5 45295.4 1011.46 3 0 4 5 45282.2 763.316 1 -1 -4 -5 5945.28 290.275 3 1 4 5 5849.76 311.047 1 1 -4 5 5846.16 388.453 3 2 -4 5 1192.04 219.502 3 -2 -4 -5 1001.45 140.427 2 2 4 5 871.931 155.867 1 3 4 5 8313.11 448.548 1 -3 -4 -5 8511.15 355.336 2 3 -4 5 8448.20 479.044 3 4 -4 5 6531.66 450.115 3 4 4 5 5975.48 411.229 1 -4 -4 -5 6390.07 293.293 2 5 -4 5-99.9105 193.138 3 5 4 5-84.2809 192.509 1 -5 -4 -5 32.5768 66.1305 2 -6 -4 -5 108.213 63.6365 2 6 4 5 2.10886 193.340 1 7 4 5 207.845 209.006 1 8 4 5 67.8136 234.593 1 9 4 5 5813.65 548.067 1 10 4 5 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5192.44 361.222 1 4 5 5-226.496 205.606 1 4 -5 5 213.625 184.096 3 -4 -5 -5 32.4679 91.5474 2 5 -5 5 19940.3 807.460 3 5 5 5 20853.4 810.881 1 -5 -5 -5 20109.7 549.012 2 -6 -5 -5 255.278 99.6880 2 6 5 5 484.390 203.953 1 7 5 5 3982.09 413.528 1 8 5 5 260.538 230.003 1 9 5 5 128.697 216.268 1 10 5 5 2125.74 393.211 1 11 5 5 756.342 303.702 1 11 -5 5-22.6961 283.666 1 12 5 5 262.078 283.025 1 12 -5 5-307.716 278.309 1 13 -5 5-63.6707 256.284 1 13 5 5 153.097 241.251 1 14 -5 5 383.303 311.975 1 14 6 -5-589.784 293.699 1 -14 -6 5 468.392 270.532 3 13 6 -5 13.6917 245.968 1 -13 -6 5 461.563 281.574 3 -12 -6 5 3095.49 459.856 3 -11 -6 5 3178.07 422.588 3 -10 -6 5-234.016 304.735 3 -9 -6 5 1292.88 281.647 3 -8 -6 5 11790.2 686.175 3 -7 -6 5 867.837 208.556 3 -6 -6 5 4831.60 412.269 3 -5 -6 5 3372.40 358.596 3 -4 -6 5 340.769 206.604 3 -3 -6 5 12545.3 612.600 3 3 -6 -5 11940.6 294.423 1 -2 -6 5 44983.0 1115.97 3 2 -6 -5 44884.6 688.092 1 -1 -6 5 33783.7 962.709 3 1 -6 -5 31622.9 449.912 3 -1 6 5 33008.8 663.180 1 1 -6 -5 32819.7 676.790 1 0 -6 5 64991.1 1323.96 3 0 6 5 62270.3 1005.36 1 0 -6 -5 61782.6 1025.61 1 1 6 5 34390.1 821.323 1 1 -6 5 32205.2 958.728 3 2 -6 5 13827.7 642.492 3 2 6 5 14477.7 574.008 1 3 -6 5 162.144 179.565 3 3 6 5 388.628 150.489 1 4 -6 5 44596.9 1203.43 3 4 6 5 44816.2 1142.20 1 5 6 5 47816.4 1259.45 1 5 -6 5 49499.4 1279.70 3 6 6 5 27715.1 1002.25 1 6 -6 5 27368.9 1004.57 3 7 6 5 5432.03 504.735 1 8 6 5 19653.8 945.981 1 9 6 5 25847.1 1129.43 1 10 6 5 3694.81 482.725 1 11 6 5 497.637 274.986 1 12 -6 5 10453.6 815.680 1 12 6 5 9960.31 821.234 1 13 -6 5 258.241 282.221 1 13 6 5-33.5646 273.204 1 14 -6 5 1912.46 469.582 1 -14 -7 5 427.509 308.312 3 -13 -7 5 40.5952 226.917 3 -12 -7 5 2058.10 424.098 3 -11 -7 5 4348.27 496.191 3 -10 -7 5 3724.98 465.092 3 -9 -7 5 19.4377 235.751 3 -8 -7 5 97.9149 217.147 3 -7 -7 5-95.3929 223.784 3 -6 -7 5 1025.96 249.677 3 -5 -7 5 27862.2 978.384 3 5 -7 -5 24056.7 314.169 1 -4 -7 5 73874.5 1531.88 3 4 -7 -5 66031.1 704.118 1 -3 -7 5 26902.4 919.669 3 3 -7 -5 25250.2 518.943 1 -2 -7 5 13460.5 640.058 3 2 -7 -5 12777.3 425.816 1 -1 -7 5 75473.2 1487.00 3 -1 7 5 73170.2 1081.67 1 1 -7 -5 71540.8 706.486 3 1 -7 -5 73813.1 1107.39 1 0 -7 5 97344.1 1721.47 3 0 7 5 103398. 1380.32 1 1 -7 5 39401.8 1102.38 3 1 7 5 39789.8 932.478 1 2 -7 5 18663.9 779.652 3 2 7 5 18294.8 674.656 1 3 -7 5 16683.8 729.711 3 3 7 5 17146.0 706.607 1 4 7 5 7172.21 505.955 1 4 -7 5 6720.42 497.040 3 5 7 5 45116.3 1248.85 1 5 -7 5 42168.2 1241.95 3 6 7 5 22471.5 936.637 1 6 -7 5 22047.9 937.131 3 7 7 5 4925.81 480.503 1 8 7 5 1745.14 349.392 1 9 7 5 1581.11 354.362 1 10 7 5 2061.99 396.096 1 11 7 5 21148.5 1132.92 1 12 -7 5 1249.55 373.008 1 12 7 5 162.500 288.433 1 13 7 5 607.979 311.762 1 13 -7 5 908.544 348.684 1 14 -7 5 688.841 310.570 1 -13 -8 5 109.553 273.845 3 -12 -8 5 798.153 334.874 3 -11 -8 5 330.480 288.486 3 -10 -8 5 1372.71 346.964 3 -9 -8 5 721.749 270.490 3 -8 -8 5 5886.80 543.375 3 -7 -8 5 650.081 228.474 3 -6 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5944.84 271.817 2 4 1 7 5367.18 419.507 1 5 1 7 7186.10 513.760 1 5 -1 7 7502.98 275.450 2 6 -1 7 186.400 42.6538 2 6 1 7 178.092 207.374 1 7 -1 7 11502.0 714.112 1 7 1 7 11792.9 711.070 1 8 1 7 10402.8 705.370 1 8 -1 7 9927.78 690.408 1 9 -1 7-205.980 242.457 1 9 1 7-30.5403 213.795 1 10 1 7 284.506 219.487 1 10 -1 7 89.0413 208.289 1 11 -1 7 1791.76 381.822 1 11 1 7 2000.07 419.294 1 12 -1 7-334.662 326.634 1 12 1 7-313.437 297.394 1 13 -1 7-46.7130 264.178 1 13 1 7 456.677 274.543 1 -15 2 7 399.600 268.647 2 -15 -2 7 99.2246 283.581 2 -14 -2 7 368.976 267.543 2 -14 -2 7 315.654 222.127 3 -13 2 7 3368.07 479.630 2 -13 -2 7 3068.50 463.142 2 -13 -2 7 2919.95 425.064 3 -12 -2 7 9083.77 665.278 3 -12 2 7 9741.36 723.783 2 -12 -2 7 8492.61 706.377 2 -11 -2 7 5080.08 482.837 3 -11 2 7 5397.33 552.121 2 -10 -2 7 7960.53 558.910 3 -10 2 7 7756.81 462.948 3 -10 2 7 8520.51 629.399 2 -9 2 7 17186.0 636.746 3 -9 -2 7 16904.7 772.262 3 -9 2 7 18045.2 875.168 2 -8 2 7 27544.9 746.833 3 -8 -2 7 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3927.99 509.491 1 10 3 7 4510.74 536.674 1 11 -3 7 4627.34 571.847 1 11 3 7 3926.43 549.654 1 12 3 7 1893.23 432.057 1 12 -3 7 2267.44 454.765 1 13 3 7 1618.03 413.153 1 13 -3 7 1131.25 362.612 1 -15 -4 7 368.887 309.501 2 -15 -4 7 6.06028 266.496 3 -14 -4 7 67.0875 243.653 3 -13 -4 7 962.502 315.933 3 -12 -4 7 2579.04 414.635 3 -12 4 7 1821.11 373.560 2 -11 4 7 1265.32 323.639 2 -11 -4 7 991.071 292.771 3 -10 -4 7 5604.14 523.145 3 -10 4 7 5665.48 534.653 2 -9 4 7 1643.14 350.206 2 -9 -4 7 1647.14 294.304 3 -8 -4 7 19724.6 861.702 3 -8 4 7 19988.4 902.151 2 -7 -4 7 7317.92 525.180 3 -7 4 7 8246.11 591.716 2 -6 4 7 3305.74 372.513 2 -6 4 7 3215.40 160.481 3 -5 4 7 31.1551 204.450 2 -5 4 7 104.627 39.6190 3 -5 -4 7 8.57695 178.453 3 -4 -4 7 37061.4 1033.04 3 -4 4 7 37650.0 1071.90 2 -3 4 7 952.787 230.407 2 -3 4 7 1018.32 75.2182 1 -3 -4 7 959.870 211.080 3 -2 4 7-34.4749 215.844 2 -2 4 7 377.354 79.5612 1 -2 -4 7 71.9885 159.270 3 2 -4 -7 203.682 65.1709 3 -1 4 7-182.029 239.351 2 -1 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3357.00 495.772 3 2 13 7 120.415 192.994 1 2 -13 7-197.244 286.703 3 3 -13 7 10394.6 799.461 3 3 13 7 10118.2 720.096 1 4 -13 7 3906.63 527.032 3 4 13 7 3166.72 453.259 1 5 -13 7 812.936 315.126 3 5 13 7 1236.36 343.430 1 6 -13 7 334.293 305.102 3 6 13 7 362.580 260.038 1 7 -13 7 1978.42 414.569 3 7 13 7 2219.85 430.753 1 8 -13 7 146.195 279.745 3 8 13 7 347.711 322.796 1 -6 -14 7 2558.94 511.113 3 -5 -14 7 1201.43 383.242 3 -4 -14 7 928.811 311.748 3 -3 -14 7 1694.15 431.979 3 -2 -14 7 885.791 333.985 3 -1 -14 7 1959.12 409.911 3 0 -14 7 756.172 282.947 3 1 -14 7 6.36402 263.583 3 2 -14 7 1140.46 342.300 3 3 14 7 2629.83 415.366 1 3 -14 7 2324.78 435.668 3 4 14 7-41.4836 204.413 1 4 -14 7-152.260 247.210 3 5 -14 7 662.112 286.040 3 5 14 7 518.669 295.478 1 6 -14 7 1606.49 394.011 3 6 14 7 1957.32 420.135 1 7 14 7 403.094 288.574 1 7 -14 7 126.515 264.633 3 -4 -15 7 12.1703 285.320 3 -3 -15 7 1456.20 423.172 3 -2 -15 7 1098.33 423.039 3 -1 -15 7 3661.36 546.667 3 0 -15 7 1766.30 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43375.2 699.227 2 6 0 8 2119.66 340.957 1 7 0 8 20841.8 955.716 1 8 0 8-367.543 298.997 1 9 0 8 1480.68 330.454 1 10 0 8 520.109 264.596 1 11 0 8 252.409 248.811 1 12 0 8 240.972 243.046 1 -15 -1 8-27.9904 289.776 2 -15 1 8 46.2168 275.965 2 -14 1 8 353.173 298.592 2 -14 -1 8 499.110 320.964 2 -13 1 8-431.503 293.861 2 -13 -1 8-429.273 285.612 2 -12 1 8 1275.20 324.681 2 -12 -1 8 1035.75 364.435 2 -12 -1 8 1411.84 288.920 3 -11 1 8 381.265 222.788 2 -11 -1 8 490.476 274.090 2 -11 -1 8 300.969 182.008 3 -10 1 8 220.323 296.095 2 -10 -1 8 212.680 237.563 2 -10 -1 8 404.814 194.532 3 -9 1 8 608.126 177.471 3 -9 -1 8 594.450 189.218 3 -8 1 8 2595.92 380.049 2 -8 1 8 3101.17 294.596 3 -8 -1 8 2502.53 308.815 3 -7 1 8 6593.95 396.411 3 -7 -1 8 6075.84 433.255 3 -7 1 8 6614.40 534.847 2 -6 1 8 83.8972 209.701 2 -6 1 8 30.2618 129.686 3 -6 -1 8 108.926 168.491 3 -5 -1 8 7072.82 443.667 3 -5 1 8 6718.63 270.051 1 -5 1 8 7276.94 393.443 3 -5 1 8 7681.21 552.594 2 -4 1 8 9032.41 418.533 3 -4 -1 8 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505.854 1 11 1 10 6683.57 725.698 1 11 -1 10 5973.92 690.516 1 -12 2 10 815.334 326.801 2 -12 -2 10 1781.36 466.723 2 -11 2 10-121.042 278.436 2 -11 -2 10 123.253 310.759 2 -10 2 10 1284.83 349.311 2 -10 -2 10 584.209 191.628 3 -9 2 10 126.251 242.814 2 -9 -2 10 40.9427 189.989 3 -8 -2 10 7333.32 547.942 3 -8 2 10 6788.79 615.333 2 -7 2 10 2739.47 399.126 2 -7 -2 10 3262.63 370.323 3 -6 2 10 1540.28 358.399 2 -6 -2 10 1534.89 282.192 3 -5 2 10 9772.21 463.261 3 -5 -2 10 9792.76 614.431 3 -5 2 10 10562.8 711.614 2 -4 -2 10 2994.00 377.356 3 -4 2 10 2537.77 428.101 2 -4 2 10 2339.76 247.692 3 -3 2 10 8552.98 383.733 1 -3 -2 10 8563.85 546.975 3 -3 2 10 9264.81 615.974 2 -3 2 10 9235.36 454.640 3 -2 2 10 4813.66 322.263 1 -2 -2 10 4714.37 425.366 3 -2 2 10 5939.73 509.012 2 -2 2 10 5261.75 363.431 3 -1 -2 10 5575.06 465.801 3 -1 2 10 5348.99 452.587 2 -1 2 10 5600.92 395.086 3 -1 2 10 5474.97 361.455 1 0 2 10 22866.0 848.794 2 0 2 10 24445.4 803.752 1 0 -2 10 23981.0 925.098 3 1 2 10-126.542 188.607 2 1 -2 10 40.3640 212.378 3 1 2 10 48.4141 167.307 1 2 2 10 11733.0 581.330 2 2 2 10 12394.9 637.590 1 2 -2 10 11406.5 667.717 3 3 2 10 579.255 149.902 2 3 -2 10 238.126 233.497 3 4 2 10 8195.48 587.621 1 5 2 10 175.922 199.957 1 6 2 10 1636.68 326.123 1 7 2 10 1650.08 361.301 1 8 2 10-146.194 257.274 1 8 -2 10 956.642 362.027 1 9 2 10 1469.73 342.620 1 9 -2 10 2365.91 469.198 1 10 -2 10 193.823 253.814 1 10 2 10 121.220 297.313 1 11 2 10 476.245 348.588 1 -12 3 10 2600.48 500.883 2 -12 -3 10 2680.64 523.411 2 -11 3 10 380.481 300.919 2 -11 -3 10-41.3017 222.385 3 -10 3 10 1258.14 310.488 2 -10 -3 10 1755.46 336.060 3 -9 3 10 49.0163 243.755 2 -9 -3 10 249.903 233.412 3 -8 -3 10 13500.5 761.555 3 -8 3 10 12163.8 807.146 2 -7 3 10 29.5638 258.866 2 -7 -3 10 123.149 195.470 3 -6 -3 10 6399.82 507.190 3 -6 3 10 6407.80 566.549 2 -5 3 10 804.869 317.942 2 -5 -3 10 824.100 285.984 3 -4 -3 10 48931.3 1336.42 3 -4 3 10 47669.9 1416.71 2 -3 -3 10 12219.3 687.524 3 -3 3 10 12173.3 718.791 2 -3 3 10 11857.5 469.127 3 -2 3 10 2917.97 389.510 2 -2 -3 10 2558.30 341.134 3 -2 3 10 2812.16 241.744 1 -1 -3 10 12897.6 711.352 3 -1 3 10 13483.1 544.662 1 -1 3 10 13076.7 695.277 2 0 -3 10 17232.3 818.884 3 0 3 10 18086.1 775.572 2 0 3 10 16660.6 653.354 1 1 -3 10 2471.56 386.538 3 1 3 10 2977.49 355.291 2 1 3 10 2784.95 325.194 1 2 3 10 15583.2 652.552 2 2 3 10 15958.1 728.564 1 2 -3 10 16637.6 828.017 3 3 3 10 4505.12 418.552 1 3 -3 10 4819.36 474.199 3 4 -3 10 670.411 227.897 3 4 3 10 1684.37 290.430 1 5 3 10 1418.88 300.718 1 6 3 10 406.572 246.312 1 7 3 10 4332.38 528.146 1 8 3 10 3648.66 487.846 1 9 3 10-72.6114 268.340 1 9 -3 10 498.449 303.236 1 10 3 10 1400.64 379.588 1 10 -3 10 1412.38 407.744 1 -12 4 10 2650.09 518.853 2 -12 -4 10 2812.55 470.871 3 -11 4 10 1249.70 394.001 2 -11 -4 10 1271.65 347.597 3 -10 4 10 2920.75 472.276 2 -10 -4 10 2514.62 386.932 3 -9 4 10 3719.83 507.487 2 -9 -4 10 4243.01 483.316 3 -8 4 10 1149.04 323.096 2 -8 -4 10 1419.30 331.904 3 -7 4 10 137.134 278.400 2 -7 -4 10 282.717 258.679 3 -6 4 10 278.607 290.276 2 -6 -4 10 543.051 231.562 3 -5 -4 10 24924.6 997.940 3 -5 4 10 25327.1 1056.84 2 -4 -4 10 9557.82 640.978 3 -4 4 10 9477.53 657.592 2 -3 -4 10 17325.5 840.696 3 -3 4 10 16808.3 827.554 2 -2 -4 10 4265.38 440.312 3 -2 4 10 4799.88 289.113 1 -2 4 10 4724.17 468.678 2 -1 -4 10 3901.44 421.506 3 -1 4 10 4181.26 305.706 1 -1 4 10 4648.10 430.592 2 0 -4 10 11230.0 699.344 3 0 4 10 10578.3 517.405 1 0 4 10 9838.52 586.451 2 1 4 10 15933.7 677.327 1 1 -4 10 16249.9 834.423 3 2 4 10 486.309 182.987 1 2 -4 10 509.278 245.047 3 3 4 10 20982.9 875.858 1 3 -4 10 21295.5 979.956 3 4 4 10 8184.56 588.605 1 4 -4 10 6472.88 566.466 3 5 -4 10 692.334 268.617 3 5 4 10 1281.74 321.099 1 6 4 10 7217.20 621.871 1 7 4 10 22625.1 1096.09 1 8 4 10 351.343 230.404 1 9 4 10 3340.43 519.970 1 10 4 10 228.175 308.033 1 10 -4 10-686.416 374.584 1 -12 -5 10 2406.76 469.863 3 -11 -5 10 736.194 320.949 3 -11 5 10 679.033 337.321 2 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10 1981.93 469.571 3 -11 -6 10 643.177 337.162 3 -10 -6 10 616.036 300.095 3 -9 -6 10 687.423 334.307 3 -8 -6 10 663.365 326.560 3 -7 -6 10 2426.49 405.445 3 -6 -6 10 698.501 250.134 3 -5 -6 10 587.056 258.122 3 -4 -6 10 157.656 220.100 3 -3 -6 10 9237.01 669.873 3 -2 -6 10 145.495 214.488 3 -1 -6 10 2055.37 370.062 3 0 -6 10 4352.99 475.796 3 0 6 10 4788.31 362.510 1 1 6 10 1194.94 224.395 1 1 -6 10 1307.24 340.245 3 2 6 10 4976.19 428.640 1 2 -6 10 5294.06 539.991 3 3 6 10 8386.20 578.729 1 3 -6 10 8968.23 700.619 3 4 6 10 8126.54 599.761 1 4 -6 10 7141.80 640.637 3 5 6 10 6220.48 564.785 1 5 -6 10 5644.65 582.631 3 6 -6 10 1128.03 354.358 3 6 6 10 673.879 292.661 1 7 6 10 7189.91 653.620 1 8 6 10 2137.49 436.483 1 9 6 10 2822.03 483.838 1 10 6 10 689.177 348.392 1 -12 -7 10 104.649 297.428 3 -11 -7 10 478.471 307.131 3 -10 -7 10-437.195 308.417 3 -9 -7 10 434.122 272.197 3 -8 -7 10 147.648 255.906 3 -7 -7 10 943.664 310.399 3 -6 -7 10 7172.41 621.334 3 -5 -7 10 3779.23 455.137 3 -4 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4596.82 475.771 1 4 -8 10 5478.91 602.953 3 5 -8 10 105.248 237.127 3 5 8 10 122.997 247.472 1 6 -8 10-321.924 255.774 3 6 8 10-101.843 218.429 1 7 8 10 1055.18 317.394 1 8 8 10 77.1225 244.403 1 9 8 10 861.489 329.964 1 -10 -9 10-459.057 316.941 3 -9 -9 10 402.289 260.704 3 -8 -9 10-81.3499 280.401 3 -7 -9 10 90.6775 248.137 3 -6 -9 10 294.000 272.905 3 -5 -9 10 1266.98 325.302 3 -4 -9 10 3400.81 494.245 3 -3 -9 10 857.869 365.926 3 -2 -9 10 1873.03 407.512 3 -1 -9 10 9902.21 761.472 3 0 -9 10 928.736 308.273 3 1 -9 10-28.7017 247.898 3 2 -9 10 443.322 252.485 3 2 9 10 1135.81 215.209 1 3 -9 10 2445.40 436.427 3 3 9 10 3212.16 386.805 1 4 -9 10-128.542 270.897 3 4 9 10 23.6393 208.122 1 5 -9 10 83.2040 237.347 3 5 9 10 508.267 255.970 1 6 -9 10 875.687 336.718 3 6 9 10 1449.48 358.456 1 7 -9 10 219.379 297.340 3 7 9 10 447.214 286.965 1 8 9 10 1622.57 406.917 1 9 9 10 642.268 350.039 1 -9 -10 10-123.166 323.708 3 -8 -10 10 142.158 282.703 3 -7 -10 10 102.805 289.024 3 -6 -10 10 99.2454 300.645 3 -5 -10 10 10278.4 824.536 3 -4 -10 10-44.7970 255.698 3 -3 -10 10 797.294 346.632 3 -2 -10 10 3527.16 502.588 3 -1 -10 10 8241.19 722.277 3 0 -10 10 485.722 278.200 3 1 -10 10 388.163 303.536 3 2 -10 10 301.390 279.137 3 3 -10 10 93.2172 287.866 3 3 10 10-427.135 233.156 1 4 -10 10 263.486 267.921 3 4 10 10 26.4378 237.463 1 5 -10 10 517.366 253.555 3 5 10 10 682.005 270.342 1 6 -10 10 108.165 251.009 3 6 10 10-178.836 224.036 1 7 -10 10 3600.43 566.057 3 7 10 10 3854.58 555.819 1 8 10 10 1428.32 387.953 1 -7 -11 10 233.897 328.079 3 -6 -11 10 6224.64 680.150 3 -5 -11 10 309.966 339.609 3 -4 -11 10 1069.85 360.257 3 -3 -11 10 695.246 330.299 3 -2 -11 10 13413.9 935.576 3 -1 -11 10 891.422 390.670 3 0 -11 10 2938.02 493.599 3 1 -11 10 217.028 259.343 3 2 -11 10 175.143 297.588 3 3 -11 10 239.590 237.571 3 4 -11 10-159.006 236.887 3 4 11 10 78.8689 212.725 1 5 -11 10 222.297 257.317 3 5 11 10 68.6465 218.293 1 6 -11 10 2162.76 484.844 3 6 11 10 2727.83 469.142 1 7 11 10 1263.76 377.874 1 8 11 10 126.627 247.167 1 -5 -12 10 1255.28 452.095 3 -4 -12 10 340.970 301.940 3 -3 -12 10 466.862 352.063 3 -2 -12 10 1116.77 407.703 3 -1 -12 10 658.688 342.527 3 0 -12 10 462.797 328.906 3 1 -12 10 620.654 284.804 3 2 -12 10 788.779 312.100 3 3 -12 10 265.266 246.678 3 4 -12 10 3222.41 521.547 3 5 12 10 2801.80 434.217 1 6 12 10 3.93316 240.711 1 7 12 10 478.857 324.501 1 -2 -13 10 895.650 375.152 3 -1 -13 10 2736.16 512.049 3 0 -13 10 655.918 304.108 3 1 -13 10 195.356 299.700 3 6 13 10 723.468 301.162 1 -11 0 11-251.035 323.794 2 -10 0 11-83.5078 288.164 2 -9 0 11-150.896 288.422 2 -8 0 11-335.943 326.056 2 -7 0 11 70.5628 240.031 2 -6 0 11-112.343 249.022 2 -6 0 11-237.475 232.328 3 -5 0 11 66.6854 282.817 2 -5 0 11-164.636 162.787 3 -4 0 11-107.318 300.898 2 -4 0 11 111.315 172.692 3 -3 0 11-171.601 164.969 3 -3 0 11-31.2223 249.013 2 -2 0 11-250.133 202.614 3 -2 0 11-336.181 260.493 2 -1 0 11-11.7462 176.747 3 -1 0 11-342.775 278.159 2 0 0 11 284.570 183.725 3 0 0 11-251.366 269.367 2 1 0 11-200.452 226.163 3 1 0 11-139.751 240.249 2 2 0 11-38.0629 159.002 2 3 0 11 113.508 141.662 2 4 0 11 61.4459 126.007 2 4 0 11-98.5991 190.653 1 5 0 11-467.657 272.439 1 6 0 11-431.154 275.915 1 7 0 11-57.3741 224.408 1 8 0 11-59.6280 250.560 1 9 0 11-117.953 299.313 1 10 0 11-253.897 295.988 1 -11 1 11 146.748 277.953 2 -11 -1 11 409.337 305.234 2 -10 1 11 49.7025 258.598 2 -10 -1 11-54.0761 271.670 2 -9 1 11 2713.34 476.433 2 -9 -1 11 3258.88 512.892 2 -8 1 11 9332.37 770.733 2 -8 -1 11 10769.9 820.814 2 -7 1 11 651.937 293.930 2 -7 -1 11 512.944 307.247 2 -7 -1 11 527.644 202.867 3 -6 1 11-32.1497 272.913 2 -6 -1 11-3.16930 192.993 3 -5 -1 11 4796.86 441.102 3 -5 1 11 4737.47 523.512 2 -4 1 11 1580.69 363.926 2 -4 1 11 1521.88 242.646 3 -4 -1 11 1507.64 283.627 3 -3 1 11 966.727 213.946 3 -3 1 11 1032.21 308.029 2 -3 -1 11 599.294 192.501 3 -2 1 11 1669.69 249.444 3 -2 1 11 2254.72 370.217 2 -2 -1 11 2168.16 310.028 3 -1 1 11 421.220 207.288 3 -1 -1 11-273.960 210.718 3 -1 1 11 272.339 213.235 2 0 -1 11 2639.45 373.404 3 0 1 11 2495.71 339.574 2 0 1 11 2691.40 349.097 3 1 -1 11-131.921 197.784 3 1 1 11-74.1421 179.449 2 1 -1 11-154.513 231.707 2 2 -1 11 772.050 223.473 3 2 1 11 1108.07 231.379 2 2 -1 11 1510.47 261.865 2 2 1 11 923.562 211.150 1 3 1 11 1736.98 251.077 2 3 -1 11 1891.41 281.264 2 3 1 11 1754.94 304.456 1 4 -1 11 4601.60 356.639 2 4 1 11 4546.47 473.207 1 5 1 11 275.992 229.861 1 6 1 11 33.8019 258.065 1 6 -1 11-134.101 250.028 1 7 1 11 4324.42 539.840 1 7 -1 11 4534.14 571.865 1 8 1 11 286.833 282.774 1 8 -1 11 1072.36 361.566 1 9 -1 11 893.939 342.662 1 9 1 11 849.906 320.448 1 10 1 11 289.459 326.817 1 10 -1 11 443.783 324.737 1 -11 2 11 237.842 292.060 2 -11 -2 11 434.684 327.130 2 -10 2 11 411.825 289.086 2 -10 -2 11 173.787 272.087 2 -9 2 11 2983.74 487.144 2 -8 2 11 1027.34 358.718 2 -8 -2 11 1338.95 312.239 3 -7 2 11 2642.76 421.823 2 -7 -2 11 2296.03 338.007 3 -6 2 11 3941.45 504.738 2 -6 -2 11 3617.49 399.221 3 -5 2 11 1318.74 336.585 2 -5 -2 11 727.007 270.265 3 -4 -2 11 10075.3 623.320 3 -4 2 11 10821.3 733.321 2 -3 -2 11 13218.7 726.968 3 -3 2 11 13663.1 776.500 2 -3 2 11 13258.1 569.803 3 -2 2 11 226.704 119.155 1 -2 2 11 344.563 151.447 3 -2 2 11 278.480 216.501 2 -2 -2 11 80.5814 209.683 3 -1 -2 11 14339.1 736.753 3 -1 2 11 14323.1 742.538 2 -1 2 11 14956.9 649.031 3 -1 2 11 13352.2 593.326 1 0 2 11 20215.4 860.935 2 0 2 11 18777.5 752.573 1 0 -2 11 18835.1 885.002 3 1 2 11 16765.7 747.309 2 1 2 11 17636.5 760.409 1 1 -2 11 16904.1 831.160 3 2 2 11 10246.6 576.672 2 2 2 11 10412.6 613.499 1 2 -2 11 9784.59 663.380 3 3 -2 11 1579.75 317.539 3 3 2 11 1474.29 308.932 1 3 2 11 1457.91 247.887 2 4 -2 11 796.419 213.676 2 4 2 11 543.329 255.354 1 5 2 11 1799.67 335.210 1 6 2 11 1448.76 335.700 1 7 2 11-250.546 284.126 1 7 -2 11 393.800 274.401 1 8 2 11 8391.35 734.275 1 8 -2 11 9128.28 797.208 1 9 2 11 5.22958 299.078 1 9 -2 11 402.626 257.537 1 10 2 11 332.468 257.410 1 -11 3 11 47.9866 285.618 2 -10 3 11 427.291 310.988 2 -9 3 11 68.1284 331.313 2 -9 -3 11 34.5386 227.330 3 -8 -3 11 10790.7 712.951 3 -8 3 11 10907.3 813.604 2 -7 3 11 48.1230 236.281 2 -7 -3 11-138.549 218.353 3 -6 3 11-13.1923 239.999 2 -6 -3 11 63.2951 206.144 3 -5 3 11 137.130 253.462 2 -5 -3 11 289.297 223.261 3 -4 3 11 2069.54 363.193 2 -4 -3 11 2415.17 381.177 3 -3 3 11 1014.55 298.764 2 -3 -3 11 1057.83 258.259 3 -2 -3 11 6907.45 547.144 3 -2 3 11 7045.56 562.841 2 -1 3 11 3396.53 410.743 2 -1 -3 11 3626.43 419.510 3 -1 3 11 3130.01 292.919 1 0 3 11-261.549 244.469 2 0 -3 11 50.7551 216.235 3 0 3 11 232.398 155.278 1 1 3 11 2865.78 345.280 2 1 -3 11 3168.78 418.753 3 1 3 11 2781.92 321.819 1 2 3 11 14336.7 706.537 1 2 -3 11 14860.2 826.519 3 3 -3 11 735.993 256.912 3 3 3 11 918.993 258.885 1 4 3 11 9826.88 661.374 1 4 -3 11 8926.72 695.618 3 5 3 11 888.063 263.538 1 6 3 11 6321.72 606.498 1 7 3 11 3279.83 474.457 1 8 -3 11 4816.75 620.055 1 8 3 11 4505.10 549.064 1 9 -3 11 529.103 326.389 1 9 3 11-587.160 377.417 1 10 3 11-49.7472 304.363 1 -10 4 11 630.680 338.364 2 -10 -4 11 47.1559 230.651 3 -9 4 11 583.403 315.923 2 -9 -4 11 715.355 292.297 3 -8 4 11-49.1822 318.578 2 -8 -4 11 1030.65 321.523 3 -7 4 11 2739.29 442.033 2 -7 -4 11 2143.84 361.683 3 -6 4 11 1385.17 352.017 2 -6 -4 11 365.409 232.502 3 -5 4 11 467.916 241.492 2 -5 -4 11 735.430 248.862 3 -4 4 11 3411.89 455.209 2 -4 -4 11 3886.81 441.605 3 -3 4 11 54.9895 231.231 2 -3 -4 11 235.724 234.495 3 -2 4 11 491.429 263.438 2 -2 -4 11 1.70559 220.815 3 -1 4 11 2793.70 384.511 2 -1 -4 11 2602.68 392.890 3 0 -4 11 445.752 262.889 3 0 4 11 28.1145 146.721 1 0 4 11-82.7316 190.278 2 1 4 11 4567.20 390.531 1 1 -4 11 4359.04 463.822 3 2 4 11-102.666 200.428 1 2 -4 11-78.4377 235.182 3 3 -4 11 2344.15 404.113 3 3 4 11 1979.25 330.049 1 4 -4 11-21.8599 254.677 3 4 4 11 129.851 223.568 1 5 4 11 8425.12 647.894 1 6 4 11 1501.39 349.879 1 7 4 11 6775.88 644.244 1 8 4 11-227.987 295.722 1 9 4 11 1459.05 391.529 1 9 -4 11 904.055 371.604 1 -11 -5 11 168.550 241.328 3 -10 -5 11 251.426 223.928 3 -10 5 11 289.811 294.860 2 -9 5 11 1659.98 386.945 2 -9 -5 11 1591.59 362.133 3 -8 5 11 74.0963 312.411 2 -8 -5 11 121.771 224.413 3 -7 5 11 1250.11 361.939 2 -7 -5 11 1187.89 318.765 3 -6 5 11 1474.18 342.977 2 -6 -5 11 1257.64 292.563 3 -5 5 11 266.144 259.962 2 -5 -5 11-13.2208 250.907 3 -4 5 11 2786.16 394.083 2 -4 -5 11 3314.70 448.879 3 -3 -5 11 654.034 287.045 3 -3 5 11 572.174 232.170 2 -2 -5 11 117.020 241.208 3 -1 -5 11 7291.05 626.425 3 0 -5 11 7507.40 618.921 3 0 5 11 6339.13 424.512 1 1 -5 11 192.481 264.055 3 1 5 11 481.516 187.465 1 2 -5 11 468.666 247.029 3 2 5 11 299.496 197.390 1 3 -5 11 25.6276 228.397 3 3 5 11 210.451 217.504 1 4 -5 11 126.989 260.889 3 4 5 11 57.0061 200.529 1 5 -5 11 1526.61 392.008 3 5 5 11 1869.01 359.318 1 6 5 11 5468.58 580.575 1 7 5 11 169.855 249.731 1 8 5 11 454.816 297.690 1 9 5 11 835.536 343.578 1 -12 -6 11 2993.40 534.545 3 -11 -6 11 252.337 246.663 3 -10 -6 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2 -1 0 14 7563.41 655.937 2 0 0 14 862.992 274.512 2 1 0 14 498.670 205.127 2 1 0 14 784.613 281.602 1 2 0 14 6158.63 580.921 1 3 0 14 4320.71 546.772 1 4 0 14 4748.85 577.305 1 5 0 14 3227.61 503.216 1 6 0 14 3723.67 568.535 1 -6 1 14 482.077 260.418 2 -6 -1 14 210.467 276.604 2 -5 1 14-191.424 288.148 2 -5 -1 14 288.342 296.414 2 -4 1 14 1106.08 325.087 2 -4 -1 14 1048.84 369.688 2 -3 1 14-206.768 256.432 2 -3 -1 14-218.169 270.519 2 -2 1 14 106.260 217.467 2 -2 -1 14-238.566 234.124 2 -1 -1 14 2177.70 378.460 3 -1 1 14 1821.19 362.981 2 -1 -1 14 2081.54 374.998 2 0 -1 14 345.765 238.491 3 0 1 14-126.737 226.931 2 0 -1 14 255.989 238.629 2 1 -1 14 3508.24 437.194 2 1 1 14 4299.60 465.931 2 2 1 14 2454.23 405.933 1 3 -1 14 7034.66 674.857 1 3 1 14 6417.27 617.614 1 4 -1 14 4902.13 595.210 1 4 1 14 4320.02 554.815 1 5 -1 14 4435.66 582.318 1 5 1 14 3421.89 508.826 1 6 1 14 934.325 344.832 1 6 -1 14 451.317 301.357 1 7 1 14 3927.67 572.632 1 -6 2 14 1188.32 389.431 2 -6 -2 14 860.247 352.672 2 -5 2 14 237.513 327.410 2 -5 -2 14 449.883 365.339 2 -4 2 14 377.428 266.583 2 -4 -2 14 579.417 313.243 2 -3 2 14 1669.55 367.812 2 -3 -2 14 1879.02 353.997 3 -3 -2 14 1784.58 405.069 2 -2 2 14 18.8819 221.704 2 -2 -2 14 119.564 203.507 3 -2 -2 14 269.558 282.762 2 -1 2 14 1953.62 377.200 2 -1 -2 14 2621.35 401.847 3 -1 -2 14 2393.18 416.153 2 0 2 14 308.083 230.278 2 0 -2 14 586.129 318.303 3 0 -2 14 327.415 263.952 2 1 2 14 1358.54 308.930 2 1 -2 14 1108.76 316.989 3 1 -2 14 1529.51 326.922 2 3 2 14 663.619 286.614 1 4 2 14 1674.90 362.866 1 5 2 14 795.153 308.047 1 5 -2 14 652.678 332.924 1 6 2 14 342.068 281.413 1 6 -2 14 352.084 270.775 1 7 2 14-25.6640 282.476 1 -6 3 14 2162.12 432.891 2 -5 3 14 1004.69 374.636 2 -4 3 14 763.667 371.072 2 -4 -3 14 158.765 241.558 3 -3 3 14 192.408 278.200 2 -3 -3 14-157.241 247.962 3 -2 3 14 1373.16 331.455 2 -2 -3 14 409.524 258.940 3 -1 3 14 959.614 320.251 2 -1 -3 14 653.791 276.314 3 0 3 14 635.797 315.961 2 0 -3 14 519.227 306.717 3 1 -3 14 1587.53 364.350 3 2 -3 14-459.451 360.138 3 4 3 14 1134.91 313.048 1 5 3 14 2861.82 444.286 1 6 3 14 117.983 262.817 1 6 -3 14 105.567 270.006 1 7 3 14 340.712 268.437 1 -6 4 14 2292.51 485.314 2 -5 4 14 2564.48 494.201 2 -5 -4 14 2026.18 414.703 3 -4 -4 14 4876.77 562.397 3 -4 4 14 6896.57 688.926 2 -3 4 14 760.804 314.228 2 -3 -4 14 498.118 260.664 3 -2 -4 14 410.448 275.607 3 -2 4 14 1039.80 361.656 2 -1 4 14 8500.39 691.472 2 -1 -4 14 8835.30 724.709 3 0 -4 14 4057.58 527.817 3 1 -4 14 3612.19 511.006 3 2 -4 14 896.218 316.637 3 3 -4 14-76.2142 263.181 3 5 4 14 367.259 238.711 1 6 4 14-428.363 334.339 1 7 4 14 200.231 260.590 1 -6 -5 14 537.325 273.318 3 -5 -5 14 3419.43 528.719 3 -5 5 14 4524.04 608.392 2 -4 -5 14 582.365 368.759 3 -3 -5 14 2274.94 422.856 3 -2 -5 14 881.953 325.027 3 -1 -5 14 5881.53 635.795 3 0 -5 14 550.969 354.698 3 1 -5 14 2831.07 492.476 3 2 -5 14-187.859 271.901 3 3 -5 14-40.1670 270.641 3 4 -5 14 256.623 287.303 3 6 5 14-46.4256 251.716 1 -7 -6 14-371.349 332.592 3 -6 -6 14 620.457 341.952 3 -5 -6 14 456.138 330.106 3 -4 -6 14 3849.08 563.101 3 -3 -6 14 91.8836 268.424 3 -2 -6 14 1799.26 364.479 3 -1 -6 14 1.87480 257.641 3 0 -6 14 2950.65 494.786 3 1 -6 14-216.383 267.098 3 2 -6 14 205.287 253.810 3 3 -6 14-77.0427 292.811 3 -7 -7 14-96.8087 300.670 3 -6 -7 14 189.826 290.392 3 -5 -7 14 365.276 321.517 3 -4 -7 14 788.666 362.728 3 -3 -7 14 19.2897 273.598 3 -2 -7 14 178.539 273.628 3 -1 -7 14 349.016 300.868 3 0 -7 14 22.1206 250.581 3 1 -7 14 626.682 357.243 3 2 -7 14-161.097 271.859 3 -4 -8 14 920.241 374.818 3 -3 -8 14-67.5542 285.381 3 -2 -8 14 522.622 318.291 3 -1 -8 14 3631.49 562.763 3 -4 0 15-371.074 338.593 2 -3 0 15-235.390 289.181 2 -2 0 15-391.120 304.422 2 -1 0 15-152.677 266.006 2 0 0 15-1.92132 230.748 2 3 0 15 208.486 285.234 1 4 0 15 437.043 303.241 1 5 0 15 426.836 354.923 1 -4 1 15 217.556 253.881 2 -4 -1 15 392.889 267.636 2 -3 1 15 259.305 260.831 2 -3 -1 15 365.156 291.896 2 -2 1 15-105.604 244.330 2 -2 -1 15 545.983 320.755 2 -1 1 15 1552.23 381.480 2 -1 -1 15 1564.83 381.460 2 0 1 15-153.450 224.123 2 0 -1 15 63.3474 252.325 2 3 -1 15 1514.09 390.608 1 4 -1 15 682.574 351.658 1 4 1 15 778.656 343.482 1 5 1 15 149.604 268.323 1 5 -1 15 471.558 299.663 1 -4 2 15 929.044 376.036 2 -4 -2 15 11.8754 301.224 2 -3 2 15 58.6881 296.135 2 -3 -2 15 18.0596 266.757 2 -2 2 15 562.818 268.035 2 -2 -2 15 685.873 322.039 2 -1 2 15 349.922 291.267 2 -1 -2 15 403.596 285.558 3 -1 -2 15 170.662 309.566 2 0 2 15 169.357 224.409 2 0 -2 15 358.903 280.123 3 0 -2 15 436.276 276.881 2 1 -2 15 896.508 310.555 3 4 -2 15 1094.84 348.064 1 5 2 15 300.538 306.063 1 5 -2 15-397.068 318.506 1 -4 3 15 1300.33 364.898 2 -4 -3 15 1082.75 394.386 2 -3 3 15 341.085 272.806 2 -3 -3 15 183.038 317.234 2 -2 3 15 649.218 302.679 2 -2 -3 15 461.488 293.379 3 -2 -3 15 396.508 322.503 2 -1 3 15 147.861 244.768 2 -1 -3 15 422.094 274.021 3 -1 -3 15 115.567 257.537 2 0 -3 15 1291.33 363.502 3 0 -3 15 1017.53 313.908 2 0 3 15 809.465 278.425 2 1 -3 15 258.539 262.184 3 2 -3 15 364.192 300.954 3 -3 -4 15-103.949 262.801 3 -3 4 15 789.823 349.965 2 -2 -4 15 80.4998 262.801 3 -2 4 15 220.251 279.582 2 -1 -4 15 986.397 338.119 3 0 -4 15 1086.91 379.050 3 1 -4 15 1992.48 426.536 3 2 -4 15 604.976 315.800 3 -4 -5 15 190.803 262.948 3 -3 -5 15 529.925 316.066 3 -2 -5 15 704.813 314.824 3 -1 -5 15 1920.85 427.343 3 0 -5 15 265.262 310.182 3 1 -5 15 262.731 270.950 3 2 -5 15 163.085 280.323 3 -5 -6 15 1582.92 432.028 3 -4 -6 15 214.772 309.125 3 -3 -6 15 856.805 356.361 3 -2 -6 15 980.662 372.339 3 -1 -6 15 363.374 348.452 3 0 -6 15 2675.03 515.110 3 -2 0 16 109.018 277.638 2 -1 0 16 3297.78 514.533 2 -2 1 16 1345.39 409.723 2 -2 -1 16 732.241 305.203 2 -1 1 16 2148.26 455.203 2 -1 -1 16 2145.42 452.978 2 -2 2 16 1336.70 403.753 2 -2 -2 16 738.480 304.491 2 -1 2 16-127.898 283.327 2 -1 -2 16-128.794 307.825 2 -2 3 16 340.669 279.584 2 -1 -3 16-251.981 338.834 2 -1 3 16-314.944 325.941 2 0 -3 16 1.94675 255.238 3 1 -3 16 961.068 342.338 3 -1 -4 16 329.132 259.446 3 -1 -4 16 196.238 282.329 2 0 -4 16 261.661 273.958 3 0 0 0 0.00 0.00 0 TITL W-SML4Fe in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 12.448923 14.074246 12.068763 90.0000 93.4034 90.0000 ZERR 6.00 0.000750 0.000921 0.000773 0.0000 0.0055 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O S Cl Fe UNIT 66.00 90.00 12.00 6.00 12.00 18.00 6.00 TREF HKLF 4 END ; _shelx_hkl_checksum 27851