#------------------ SECTION 1. GLOBAL INFORMATION ---------------------------# data_publication_text _publ_requested_journal 'Acta Chim.Slov.' _publ_contact_author_name 'Slyvka, Yurii' _publ_contact_author_address ;Department of Inorganic Chemistry, Ivan Franko National University of Lviv, Kyryla i Mefodiya Str., 6, 79005, Lviv, Ukraine ; _publ_contact_author_email y_slyvka@franko.lviv.ua loop_ _publ_author_name _publ_author_address 'Slyvka, Yurii' ; Department of Inorganic Chemistry, Ivan Franko National University, Kyryla i Mefodia Str, 6, 79005 L'viv, Ukraine ; 'Goreshnik, Evgeny' ;Department of Inorganic Chemistry and Technology, Jozef Stefan Institute, Jamova 39, SI-1000 Ljubljana, Slovenia ; 'Pokhodylo, Nazariy' ;Department of Organic Chemistry, Ivan Franko National University, Kyryla i Mefodia Str, 6, 79005 L'viv, Ukraine ; 'Pavlyuk, Oleksiy' ;Department of Inorganic Chemistry, Ivan Franko National University, Kyryla i Mefodia Str, 6, 79005 L'viv, Ukraine ; 'Mys`kiv, Marian' ;Department of Inorganic Chemistry, Ivan Franko National University, Kyryla i Mefodia Str, 6, 79005 L'viv, Ukraine ; #------------------ SECTION 2. COMPOUND(S) DETAILS -------------------------# data_shelxl _audit_creation_date 2016-03-10 _audit_creation_method ; Olex2 1.2 (compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998) ; _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C9 H9 Cu N6 O3' _chemical_formula_sum 'C9 H9 Cu N6 O3' _chemical_formula_weight 312.76 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 9.247(3) _cell_length_b 12.543(4) _cell_length_c 11.197(4) _cell_angle_alpha 90 _cell_angle_beta 113.54(3) _cell_angle_gamma 90 _cell_volume 1190.6(7) _cell_formula_units_Z 4 _cell_measurement_reflns_used 1074 _cell_measurement_temperature 200(2) _cell_measurement_theta_max 28.1219 _cell_measurement_theta_min 1.9864 _exptl_absorpt_coefficient_mu 1.849 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.4395 _exptl_absorpt_correction_type 'Multi-scan' _exptl_absorpt_process_details 'Blessing R.H., 1995' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.745 _exptl_crystal_description Chunk _exptl_crystal_F_000 632 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _diffrn_reflns_av_R_equivalents 0.0276 _diffrn_reflns_av_unetI/netI 0.0288 _diffrn_reflns_Laue_measured_fraction_full 0.975 _diffrn_reflns_Laue_measured_fraction_max 0.834 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min 0 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 3373 _diffrn_reflns_point_group_measured_fraction_full 0.975 _diffrn_reflns_point_group_measured_fraction_max 0.834 _diffrn_reflns_theta_full 25.000 _diffrn_reflns_theta_max 28.289 _diffrn_reflns_theta_min 2.402 _diffrn_ambient_temperature 200.15 _diffrn_detector_area_resol_mean 5.3213 _diffrn_measured_fraction_theta_full 0.975 _diffrn_measured_fraction_theta_max 0.834 _diffrn_measurement_device_type 'four-circle diffractometer' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2219 _reflns_number_total 2472 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrystalClear (Rigaku Corporation, 1999)' _computing_data_collection 'CrystalClear (Rigaku Corporation, 1999)' _computing_data_reduction 'CrystalClear (Rigaku Corporation, 1999)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2008)' _computing_structure_solution 'ShelXS (Sheldrick, 2008)' _refine_diff_density_max 0.772 _refine_diff_density_min -0.645 _refine_diff_density_rms 0.081 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.060 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 176 _refine_ls_number_reflns 2472 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0986 _refine_ls_R_factor_gt 0.0867 _refine_ls_restrained_S_all 1.060 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0392P)^2^+8.0140P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1614 _refine_ls_wR_factor_ref 0.1681 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2. Others Fixed Sof: Cu1A(0.9) Cu1B(0.1) 3.a Secondary CH2 refined with riding coordinates: C3(H3A,H3B) 3.b Aromatic/amide H refined with riding coordinates: C2(H2), C7(H7), C8(H8), C10(H10), C9(H9) 3.c X=CH2 refined with riding coordinates: C1(H1A,H1B) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1A Cu 0.88477(14) 0.12593(10) 0.68298(12) 0.0444(3) Uani 0.9 1 d . . P A 1 N3 N 0.8446(6) 0.0466(4) 0.3974(5) 0.0464(13) Uani 1 1 d . . . . . N4 N 0.8207(6) 0.0465(4) 0.5071(5) 0.0428(12) Uani 1 1 d . . . . . O1 O 0.7023(5) 0.2411(4) 0.6334(5) 0.0508(11) Uani 1 1 d . . . . . O2 O 0.6081(6) 0.3806(4) 0.5135(5) 0.0607(13) Uani 1 1 d . . . . . N6 N 0.7219(6) 0.3212(4) 0.5720(5) 0.0463(13) Uani 1 1 d . . . . . N5 N 0.7452(6) 0.0068(4) 0.7096(5) 0.0446(12) Uani 1 1 d . . . . . N1 N 0.6993(6) -0.0975(4) 0.3955(5) 0.0478(13) Uani 1 1 d . . . . . N2 N 0.7713(6) -0.0391(4) 0.3355(5) 0.0448(13) Uani 1 1 d . . . . . C5 C 0.7337(7) -0.0397(5) 0.5046(6) 0.0425(14) Uani 1 1 d . . . . . O3 O 0.8539(6) 0.3404(5) 0.5746(6) 0.0742(17) Uani 1 1 d . . . . . C3 C 0.7721(7) -0.0750(6) 0.2096(6) 0.0501(16) Uani 1 1 d . . . . . H3A H 0.8061 -0.0153 0.1691 0.060 Uiso 1 1 calc R . . . . H3B H 0.6636 -0.0952 0.1502 0.060 Uiso 1 1 calc R . . . . C6 C 0.6843(7) -0.0617(5) 0.6086(6) 0.0419(14) Uani 1 1 d . . . . . C2 C 0.8801(7) -0.1684(6) 0.2260(6) 0.0478(15) Uani 1 1 d . . . . . H2 H 0.8963 -0.2179 0.2944 0.057 Uiso 1 1 calc R . . . . C7 C 0.5830(7) -0.1446(5) 0.6065(7) 0.0474(15) Uani 1 1 d . . . . . H7 H 0.5424 -0.1920 0.5345 0.057 Uiso 1 1 calc R . . . . C8 C 0.5439(8) -0.1557(6) 0.7122(8) 0.0580(19) Uani 1 1 d . . . . . H8 H 0.4752 -0.2115 0.7140 0.070 Uiso 1 1 calc R . . . . C10 C 0.7042(9) -0.0076(6) 0.8104(7) 0.0555(17) Uani 1 1 d . . . . . H10 H 0.7466 0.0391 0.8829 0.067 Uiso 1 1 calc R . . . . C1 C 0.9544(8) -0.1832(7) 0.1453(7) 0.062(2) Uani 1 1 d . . . . . H1A H 0.9389 -0.1341 0.0767 0.075 Uiso 1 1 calc R . . . . H1B H 1.0223 -0.2427 0.1571 0.075 Uiso 1 1 calc R . . . . C9 C 0.6033(9) -0.0871(6) 0.8136(8) 0.0608(19) Uani 1 1 d . . . . . H9 H 0.5756 -0.0939 0.8863 0.073 Uiso 1 1 calc R . . . . Cu1B Cu 0.9164(16) 0.1217(12) 0.6587(13) 0.051(4) Uiso 0.1 1 d . . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1A 0.0363(5) 0.0542(6) 0.0442(6) -0.0056(5) 0.0178(5) -0.0021(5) N3 0.034(3) 0.047(3) 0.052(3) 0.002(3) 0.010(2) 0.004(2) N4 0.039(3) 0.051(3) 0.039(3) 0.003(2) 0.016(2) 0.006(2) O1 0.045(2) 0.046(3) 0.060(3) 0.006(2) 0.020(2) 0.001(2) O2 0.051(3) 0.052(3) 0.075(3) 0.009(3) 0.020(2) 0.011(2) N6 0.045(3) 0.044(3) 0.046(3) -0.003(2) 0.014(3) 0.006(2) N5 0.047(3) 0.042(3) 0.044(3) 0.000(2) 0.016(2) 0.003(2) N1 0.042(3) 0.046(3) 0.050(3) 0.001(3) 0.012(2) 0.000(2) N2 0.039(3) 0.050(3) 0.041(3) 0.003(2) 0.011(2) 0.006(2) C5 0.030(3) 0.041(3) 0.049(4) -0.006(3) 0.008(3) 0.003(2) O3 0.051(3) 0.080(4) 0.102(4) 0.033(3) 0.041(3) 0.014(3) C3 0.039(3) 0.061(4) 0.044(4) 0.002(3) 0.009(3) 0.008(3) C6 0.039(3) 0.040(3) 0.042(3) 0.001(3) 0.012(3) 0.011(3) C2 0.038(3) 0.055(4) 0.041(3) -0.009(3) 0.006(3) -0.003(3) C7 0.042(3) 0.042(4) 0.050(4) -0.001(3) 0.009(3) 0.001(3) C8 0.042(4) 0.056(4) 0.074(5) 0.013(4) 0.021(4) 0.005(3) C10 0.059(4) 0.060(4) 0.047(4) 0.000(3) 0.022(3) 0.003(3) C1 0.049(4) 0.076(5) 0.052(4) -0.010(4) 0.010(3) 0.002(4) C9 0.055(4) 0.070(5) 0.061(5) 0.013(4) 0.027(4) 0.003(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1A N4 2.071(5) . ? Cu1A O1 2.120(5) . ? Cu1A N5 2.072(6) . ? Cu1A C2 2.069(6) 3_756 ? Cu1A C1 2.035(7) 3_756 ? N3 N4 1.332(7) . ? N3 N2 1.312(7) . ? N4 C5 1.342(8) . ? N4 Cu1B 1.831(15) . ? O1 N6 1.271(7) . ? O1 Cu1B 2.407(14) . ? O2 N6 1.241(7) . ? N6 O3 1.233(7) . ? N5 C6 1.352(8) . ? N5 C10 1.338(8) . ? N5 Cu1B 2.372(14) . ? N1 N2 1.338(7) . ? N1 C5 1.345(8) . ? N2 C3 1.482(8) . ? C5 C6 1.437(9) . ? C3 H3A 0.9900 . ? C3 H3B 0.9900 . ? C3 C2 1.503(9) . ? C6 C7 1.394(9) . ? C2 Cu1A 2.069(6) 3_756 ? C2 H2 0.9500 . ? C2 C1 1.349(10) . ? C2 Cu1B 1.900(15) 3_756 ? C7 H7 0.9500 . ? C7 C8 1.376(10) . ? C8 H8 0.9500 . ? C8 C9 1.354(11) . ? C10 H10 0.9500 . ? C10 C9 1.376(10) . ? C1 Cu1A 2.035(7) 3_756 ? C1 H1A 0.9500 . ? C1 H1B 0.9500 . ? C1 Cu1B 2.178(15) 3_756 ? C9 H9 0.9500 . ? Cu1B C2 1.900(15) 3_756 ? Cu1B C1 2.178(15) 3_756 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N4 Cu1A O1 100.56(19) . . ? N4 Cu1A N5 80.3(2) . . ? N5 Cu1A O1 93.00(19) . . ? C2 Cu1A N4 115.9(2) 3_756 . ? C2 Cu1A O1 121.6(2) 3_756 . ? C2 Cu1A N5 135.0(3) 3_756 . ? C1 Cu1A N4 153.1(3) 3_756 . ? C1 Cu1A O1 102.2(3) 3_756 . ? C1 Cu1A N5 112.4(3) 3_756 . ? C1 Cu1A C2 38.4(3) 3_756 3_756 ? N2 N3 N4 104.3(5) . . ? N3 N4 Cu1A 141.9(4) . . ? N3 N4 C5 107.4(5) . . ? N3 N4 Cu1B 131.2(6) . . ? C5 N4 Cu1A 110.4(4) . . ? C5 N4 Cu1B 119.9(6) . . ? N6 O1 Cu1A 114.2(4) . . ? N6 O1 Cu1B 105.5(5) . . ? O2 N6 O1 119.0(5) . . ? O3 N6 O1 119.7(5) . . ? O3 N6 O2 121.2(6) . . ? C6 N5 Cu1A 114.4(4) . . ? C6 N5 Cu1B 106.3(5) . . ? C10 N5 Cu1A 128.4(5) . . ? C10 N5 C6 117.1(6) . . ? C10 N5 Cu1B 136.5(6) . . ? N2 N1 C5 100.2(5) . . ? N3 N2 N1 116.0(5) . . ? N3 N2 C3 123.6(6) . . ? N1 N2 C3 120.3(5) . . ? N4 C5 N1 112.1(6) . . ? N4 C5 C6 121.3(6) . . ? N1 C5 C6 126.6(6) . . ? N2 C3 H3A 109.2 . . ? N2 C3 H3B 109.2 . . ? N2 C3 C2 112.1(5) . . ? H3A C3 H3B 107.9 . . ? C2 C3 H3A 109.2 . . ? C2 C3 H3B 109.2 . . ? N5 C6 C5 113.3(6) . . ? N5 C6 C7 122.7(6) . . ? C7 C6 C5 124.0(6) . . ? Cu1A C2 H2 88.6 3_756 . ? C3 C2 Cu1A 112.1(5) . 3_756 ? C3 C2 H2 119.4 . . ? C3 C2 Cu1B 105.8(6) . 3_756 ? C1 C2 Cu1A 69.4(4) . 3_756 ? C1 C2 C3 121.1(7) . . ? C1 C2 H2 119.4 . . ? C1 C2 Cu1B 82.3(6) . 3_756 ? Cu1B C2 H2 81.9 3_756 . ? C6 C7 H7 121.1 . . ? C8 C7 C6 117.9(6) . . ? C8 C7 H7 121.1 . . ? C7 C8 H8 120.0 . . ? C9 C8 C7 119.9(7) . . ? C9 C8 H8 120.0 . . ? N5 C10 H10 118.5 . . ? N5 C10 C9 123.0(7) . . ? C9 C10 H10 118.5 . . ? Cu1A C1 H1A 110.7 3_756 . ? Cu1A C1 H1B 87.3 3_756 . ? C2 C1 Cu1A 72.2(4) . 3_756 ? C2 C1 H1A 120.0 . . ? C2 C1 H1B 120.0 . . ? C2 C1 Cu1B 59.9(5) . 3_756 ? H1A C1 H1B 120.0 . . ? Cu1B C1 H1A 115.5 3_756 . ? Cu1B C1 H1B 94.1 3_756 . ? C8 C9 C10 119.4(7) . . ? C8 C9 H9 120.3 . . ? C10 C9 H9 120.3 . . ? N4 Cu1B O1 98.1(6) . . ? N4 Cu1B N5 77.8(5) . . ? N4 Cu1B C2 140.2(7) . 3_756 ? N4 Cu1B C1 169.7(9) . 3_756 ? N5 Cu1B O1 79.0(4) . . ? C2 Cu1B O1 115.7(7) 3_756 . ? C2 Cu1B N5 126.8(7) 3_756 . ? C2 Cu1B C1 37.9(4) 3_756 3_756 ? C1 Cu1B O1 89.6(5) 3_756 . ? C1 Cu1B N5 97.1(5) 3_756 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cu1A N4 C5 N1 -175.6(4) . . . . ? Cu1A N4 C5 C6 5.6(7) . . . . ? Cu1A O1 N6 O2 164.0(4) . . . . ? Cu1A O1 N6 O3 -18.1(7) . . . . ? Cu1A N5 C6 C5 2.0(6) . . . . ? Cu1A N5 C6 C7 -177.6(5) . . . . ? Cu1A N5 C10 C9 176.5(5) . . . . ? N3 N4 C5 N1 0.2(7) . . . . ? N3 N4 C5 C6 -178.6(5) . . . . ? N3 N4 Cu1B O1 107.9(7) . . . . ? N3 N4 Cu1B N5 -175.2(6) . . . . ? N3 N4 Cu1B C2 -40.9(17) . . . 3_756 ? N3 N4 Cu1B C1 -114(4) . . . 3_756 ? N3 N2 C3 C2 104.1(7) . . . . ? N4 N3 N2 N1 -0.1(6) . . . . ? N4 N3 N2 C3 -177.0(5) . . . . ? N4 C5 C6 N5 -5.3(8) . . . . ? N4 C5 C6 C7 174.3(6) . . . . ? N5 C6 C7 C8 0.4(9) . . . . ? N5 C10 C9 C8 1.2(11) . . . . ? N1 N2 C3 C2 -72.7(7) . . . . ? N1 C5 C6 N5 176.1(6) . . . . ? N1 C5 C6 C7 -4.3(10) . . . . ? N2 N3 N4 Cu1A 173.5(5) . . . . ? N2 N3 N4 C5 -0.1(6) . . . . ? N2 N3 N4 Cu1B 165.4(7) . . . . ? N2 N1 C5 N4 -0.2(6) . . . . ? N2 N1 C5 C6 178.5(6) . . . . ? N2 C3 C2 Cu1A -70.7(6) . . . 3_756 ? N2 C3 C2 C1 -149.2(6) . . . . ? N2 C3 C2 Cu1B -58.8(7) . . . 3_756 ? C5 N4 Cu1B O1 -88.0(7) . . . . ? C5 N4 Cu1B N5 -11.2(7) . . . . ? C5 N4 Cu1B C2 123.1(12) . . . 3_756 ? C5 N4 Cu1B C1 50(4) . . . 3_756 ? C5 N1 N2 N3 0.2(6) . . . . ? C5 N1 N2 C3 177.2(5) . . . . ? C5 C6 C7 C8 -179.2(6) . . . . ? C3 C2 C1 Cu1A 104.0(6) . . . 3_756 ? C3 C2 C1 Cu1B 103.8(8) . . . 3_756 ? C6 N5 C10 C9 -0.8(10) . . . . ? C6 C7 C8 C9 0.1(10) . . . . ? C7 C8 C9 C10 -0.8(11) . . . . ? C10 N5 C6 C5 179.6(6) . . . . ? C10 N5 C6 C7 0.0(9) . . . . ? Cu1B N4 C5 N1 -167.3(6) . . . . ? Cu1B N4 C5 C6 13.9(9) . . . . ? Cu1B O1 N6 O2 159.7(6) . . . . ? Cu1B O1 N6 O3 -22.4(8) . . . . ? Cu1B N5 C6 C5 -3.3(7) . . . . ? Cu1B N5 C6 C7 177.1(6) . . . . ? Cu1B N5 C10 C9 -176.8(7) . . . . ? _shelx_res_file ; shelxl.res created by SHELXL-2014/7 TITL shelxl in P21/c #14 REM reset to P21/c #14 CELL 0.71073 9.247 12.543 11.197 90 113.54 90 ZERR 4 0.003 0.004 0.004 0 0.03 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cu N O UNIT 36 36 4 24 12 L.S. 12 PLAN 25 TEMP -73 BOND MORE -1 BOND $H CONF fmap 2 acta 50 OMIT -7 4 13 REM REM REM WGHT 0.039200 8.014000 FVAR 0.63306 PART 1 CU1A 3 0.884772 0.125935 0.682979 10.90000 0.03634 0.05418 = 0.04417 -0.00558 0.01780 -0.00209 PART 0 N3 4 0.844607 0.046585 0.397433 11.00000 0.03380 0.04685 = 0.05160 0.00194 0.00966 0.00391 N4 4 0.820740 0.046547 0.507145 11.00000 0.03911 0.05105 = 0.03869 0.00296 0.01593 0.00648 O1 5 0.702278 0.241105 0.633387 11.00000 0.04547 0.04641 = 0.05988 0.00585 0.02029 0.00078 O2 5 0.608079 0.380574 0.513531 11.00000 0.05079 0.05181 = 0.07456 0.00860 0.01975 0.01145 N6 4 0.721904 0.321214 0.571974 11.00000 0.04547 0.04357 = 0.04551 -0.00256 0.01361 0.00554 N5 4 0.745150 0.006847 0.709626 11.00000 0.04662 0.04212 = 0.04350 -0.00029 0.01620 0.00308 N1 4 0.699312 -0.097549 0.395537 11.00000 0.04158 0.04616 = 0.05002 0.00114 0.01233 -0.00023 N2 4 0.771286 -0.039128 0.335487 11.00000 0.03860 0.04967 = 0.04129 0.00309 0.01077 0.00588 C5 1 0.733686 -0.039724 0.504623 11.00000 0.02992 0.04105 = 0.04907 -0.00557 0.00786 0.00311 O3 5 0.853932 0.340384 0.574582 11.00000 0.05050 0.07994 = 0.10181 0.03324 0.04058 0.01376 C3 1 0.772064 -0.075017 0.209632 11.00000 0.03858 0.06139 = 0.04371 0.00186 0.00933 0.00794 AFIX 23 H3A 2 0.806115 -0.015280 0.169144 11.00000 -1.20000 H3B 2 0.663575 -0.095159 0.150151 11.00000 -1.20000 AFIX 0 C6 1 0.684301 -0.061687 0.608599 11.00000 0.03950 0.03981 = 0.04225 0.00080 0.01197 0.01117 C2 1 0.880079 -0.168439 0.226036 11.00000 0.03814 0.05539 = 0.04060 -0.00940 0.00583 -0.00346 AFIX 43 H2 2 0.896290 -0.217942 0.294412 11.00000 -1.20000 AFIX 0 C7 1 0.583047 -0.144628 0.606546 11.00000 0.04161 0.04202 = 0.04999 -0.00094 0.00911 0.00138 AFIX 43 H7 2 0.542376 -0.191974 0.534502 11.00000 -1.20000 AFIX 0 C8 1 0.543900 -0.155724 0.712203 11.00000 0.04226 0.05591 = 0.07372 0.01283 0.02105 0.00462 AFIX 43 H8 2 0.475241 -0.211457 0.714017 11.00000 -1.20000 AFIX 0 C10 1 0.704162 -0.007645 0.810365 11.00000 0.05935 0.06009 = 0.04732 0.00035 0.02158 0.00275 AFIX 43 H10 2 0.746618 0.039067 0.882911 11.00000 -1.20000 AFIX 0 C1 1 0.954419 -0.183217 0.145336 11.00000 0.04928 0.07574 = 0.05226 -0.00977 0.01001 0.00188 AFIX 93 H1A 2 0.938892 -0.134110 0.076699 11.00000 -1.20000 H1B 2 1.022303 -0.242733 0.157138 11.00000 -1.20000 AFIX 0 C9 1 0.603315 -0.087139 0.813600 11.00000 0.05527 0.06977 = 0.06072 0.01348 0.02657 0.00273 AFIX 43 H9 2 0.575613 -0.093850 0.886329 11.00000 -1.20000 AFIX 0 PART 2 CU1B 3 0.916356 0.121717 0.658737 10.10000 0.05099 HKLF 4 REM shelxl in P21/c #14 REM R1 = 0.0867 for 2219 Fo > 4sig(Fo) and 0.0986 for all 2472 data REM 176 parameters refined using 0 restraints END WGHT 0.0380 3.9404 REM Highest difference peak 0.772, deepest hole -0.645, 1-sigma level 0.081 Q1 1 0.8962 0.1825 0.7290 11.00000 0.05 0.77 Q2 1 0.8989 0.1343 0.4344 11.00000 0.05 0.51 Q3 1 0.8553 0.1093 0.5442 11.00000 0.05 0.44 Q4 1 0.8927 0.1859 0.6440 11.00000 0.05 0.40 Q5 1 0.9432 -0.2648 0.1037 11.00000 0.05 0.34 Q6 1 0.8008 0.0250 0.6790 11.00000 0.05 0.33 Q7 1 0.8666 0.0709 0.3159 11.00000 0.05 0.32 Q8 1 0.7107 0.0331 0.7571 11.00000 0.05 0.31 Q9 1 0.7384 -0.1277 0.2960 11.00000 0.05 0.30 Q10 1 0.8063 0.2771 0.5003 11.00000 0.05 0.29 Q11 1 0.6701 -0.1237 1.0214 11.00000 0.05 0.28 Q12 1 0.8034 -0.1864 0.3190 11.00000 0.05 0.27 Q13 1 0.6335 -0.1367 0.5437 11.00000 0.05 0.27 Q14 1 0.7629 0.1605 0.5374 11.00000 0.05 0.26 Q15 1 0.8571 -0.2561 0.2788 11.00000 0.05 0.25 Q16 1 0.7128 0.2529 0.5486 11.00000 0.05 0.24 Q17 1 0.8200 0.1241 0.6441 11.00000 0.05 0.24 Q18 1 0.8208 0.0605 0.4580 11.00000 0.05 0.24 Q19 1 0.8972 -0.2254 0.1996 11.00000 0.05 0.23 Q20 1 0.8935 0.0449 0.7260 11.00000 0.05 0.23 Q21 1 0.5854 -0.1963 0.5886 11.00000 0.05 0.22 Q22 1 0.5806 -0.0744 0.5833 11.00000 0.05 0.22 Q23 1 0.6336 -0.0288 0.7591 11.00000 0.05 0.21 Q24 1 0.8376 0.2474 0.6941 11.00000 0.05 0.21 Q25 1 0.8239 0.1034 0.8200 11.00000 0.05 0.21 ; _shelx_res_checksum 62038 _shelx_hkl_file ; 0 -16 0 24.66 5.53 0 -16 1 7.68 5.92 0 -16 2 13.34 5.90 0 -15 0 11.24 4.93 0 -15 1 3.99 5.22 0 -15 2 17.48 5.24 0 -15 3 23.42 5.46 0 -14 0 22.56 4.43 0 -14 1 28.96 4.51 0 -14 2 18.33 4.78 0 -14 3 30.15 5.30 0 -14 4 13.24 5.48 0 -14 5 14.88 3.73 0 -13 0 5.19 4.25 0 -13 1 21.65 4.15 0 -13 2 10.42 3.94 0 -13 3 45.78 4.97 0 -13 4 88.92 5.17 0 -13 5 62.62 5.66 0 -13 6 9.12 3.66 0 -12 0 114.31 3.98 0 -12 1 25.41 3.60 0 -12 2 9.74 3.20 0 -12 3 9.58 4.01 0 -12 4 8.85 4.28 0 -12 5 5.25 4.53 0 -12 6 198.93 5.67 0 -12 7 11.93 3.83 0 -11 0 5.18 2.92 0 -11 1 352.60 4.28 0 -11 2 147.33 3.52 0 -11 3 202.26 3.88 0 -11 4 268.47 4.62 0 -11 5 66.08 4.23 0 -11 6 77.13 5.06 0 -11 7 2.16 4.69 0 -11 9 14.18 4.19 0 -10 0 170.42 3.31 0 -10 1 474.15 4.37 0 -10 2 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27.63 2.61 1 -8 4 631.75 4.43 1 -8 5 80.11 3.62 1 -8 6 132.73 3.91 1 -8 7 6.71 3.44 1 -8 8 34.93 4.01 1 -8 9 7.05 4.80 1 -8 10 9.06 5.11 1 -8 11 31.52 6.70 1 -7 -12 28.74 5.69 1 -7 -11 24.84 5.65 1 -7 -10 46.34 4.76 1 -7 -9 -1.13 4.12 1 -7 -8 12.47 4.34 1 -7 -7 45.02 3.37 1 -7 -6 676.05 5.21 1 -7 -5 391.48 3.06 1 -7 -4 292.47 2.95 1 -7 -3 17.10 1.88 1 -7 -2 74.57 2.57 1 -7 -2 58.17 2.16 1 -7 -1 484.44 3.47 1 -7 0 282.44 3.04 1 -7 1 929.07 4.36 1 -7 2 759.36 4.07 1 -7 3 616.64 3.76 1 -7 4 260.99 2.97 1 -7 5 26.37 3.22 1 -7 6 218.57 3.89 1 -7 7 158.97 4.01 1 -7 8 18.47 3.84 1 -7 9 178.13 5.22 1 -7 10 4.51 5.15 1 -7 11 22.22 5.87 1 -6 -12 27.34 5.43 1 -6 -11 54.35 5.34 1 -6 -10 13.34 4.27 1 -6 -9 418.46 5.17 1 -6 -8 56.53 3.93 1 -6 -7 190.08 3.93 1 -6 -6 18.29 2.78 1 -6 -5 42.11 1.68 1 -6 -4 211.64 2.42 1 -6 -3 979.59 4.08 1 -6 -2 105.60 2.03 1 -6 -1 1073.05 4.36 1 -6 -1 1067.19 4.27 1 -6 0 185.96 2.45 1 -6 1 788.47 3.91 1 -6 2 86.31 2.23 1 -6 3 391.68 2.95 1 -6 4 7.82 1.45 1 -6 5 591.54 4.52 1 -6 6 31.75 2.86 1 -6 7 179.53 3.92 1 -6 8 11.21 3.65 1 -6 9 16.21 4.05 1 -6 10 16.91 4.97 1 -6 11 21.94 5.72 1 -5 -11 94.22 5.03 1 -5 -10 18.01 4.01 1 -5 -9 9.69 2.94 1 -5 -8 301.04 3.78 1 -5 -7 91.00 3.22 1 -5 -6 328.31 3.41 1 -5 -5 1040.54 4.92 1 -5 -4 372.64 2.48 1 -5 -3 731.78 3.26 1 -5 -2 781.40 3.52 1 -5 -1 173.96 2.03 1 -5 0 1010.16 3.81 1 -5 1 825.67 3.39 1 -5 2 1575.23 4.47 1 -5 3 316.59 2.57 1 -5 4 315.53 1.52 1 -5 5 220.23 3.05 1 -5 6 52.89 2.58 1 -5 7 95.00 3.24 1 -5 8 169.77 4.01 1 -5 9 69.78 4.20 1 -5 10 64.94 4.67 1 -4 -11 18.98 3.78 1 -4 -10 144.29 3.50 1 -4 -9 12.36 2.93 1 -4 -8 560.58 4.35 1 -4 -7 56.35 2.52 1 -4 -6 6.72 2.11 1 -4 -5 52.43 3.60 1 -4 -4 166.20 0.92 1 -4 -4 217.88 3.01 1 -4 -3 110.94 1.10 1 -4 -2 3924.49 6.24 1 -4 -1 19.02 1.57 1 -4 1 567.97 2.70 1 -4 2 23.94 1.57 1 -4 3 24.79 0.93 1 -4 4 820.48 1.73 1 -4 5 9.23 2.11 1 -4 6 847.27 4.14 1 -4 7 229.89 3.14 1 -4 8 104.38 3.08 1 -4 9 8.20 3.25 1 -4 10 99.07 4.27 1 -3 -11 48.56 3.29 1 -3 -10 21.52 3.07 1 -3 -9 62.59 2.79 1 -3 -8 21.26 2.73 1 -3 -7 60.02 2.79 1 -3 -6 210.01 2.76 1 -3 -5 2748.37 6.58 1 -3 -4 9.38 2.10 1 -3 -3 25.22 1.35 1 -3 -2 787.93 2.66 1 -3 -1 67.88 1.51 1 -3 0 343.03 2.19 1 -3 1 94.69 1.63 1 -3 2 283.60 1.89 1 -3 3 186.47 1.16 1 -3 4 1540.96 2.98 1 -3 6 62.65 1.58 1 -3 7 109.06 2.74 1 -3 8 142.01 3.05 1 -3 9 85.73 3.21 1 -3 10 25.88 3.49 1 -2 -12 8.91 4.10 1 -2 -11 36.94 3.69 1 -2 -10 10.96 3.08 1 -2 -9 287.43 3.77 1 -2 -8 44.91 2.99 1 -2 -7 534.70 2.98 1 -2 -6 206.45 2.01 1 -2 -5 697.10 2.56 1 -2 -4 21.88 1.97 1 -2 -3 5203.66 6.88 1 -2 -2 3171.97 4.17 1 -2 -1 4123.01 4.88 1 -2 0 24.77 1.09 1 -2 1 9999.00 8.95 1 -2 2 1027.79 2.67 1 -2 3 597.18 2.28 1 -2 4 4.40 1.56 1 -2 5 2894.39 5.99 1 -2 7 616.23 4.13 1 -2 8 5.29 2.64 1 -2 9 6.53 2.78 1 -2 10 28.89 2.85 1 -1 -12 63.29 4.41 1 -1 -11 21.13 3.42 1 -1 -10 68.58 3.02 1 -1 -9 7.91 2.56 1 -1 -8 126.53 2.82 1 -1 -7 223.48 2.49 1 -1 -6 698.55 2.94 1 -1 -5 2143.81 4.34 1 -1 -4 931.20 2.72 1 -1 -3 210.34 1.89 1 -1 -3 212.87 1.15 1 -1 -2 1519.91 3.12 1 -1 -1 3.20 0.67 1 -1 0 1707.27 2.73 1 -1 2 4.89 1.69 1 -1 3 1971.32 4.37 1 -1 4 105.80 1.95 1 -1 6 2.85 2.08 1 -1 7 358.69 3.37 1 -1 8 88.48 2.83 1 -1 9 193.19 3.65 1 -1 10 32.54 3.21 1 -1 11 103.23 4.08 1 0 -13 15.93 4.83 1 0 -12 9.44 4.52 1 0 -11 6.42 3.49 1 0 -10 7.33 2.84 1 0 -9 5.98 2.51 1 0 -8 277.34 3.22 1 0 -7 6.64 1.86 1 0 -6 46.06 1.68 1 0 -5 8.10 1.49 1 0 -4 52.92 1.31 1 0 -3 3.85 0.91 1 0 -1 3.94 0.57 1 0 0 1219.27 2.16 1 0 2 605.73 2.35 1 0 3 4.70 1.42 1 0 4 660.99 3.00 1 0 5 7.33 1.94 1 0 6 1862.59 5.81 1 0 7 4.02 2.02 1 0 8 256.24 3.26 1 0 9 8.95 2.80 1 0 10 5.64 3.26 1 0 11 13.27 3.64 1 0 12 14.98 4.64 1 1 -13 21.90 5.26 1 1 -12 78.41 5.21 1 1 -11 33.58 4.06 1 1 -10 63.40 3.44 1 1 -9 16.13 2.35 1 1 -8 128.35 2.59 1 1 -7 222.40 2.59 1 1 -6 768.44 2.75 1 1 -5 2185.74 3.89 1 1 -4 896.17 2.61 1 1 -3 216.78 1.23 1 1 -3 184.57 1.67 1 1 -2 1473.64 2.34 1 1 -1 4.94 0.73 1 1 0 1691.41 2.76 1 1 1 1691.54 2.99 1 1 2 7.47 1.47 1 1 4 119.90 1.94 1 1 5 347.91 2.90 1 1 6 7.12 2.06 1 1 7 351.04 3.25 1 1 8 84.60 2.71 1 1 9 168.32 3.66 1 1 10 36.72 3.58 1 1 11 89.10 4.33 1 1 12 8.62 4.73 1 2 -13 5.91 5.05 1 2 -12 12.05 4.70 1 2 -11 48.87 4.62 1 2 -10 10.14 3.15 1 2 -9 293.39 4.34 1 2 -8 29.80 2.06 1 2 -7 501.77 3.09 1 2 -6 223.43 1.52 1 2 -5 633.31 1.58 1 2 -4 19.17 0.58 1 2 -3 5129.33 3.93 1 2 -2 3140.21 4.22 1 2 -1 4070.49 4.90 1 2 0 21.90 1.14 1 2 1 9980.00 9.06 1 2 2 1035.26 3.01 1 2 3 610.82 2.42 1 2 4 3.05 1.44 1 2 5 2901.80 5.96 1 2 6 103.06 2.32 1 2 7 623.61 3.57 1 2 8 14.03 2.61 1 2 9 4.02 3.09 1 2 10 32.31 3.74 1 2 11 4.40 3.97 1 2 12 19.60 5.13 1 3 -13 44.72 6.76 1 3 -12 31.00 5.39 1 3 -11 62.69 4.42 1 3 -10 24.56 4.11 1 3 -9 73.91 3.27 1 3 -8 27.43 3.06 1 3 -7 45.90 2.42 1 3 -6 225.32 2.94 1 3 -4 4.12 0.42 1 3 -3 25.97 0.73 1 3 -2 738.70 2.42 1 3 -1 70.05 1.61 1 3 0 316.94 2.06 1 3 1 96.87 1.92 1 3 2 269.72 1.79 1 3 3 198.06 2.46 1 3 4 1588.05 5.41 1 3 5 44.12 2.25 1 3 6 58.94 2.46 1 3 7 108.16 2.99 1 3 8 160.54 3.68 1 3 9 91.05 3.60 1 3 10 34.12 3.92 1 3 11 17.68 4.15 1 3 12 10.16 5.03 1 4 -12 10.55 5.06 1 4 -11 20.75 4.28 1 4 -10 139.68 4.49 1 4 -9 5.34 3.02 1 4 -8 582.43 5.11 1 4 -7 49.54 2.67 1 4 -6 1.01 2.38 1 4 -5 32.82 2.36 1 4 -4 160.09 1.71 1 4 -3 106.99 1.16 1 4 -2 3845.06 5.47 1 4 -1 18.06 1.58 1 4 0 379.95 2.27 1 4 1 569.40 2.19 1 4 2 27.17 1.45 1 4 3 35.58 2.16 1 4 4 895.04 4.39 1 4 5 7.35 2.05 1 4 6 795.88 4.85 1 4 7 218.88 3.68 1 4 8 102.82 3.46 1 4 9 5.71 3.51 1 4 10 73.49 4.39 1 4 11 9.51 4.31 1 4 12 29.05 5.43 1 5 -12 70.31 5.22 1 5 -11 92.06 5.33 1 5 -10 19.84 4.23 1 5 -9 11.37 4.01 1 5 -8 262.44 4.14 1 5 -7 90.18 3.24 1 5 -6 368.80 3.92 1 5 -5 1044.44 4.91 1 5 -4 328.45 2.41 1 5 -3 657.83 3.04 1 5 -2 679.75 2.99 1 5 -1 176.06 1.81 1 5 0 996.15 2.64 1 5 1 823.39 3.28 1 5 2 1550.53 4.39 1 5 3 315.60 2.56 1 5 4 306.28 3.19 1 5 5 233.87 3.54 1 5 6 55.52 2.96 1 5 7 91.59 3.63 1 5 8 155.84 3.98 1 5 9 60.64 4.32 1 5 10 49.12 4.17 1 5 11 14.66 4.67 1 6 -12 5.55 4.06 1 6 -11 43.07 5.02 1 6 -10 3.27 4.65 1 6 -9 401.59 5.38 1 6 -8 76.04 4.11 1 6 -7 182.21 3.73 1 6 -6 19.09 3.09 1 6 -5 44.35 1.84 1 6 -4 195.66 2.67 1 6 -3 930.44 3.92 1 6 -2 100.56 1.95 1 6 0 177.04 1.82 1 6 1 740.27 1.93 1 6 2 82.67 2.34 1 6 3 335.55 3.06 1 6 4 5.33 2.22 1 6 5 612.92 4.89 1 6 6 19.90 3.14 1 6 7 151.97 3.71 1 6 8 6.47 3.48 1 6 9 14.57 3.78 1 6 10 21.42 4.17 1 6 11 6.30 3.25 1 7 -11 5.64 3.01 1 7 -10 34.41 4.75 1 7 -9 6.30 4.36 1 7 -8 12.21 3.22 1 7 -7 50.49 3.46 1 7 -6 652.44 5.38 1 7 -5 372.29 2.93 1 7 -4 257.78 2.64 1 7 -3 14.73 2.18 1 7 -2 63.16 2.04 1 7 -1 513.05 3.14 1 7 0 284.28 2.14 1 7 2 757.35 4.44 1 7 3 602.26 3.76 1 7 4 248.86 2.72 1 7 5 29.02 3.12 1 7 6 221.61 3.83 1 7 7 164.44 4.26 1 7 8 18.51 3.60 1 7 9 125.51 4.46 1 7 10 5.70 3.66 1 8 -11 13.11 5.07 1 8 -10 32.32 4.71 1 8 -9 32.55 4.62 1 8 -8 395.19 5.71 1 8 -7 5.22 3.65 1 8 -6 52.92 3.05 1 8 -5 6.07 2.52 1 8 -4 242.23 3.20 1 8 -3 8.81 2.78 1 8 -2 1104.08 4.55 1 8 -1 1.77 1.60 1 8 0 92.60 1.84 1 8 2 9.44 2.56 1 8 3 31.41 3.16 1 8 4 605.81 4.99 1 8 5 8.30 3.22 1 8 6 102.00 3.37 1 8 7 15.34 3.32 1 8 8 44.11 4.10 1 8 9 13.73 4.96 1 8 10 3.03 3.13 1 9 -9 29.12 5.30 1 9 -8 14.07 3.91 1 9 -7 143.73 4.21 1 9 -6 80.37 3.46 1 9 -5 261.87 4.00 1 9 -4 358.20 3.79 1 9 -3 49.89 2.31 1 9 -2 38.06 2.40 1 9 -1 161.49 2.66 1 9 0 468.69 3.04 1 9 3 332.78 3.86 1 9 4 50.55 3.61 1 9 5 62.19 3.87 1 9 6 6.85 3.21 1 9 7 27.37 4.33 1 9 8 22.78 4.83 1 10 -9 63.58 5.26 1 10 -8 2.58 5.36 1 10 -7 59.47 4.61 1 10 -6 14.76 4.17 1 10 -5 29.24 3.54 1 10 -4 9.58 2.51 1 10 -3 213.15 3.10 1 10 -2 26.62 2.68 1 10 -1 344.60 3.29 1 10 4 10.67 2.90 1 10 5 21.63 3.58 1 10 6 24.62 4.21 1 10 7 135.05 5.35 1 11 -9 14.14 5.20 1 11 -8 10.35 4.93 1 11 -7 9.36 4.41 1 11 -6 33.12 3.89 1 11 -5 54.32 3.47 1 11 -4 35.50 3.13 1 11 -3 128.16 3.41 1 11 -2 12.15 2.22 1 11 6 13.42 3.94 1 11 7 16.50 4.77 1 11 8 24.52 4.09 1 12 -8 97.57 5.75 1 12 -7 5.06 4.85 1 12 -6 35.39 4.52 1 12 -5 11.47 3.60 1 12 -4 8.71 3.20 1 12 -3 7.72 3.10 1 12 -2 58.62 2.65 1 13 -8 7.37 5.39 1 13 -7 19.23 5.17 1 13 -6 38.37 4.85 1 13 -5 19.56 4.03 1 13 -4 12.03 4.07 1 14 -7 35.50 6.50 1 14 -6 26.81 5.92 2 -16 -2 13.79 6.43 2 -16 -1 9.11 5.96 2 -16 0 28.85 6.40 2 -15 -4 20.81 6.09 2 -15 -3 13.26 5.98 2 -15 -2 14.46 6.07 2 -15 -1 14.50 5.40 2 -15 0 8.51 5.69 2 -15 1 21.84 5.89 2 -15 2 13.95 5.97 2 -14 -5 16.20 4.37 2 -14 -4 12.39 5.77 2 -14 -3 36.22 5.99 2 -14 -2 22.12 4.85 2 -14 -1 166.59 5.99 2 -14 0 11.85 5.06 2 -14 1 12.63 4.52 2 -14 2 14.99 4.70 2 -14 3 49.63 5.10 2 -13 -7 39.11 4.67 2 -13 -6 18.11 5.88 2 -13 -5 3.71 4.71 2 -13 -4 18.25 4.75 2 -13 -3 8.59 4.64 2 -13 -2 8.96 3.94 2 -13 -1 185.05 5.01 2 -13 0 99.52 4.34 2 -13 1 44.92 4.08 2 -13 2 89.97 4.65 2 -13 3 4.95 4.96 2 -13 4 20.27 4.78 2 -13 5 9.55 3.40 2 -12 -7 11.46 6.16 2 -12 -6 34.52 4.64 2 -12 -5 11.16 4.32 2 -12 -4 96.59 4.43 2 -12 -3 3.26 3.59 2 -12 -2 105.07 4.42 2 -12 -1 5.19 3.69 2 -12 0 13.44 3.73 2 -12 1 11.49 3.60 2 -12 2 7.22 3.71 2 -12 3 5.11 4.01 2 -12 4 137.01 5.16 2 -12 5 10.64 4.75 2 -12 6 6.65 3.43 2 -11 -9 10.21 4.36 2 -11 -7 245.07 5.32 2 -11 -6 39.80 4.61 2 -11 -5 13.08 3.99 2 -11 -4 8.75 3.22 2 -11 -3 34.24 3.28 2 -11 -2 113.73 3.60 2 -11 -1 237.21 3.92 2 -11 0 47.56 3.31 2 -11 1 10.22 3.13 2 -11 2 141.78 3.82 2 -11 3 151.63 4.31 2 -11 4 7.52 4.22 2 -11 5 36.77 4.63 2 -10 -10 6.77 5.93 2 -10 -9 92.48 6.60 2 -10 -8 47.62 4.65 2 -10 -7 10.77 4.10 2 -10 -6 97.21 4.17 2 -10 -5 224.23 4.57 2 -10 -4 8.97 2.97 2 -10 -3 337.04 4.19 2 -10 -2 11.04 2.88 2 -10 -1 93.98 3.22 2 -10 0 15.05 2.83 2 -10 1 136.90 3.49 2 -10 2 184.04 3.86 2 -10 3 17.18 3.11 2 -10 4 8.39 3.55 2 -10 5 153.19 4.51 2 -10 6 6.87 4.60 2 -10 7 6.04 4.61 2 -10 8 14.99 5.66 2 -9 -11 17.10 6.16 2 -9 -10 5.16 5.26 2 -9 -9 23.72 4.89 2 -9 -8 44.68 4.54 2 -9 -7 9.84 4.03 2 -9 -6 30.22 3.61 2 -9 -5 65.06 3.18 2 -9 -4 25.96 2.83 2 -9 -3 7.73 2.75 2 -9 -2 174.14 3.19 2 -9 -1 528.80 4.33 2 -9 0 406.30 4.20 2 -9 1 632.33 5.00 2 -9 2 35.87 3.08 2 -9 3 8.81 2.82 2 -9 4 67.89 3.48 2 -9 5 10.25 3.20 2 -9 6 38.09 3.92 2 -9 7 102.80 4.58 2 -9 8 42.73 5.37 2 -9 9 42.32 5.36 2 -8 -12 35.30 6.49 2 -8 -11 7.34 5.47 2 -8 -10 227.99 6.29 2 -8 -9 28.63 5.60 2 -8 -8 11.95 4.35 2 -8 -7 4.50 2.73 2 -8 -6 78.08 3.59 2 -8 -5 34.42 2.61 2 -8 -4 657.19 4.98 2 -8 -4 603.48 3.84 2 -8 -3 12.18 2.64 2 -8 -2 128.49 3.07 2 -8 -1 29.72 2.22 2 -8 0 63.17 2.59 2 -8 1 13.16 2.44 2 -8 2 828.11 4.73 2 -8 3 123.96 2.94 2 -8 4 290.08 3.58 2 -8 5 -3.97 3.36 2 -8 6 19.25 3.80 2 -8 7 24.45 4.22 2 -8 8 9.68 4.79 2 -8 9 28.46 5.32 2 -8 10 42.38 5.75 2 -7 -12 14.89 5.75 2 -7 -11 36.15 5.06 2 -7 -10 22.45 4.95 2 -7 -8 162.98 4.03 2 -7 -7 130.57 3.83 2 -7 -6 503.32 3.66 2 -7 -5 97.57 2.68 2 -7 -4 284.68 4.00 2 -7 -3 3.92 2.36 2 -7 -3 3.36 2.39 2 -7 -2 693.54 4.09 2 -7 -1 71.33 2.68 2 -7 0 133.38 2.59 2 -7 1 936.77 4.53 2 -7 2 1238.59 5.12 2 -7 3 121.98 2.70 2 -7 4 17.39 2.56 2 -7 5 294.55 4.26 2 -7 6 2.15 3.23 2 -7 7 230.47 4.44 2 -7 8 208.07 5.19 2 -7 9 16.75 4.73 2 -7 10 24.73 5.63 2 -6 -12 7.73 5.70 2 -6 -11 50.00 5.16 2 -6 -10 3.67 4.02 2 -6 -9 159.26 4.57 2 -6 -8 56.45 3.46 2 -6 -7 60.09 3.48 2 -6 -6 7.50 2.70 2 -6 -5 590.80 3.75 2 -6 -4 163.45 2.39 2 -6 -3 2131.21 5.94 2 -6 -2 69.70 2.23 2 -6 -1 395.80 3.13 2 -6 0 51.88 2.19 2 -6 1 81.67 2.13 2 -6 2 38.55 2.08 2 -6 3 413.60 2.86 2 -6 4 50.50 2.02 2 -6 5 797.31 3.90 2 -6 6 8.15 3.17 2 -6 7 67.36 3.76 2 -6 8 59.05 4.12 2 -6 9 75.97 4.81 2 -6 10 21.56 5.38 2 -5 -12 11.03 5.16 2 -5 -11 18.21 4.43 2 -5 -10 12.08 3.64 2 -5 -9 54.01 3.75 2 -5 -8 59.94 3.04 2 -5 -7 194.16 3.64 2 -5 -6 121.61 3.27 2 -5 -5 619.64 3.17 2 -5 -4 1058.46 4.00 2 -5 -3 43.42 1.92 2 -5 -2 1167.35 4.35 2 -5 -1 1779.68 5.02 2 -5 0 500.16 3.11 2 -5 1 1008.00 4.11 2 -5 2 657.52 3.48 2 -5 3 194.02 2.14 2 -5 4 5.47 1.67 2 -5 5 8.30 1.57 2 -5 6 139.98 3.57 2 -5 7 259.18 4.16 2 -5 8 492.41 5.45 2 -5 9 12.84 4.29 2 -5 10 20.90 4.91 2 -4 -11 36.64 4.10 2 -4 -10 309.92 4.53 2 -4 -9 65.92 3.67 2 -4 -8 16.31 2.97 2 -4 -7 15.80 2.77 2 -4 -6 52.24 2.69 2 -4 -5 150.52 3.22 2 -4 -4 2022.25 4.86 2 -4 -3 197.41 2.15 2 -4 -2 4960.86 7.39 2 -4 -1 9.90 1.84 2 -4 0 2586.92 5.42 2 -4 1 1149.93 3.99 2 -4 2 960.08 3.14 2 -4 3 295.53 2.12 2 -4 4 1137.25 3.29 2 -4 5 68.01 1.79 2 -4 6 434.53 3.21 2 -4 7 31.03 3.17 2 -4 8 5.87 3.18 2 -4 9 12.76 3.85 2 -4 10 46.67 4.34 2 -3 -11 9.34 3.51 2 -3 -10 136.27 3.64 2 -3 -9 187.69 3.23 2 -3 -8 136.62 3.00 2 -3 -7 1254.96 5.97 2 -3 -6 233.14 3.82 2 -3 -5 1137.31 4.42 2 -3 -4 1490.15 4.01 2 -3 -3 62.48 1.56 2 -3 -2 63.33 1.67 2 -3 -1 58.85 1.60 2 -3 0 7627.24 8.74 2 -3 1 2664.98 5.33 2 -3 2 1712.59 3.90 2 -3 3 51.70 1.56 2 -3 4 252.07 2.08 2 -3 5 97.69 2.32 2 -3 6 117.98 2.85 2 -3 7 175.52 3.49 2 -3 8 65.28 3.37 2 -3 9 37.15 3.53 2 -2 -12 10.90 3.86 2 -2 -11 51.12 3.65 2 -2 -10 68.62 3.06 2 -2 -9 9.46 2.47 2 -2 -8 16.12 2.71 2 -2 -7 21.69 2.60 2 -2 -6 410.26 3.17 2 -2 -5 1482.17 4.78 2 -2 -4 14.23 1.54 2 -2 -3 924.79 3.01 2 -2 -2 417.66 2.27 2 -2 -1 2760.40 4.92 2 -2 0 3873.32 5.81 2 -2 1 4845.08 6.12 2 -2 2 139.48 1.85 2 -2 3 2295.48 5.11 2 -2 4 273.45 2.64 2 -2 5 825.15 3.88 2 -2 6 44.68 2.83 2 -2 7 11.39 2.65 2 -2 8 7.70 2.85 2 -2 9 13.39 3.15 2 -1 -13 14.70 4.83 2 -1 -12 43.04 4.32 2 -1 -11 7.60 3.52 2 -1 -10 59.03 3.22 2 -1 -9 26.68 2.74 2 -1 -8 441.61 3.61 2 -1 -7 1942.50 5.42 2 -1 -6 453.03 2.72 2 -1 -5 92.85 1.77 2 -1 -4 937.25 3.41 2 -1 -3 56.97 1.51 2 -1 -2 3340.39 5.00 2 -1 -1 592.18 2.43 2 -1 0 2660.10 4.71 2 -1 1 1174.10 3.38 2 -1 2 206.21 2.00 2 -1 3 423.99 2.58 2 -1 4 45.31 1.99 2 -1 5 73.21 2.53 2 -1 6 39.36 2.45 2 -1 7 91.48 2.73 2 -1 8 218.15 3.57 2 -1 9 62.47 3.22 2 0 -14 10.90 5.71 2 0 -13 2.55 4.65 2 0 -12 57.66 4.66 2 0 -11 3.41 3.65 2 0 -10 98.61 3.50 2 0 -9 6.11 2.52 2 0 -8 111.90 2.47 2 0 -7 10.69 2.16 2 0 -6 1420.65 4.38 2 0 -5 6.06 1.55 2 0 -4 5466.17 6.72 2 0 -3 6.24 1.20 2 0 -2 2884.06 4.65 2 0 -1 3.76 1.17 2 0 0 6323.04 6.80 2 0 1 5.34 1.52 2 0 2 492.50 2.60 2 0 3 6.82 1.67 2 0 4 2603.64 6.31 2 0 5 1.93 2.01 2 0 6 764.39 4.34 2 0 7 9.60 2.59 2 0 8 14.00 2.64 2 0 9 6.33 3.00 2 0 10 265.46 4.44 2 1 -14 23.52 6.06 2 1 -13 17.87 5.90 2 1 -12 45.24 4.92 2 1 -11 7.01 3.53 2 1 -10 60.02 3.38 2 1 -9 18.45 2.29 2 1 -8 414.40 3.07 2 1 -7 1988.38 4.96 2 1 -6 441.77 2.40 2 1 -5 99.03 1.44 2 1 -4 913.00 3.12 2 1 -3 62.96 1.37 2 1 -2 3372.88 5.15 2 1 -1 567.69 2.39 2 1 0 2608.90 4.81 2 1 1 1261.08 3.39 2 1 3 462.13 2.52 2 1 4 47.99 2.03 2 1 5 73.18 2.31 2 1 6 42.47 2.58 2 1 7 89.56 2.84 2 1 8 227.07 3.81 2 1 9 68.47 3.53 2 1 10 46.83 3.93 2 2 -13 14.73 5.71 2 2 -12 9.22 4.86 2 2 -11 47.88 4.25 2 2 -10 60.34 3.89 2 2 -8 12.67 1.70 2 2 -7 13.99 1.68 2 2 -6 383.03 2.06 2 2 -5 1459.26 3.41 2 2 -5 1403.57 3.63 2 2 -4 10.57 1.14 2 2 -3 835.27 2.92 2 2 -2 395.24 2.22 2 2 -1 2782.50 5.01 2 2 0 3817.62 5.78 2 2 2 154.23 1.78 2 2 3 2292.12 4.68 2 2 4 266.30 2.57 2 2 5 862.03 3.97 2 2 6 37.18 2.18 2 2 7 12.17 2.23 2 2 8 7.02 3.22 2 2 9 8.16 3.68 2 2 10 45.72 4.15 2 2 11 69.84 4.89 2 3 -13 15.85 5.57 2 3 -12 9.97 4.62 2 3 -11 11.25 4.39 2 3 -10 105.98 4.21 2 3 -9 194.76 4.11 2 3 -8 122.49 1.48 2 3 -7 1030.72 2.62 2 3 -6 208.52 1.79 2 3 -6 214.01 1.54 2 3 -5 1138.83 2.81 2 3 -4 1457.90 3.29 2 3 -3 65.62 1.52 2 3 -2 67.11 1.67 2 3 -1 59.11 1.73 2 3 0 7577.25 8.45 2 3 1 2648.61 4.77 2 3 2 1731.50 3.70 2 3 3 54.67 2.09 2 3 4 236.09 2.75 2 3 5 98.32 2.83 2 3 6 112.62 2.34 2 3 7 141.80 3.37 2 3 8 59.40 3.73 2 3 9 34.94 4.03 2 3 10 21.05 4.10 2 3 11 8.26 4.55 2 4 -13 6.27 4.27 2 4 -12 33.78 4.92 2 4 -11 32.78 4.89 2 4 -10 266.90 4.77 2 4 -9 42.13 3.47 2 4 -8 18.69 3.48 2 4 -6 46.92 1.12 2 4 -5 129.00 1.44 2 4 -4 1987.66 4.06 2 4 -3 190.97 1.98 2 4 -2 4764.72 7.09 2 4 0 2504.18 5.23 2 4 1 1086.32 3.48 2 4 2 955.09 2.33 2 4 3 282.21 1.79 2 4 4 1076.79 5.29 2 4 5 68.55 2.86 2 4 6 431.30 4.58 2 4 7 39.23 3.10 2 4 8 2.76 3.73 2 4 9 18.00 4.03 2 4 10 28.39 4.12 2 4 11 14.31 4.77 2 5 -12 11.75 5.74 2 5 -11 13.60 4.65 2 5 -10 10.31 4.15 2 5 -9 43.05 3.63 2 5 -8 72.28 3.84 2 5 -7 195.02 3.67 2 5 -6 96.69 1.32 2 5 -3 39.61 1.94 2 5 2 636.92 3.06 2 5 4 7.28 2.64 2 5 5 11.83 2.83 2 5 6 130.80 3.79 2 5 7 223.89 4.06 2 5 8 458.43 5.49 2 5 9 17.28 4.57 2 5 10 9.10 4.28 2 5 11 3.84 4.32 2 6 -12 3.58 4.26 2 6 -11 40.15 5.17 2 6 -10 11.60 4.44 2 6 -9 153.49 4.51 2 6 -8 61.04 3.54 2 6 -7 58.58 3.52 2 6 -6 8.80 2.05 2 6 -5 473.68 2.49 2 6 -4 162.99 2.54 2 6 4 63.45 3.15 2 6 5 793.92 5.34 2 6 6 8.04 3.19 2 6 7 64.16 4.14 2 6 8 65.65 4.51 2 6 9 53.17 4.26 2 6 10 2.27 2.84 2 7 -11 12.36 5.16 2 7 -10 30.83 4.99 2 7 -9 23.00 4.07 2 7 -8 142.69 4.24 2 7 -7 117.92 3.79 2 7 -6 460.46 4.36 2 7 -5 78.61 2.50 2 7 -4 238.94 3.85 2 7 -3 -0.84 2.07 2 7 -2 633.28 3.50 2 7 -1 72.09 1.93 2 7 0 117.28 1.65 2 7 1 953.10 2.32 2 7 5 264.98 3.96 2 7 6 5.80 3.05 2 7 7 212.58 4.41 2 7 8 160.72 4.56 2 7 9 9.54 4.05 2 8 -11 14.89 4.60 2 8 -10 178.84 5.46 2 8 -9 17.88 4.54 2 8 -8 8.71 3.87 2 8 -7 4.38 3.54 2 8 -6 69.63 3.17 2 8 -5 23.90 2.29 2 8 -4 568.20 4.01 2 8 -3 10.83 2.43 2 8 -2 121.96 2.38 2 8 -1 36.11 2.02 2 8 0 60.26 1.73 2 8 6 26.35 3.74 2 8 7 13.08 3.92 2 8 8 9.58 5.16 2 9 -9 20.74 4.79 2 9 -8 51.07 4.71 2 9 -7 11.98 3.98 2 9 -6 28.65 3.31 2 9 -5 59.49 3.20 2 9 -4 20.88 2.58 2 9 -3 9.65 2.22 2 9 -2 170.87 2.94 2 9 -1 550.45 3.52 2 9 0 375.61 2.62 2 10 -10 4.95 4.28 2 10 -9 74.12 5.52 2 10 -8 46.24 4.65 2 10 -7 20.33 3.58 2 10 -6 82.09 3.52 2 10 -5 189.82 3.78 2 10 -4 6.15 2.67 2 10 -3 328.95 3.87 2 10 -2 8.95 2.56 2 10 -1 79.48 2.30 2 10 0 20.95 1.87 2 11 -9 13.17 5.19 2 11 -8 15.14 4.68 2 11 -7 222.64 5.04 2 11 -6 35.81 3.81 2 11 -5 10.78 3.02 2 11 -4 9.16 3.04 2 11 -3 35.40 3.15 2 11 -2 101.44 3.06 2 12 -9 21.29 5.48 2 12 -8 58.88 6.20 2 12 -7 10.55 5.07 2 12 -6 29.75 4.87 2 12 -5 14.08 3.75 2 12 -4 82.51 3.57 2 13 -8 7.10 5.99 2 13 -7 46.64 5.58 2 13 -6 13.41 4.88 2 13 -5 10.68 4.29 2 14 -7 16.34 5.30 3 -16 -2 15.31 7.40 3 -15 -4 16.82 5.80 3 -15 -3 10.65 5.56 3 -15 -2 12.48 5.75 3 -15 -1 14.36 5.29 3 -15 0 17.79 5.75 3 -15 1 20.72 5.89 3 -14 -5 42.64 5.63 3 -14 -4 8.98 5.47 3 -14 -3 93.46 5.70 3 -14 -2 8.55 5.06 3 -14 -1 2.58 5.16 3 -14 0 11.13 4.96 3 -14 1 51.14 4.78 3 -14 2 6.37 5.07 3 -14 3 25.49 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3.06 3 -10 2 6.61 3.13 3 -10 3 204.46 4.40 3 -10 4 17.01 4.16 3 -10 5 33.75 4.73 3 -10 6 16.86 4.64 3 -10 7 52.96 5.22 3 -9 -11 14.27 5.66 3 -9 -10 17.95 5.02 3 -9 -9 38.07 4.70 3 -9 -8 109.45 4.54 3 -9 -7 16.66 3.59 3 -9 -6 85.09 4.03 3 -9 -5 7.42 3.27 3 -9 -4 40.66 3.29 3 -9 -3 43.09 2.96 3 -9 -2 78.37 3.10 3 -9 -1 43.98 2.81 3 -9 0 248.59 3.52 3 -9 1 22.31 2.80 3 -9 2 10.05 2.89 3 -9 3 13.99 3.18 3 -9 4 24.53 3.42 3 -9 5 108.76 4.26 3 -9 6 201.24 4.98 3 -9 7 14.12 4.76 3 -9 8 24.23 5.20 3 -8 -12 88.55 7.62 3 -8 -11 11.39 5.28 3 -8 -10 91.27 5.48 3 -8 -9 28.95 4.45 3 -8 -8 52.36 4.05 3 -8 -7 12.01 3.83 3 -8 -6 230.86 3.16 3 -8 -6 268.81 5.12 3 -8 -5 47.16 2.83 3 -8 -4 316.63 3.75 3 -8 -3 23.74 2.64 3 -8 -2 96.98 2.89 3 -8 -1 7.17 2.30 3 -8 0 12.49 2.46 3 -8 1 18.21 2.74 3 -8 2 673.51 4.80 3 -8 3 7.70 2.88 3 -8 4 11.41 3.59 3 -8 5 6.46 3.63 3 -8 6 17.17 3.65 3 -8 7 16.23 4.43 3 -8 8 33.50 4.88 3 -8 9 8.96 5.38 3 -7 -13 26.64 6.66 3 -7 -12 28.63 6.35 3 -7 -11 20.11 6.22 3 -7 -9 10.00 3.97 3 -7 -8 28.90 3.74 3 -7 -7 42.26 4.00 3 -7 -6 29.25 2.64 3 -7 -5 17.42 2.70 3 -7 -4 227.73 3.20 3 -7 -3 150.57 2.80 3 -7 -2 76.09 2.67 3 -7 -1 219.10 2.92 3 -7 0 499.36 3.76 3 -7 1 9.72 2.22 3 -7 2 60.88 2.50 3 -7 3 271.93 3.36 3 -7 4 33.12 2.63 3 -7 5 199.43 4.12 3 -7 6 72.69 3.74 3 -7 7 21.85 4.26 3 -7 8 71.51 4.50 3 -7 9 20.00 5.44 3 -7 10 29.20 5.66 3 -6 -11 53.34 5.11 3 -6 -10 17.35 3.87 3 -6 -9 32.87 3.99 3 -6 -8 36.24 3.97 3 -6 -7 437.29 5.20 3 -6 -6 30.29 2.59 3 -6 -5 827.29 4.36 3 -6 -4 526.23 3.71 3 -6 -3 752.30 4.00 3 -6 -2 209.95 2.69 3 -6 -1 333.08 3.19 3 -6 0 354.28 3.25 3 -6 1 65.69 2.33 3 -6 2 125.26 2.58 3 -6 3 839.96 4.36 3 -6 4 13.10 2.41 3 -6 5 47.47 3.41 3 -6 6 11.60 3.26 3 -6 7 14.65 3.75 3 -6 8 21.89 4.56 3 -6 9 77.70 4.93 3 -6 10 25.66 5.63 3 -5 -12 5.84 4.96 3 -5 -11 49.30 4.76 3 -5 -10 52.74 4.09 3 -5 -9 280.42 4.51 3 -5 -8 170.04 3.93 3 -5 -7 214.59 3.73 3 -5 -6 418.61 3.90 3 -5 -5 3.22 2.00 3 -5 -4 44.31 2.21 3 -5 -3 448.88 3.24 3 -5 -2 1023.82 4.49 3 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11.30 3.23 3 -3 9 31.57 3.87 3 -2 -13 20.94 5.21 3 -2 -11 102.81 3.56 3 -2 -10 42.67 3.22 3 -2 -9 102.13 3.79 3 -2 -8 210.55 3.00 3 -2 -7 785.95 4.49 3 -2 -6 24.01 2.14 3 -2 -5 927.17 4.29 3 -2 -4 14.76 1.85 3 -2 -3 1144.43 3.84 3 -2 -2 177.32 2.15 3 -2 -1 1.28 1.65 3 -2 0 72.74 1.82 3 -2 1 1406.44 4.42 3 -2 2 43.33 2.22 3 -2 3 3943.58 8.59 3 -2 4 125.43 2.82 3 -2 5 96.15 2.56 3 -2 6 82.72 2.88 3 -2 7 171.72 3.57 3 -2 8 7.93 3.18 3 -1 -14 21.48 5.85 3 -1 -13 8.13 5.17 3 -1 -10 250.77 3.92 3 -1 -9 507.76 4.75 3 -1 -8 561.72 4.12 3 -1 -7 589.26 3.73 3 -1 -6 383.23 3.23 3 -1 -5 80.74 2.33 3 -1 -4 375.83 2.69 3 -1 -3 442.59 2.81 3 -1 -2 96.10 1.83 3 -1 -1 3569.66 6.35 3 -1 0 124.61 1.93 3 -1 1 221.01 2.54 3 -1 2 -0.46 1.95 3 -1 3 80.44 2.34 3 -1 4 13.30 2.08 3 -1 5 1288.79 5.44 3 -1 6 408.39 3.60 3 -1 7 73.82 3.07 3 -1 8 14.39 2.85 3 0 -14 20.39 6.04 3 0 -13 5.32 5.24 3 0 -12 161.33 5.36 3 0 -10 49.70 3.03 3 0 -9 10.93 2.77 3 0 -8 25.35 2.35 3 0 -7 4.53 1.89 3 0 -6 356.28 2.67 3 0 -5 8.39 1.81 3 0 -4 157.57 2.23 3 0 -3 -0.31 1.66 3 0 -2 687.25 3.14 3 0 -1 9.63 1.67 3 0 0 778.45 3.46 3 0 1 6.23 1.62 3 0 2 3328.94 6.80 3 0 3 3.63 1.97 3 0 4 2114.34 6.09 3 0 5 4.92 2.39 3 0 6 9.71 2.58 3 0 7 4.66 2.78 3 1 -14 21.86 6.56 3 1 -13 14.33 5.26 3 1 -12 4.04 4.85 3 1 -9 398.87 3.23 3 1 -8 565.60 3.64 3 1 -7 657.71 3.70 3 1 -6 358.27 2.70 3 1 -5 73.68 1.89 3 1 -4 355.71 2.56 3 1 -3 439.23 2.82 3 1 0 117.02 1.95 3 1 1 208.40 2.15 3 1 2 8.22 2.01 3 1 3 78.77 2.04 3 1 4 18.23 2.04 3 1 5 1287.27 4.83 3 1 6 412.20 3.47 3 1 7 77.52 2.64 3 2 -14 8.95 6.58 3 2 -13 31.67 5.56 3 2 -12 15.75 5.05 3 2 -9 107.57 2.65 3 2 -8 226.04 2.59 3 2 -7 820.32 3.61 3 2 -6 22.75 1.97 3 2 -5 892.47 3.47 3 2 -4 18.93 1.66 3 2 -3 987.37 3.53 3 2 2 44.88 1.99 3 2 3 3875.70 7.05 3 2 4 131.60 2.33 3 2 5 105.46 2.22 3 2 6 79.82 2.26 3 3 -13 3.19 5.36 3 3 -12 13.93 4.80 3 3 -11 62.90 5.03 3 3 -7 187.31 2.28 3 3 -6 400.31 2.66 3 3 -5 90.61 1.91 3 3 -4 49.80 1.84 3 3 6 235.86 2.70 3 4 -13 9.43 4.74 3 4 -12 52.97 5.11 3 4 -11 12.89 4.90 3 4 -8 226.02 2.20 3 4 -7 7.63 1.77 3 4 -6 628.54 3.07 3 4 -5 8.48 1.82 3 4 3 14.47 1.99 3 5 -12 14.07 5.50 3 5 -11 46.51 5.18 3 5 -10 49.93 4.60 3 5 -7 189.47 2.06 3 5 -6 411.86 2.84 3 5 3 117.16 1.81 3 6 -12 1.84 3.48 3 6 -11 27.79 5.03 3 6 -10 6.70 4.34 3 6 -9 39.24 3.74 3 6 -7 400.94 2.56 3 6 -6 25.00 2.02 3 7 -12 12.43 4.54 3 7 -11 9.85 5.05 3 7 -10 82.03 4.80 3 7 -9 16.61 3.74 3 7 -8 26.26 3.58 3 8 -10 66.67 5.33 3 8 -9 20.27 4.26 3 8 -8 33.23 3.77 3 8 -7 12.05 3.65 3 9 -10 30.45 5.40 3 9 -9 28.03 4.72 3 9 -8 82.73 4.08 3 9 -6 70.56 3.54 3 9 -5 10.28 2.93 3 9 -4 36.33 2.68 3 9 -3 38.81 2.75 3 9 -2 84.66 2.57 3 9 -1 41.22 2.26 3 9 0 246.78 2.40 3 10 -10 14.00 5.66 3 10 -9 11.73 5.06 3 10 -8 20.49 4.18 3 10 -7 99.85 4.45 3 10 -6 8.99 3.56 3 10 -5 296.84 4.20 3 10 -4 14.09 2.89 3 10 -3 87.82 2.78 3 10 -2 7.68 2.54 3 10 -1 34.26 2.22 3 11 -9 2.61 5.11 3 11 -8 19.19 5.17 3 11 -7 47.83 4.86 3 11 -6 18.62 4.08 3 11 -5 7.64 3.69 3 11 -4 64.27 3.22 3 11 -3 105.28 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549.03 4.35 4 -8 1 10.95 2.58 4 -8 2 10.71 2.97 4 -8 3 106.46 3.41 4 -8 4 18.79 3.53 4 -8 5 11.41 3.75 4 -8 6 56.82 4.46 4 -8 7 4.46 4.70 4 -8 8 79.15 5.54 4 -7 -13 27.83 6.38 4 -7 -12 45.92 6.36 4 -7 -11 29.41 5.10 4 -7 -10 74.44 4.94 4 -7 -9 239.73 5.77 4 -7 -8 0.62 3.65 4 -7 -7 245.76 3.59 4 -7 -6 24.40 2.94 4 -7 -5 40.13 2.85 4 -7 -4 306.90 3.59 4 -7 -3 514.65 4.00 4 -7 -2 401.50 3.70 4 -7 -1 23.86 2.33 4 -7 0 198.38 3.27 4 -7 1 12.68 2.80 4 -7 2 212.93 3.43 4 -7 3 121.54 3.37 4 -7 4 223.71 4.46 4 -7 5 35.11 3.57 4 -7 6 165.45 4.49 4 -7 7 5.88 4.49 4 -7 8 12.37 5.17 4 -7 9 40.71 5.75 4 -6 -12 19.26 4.93 4 -6 -11 64.45 5.02 4 -6 -10 13.35 4.15 4 -6 -9 288.42 5.41 4 -6 -8 32.67 3.58 4 -6 -7 464.70 5.11 4 -6 -6 18.35 2.83 4 -6 -5 883.54 4.77 4 -6 -4 8.83 2.45 4 -6 -3 204.32 3.05 4 -6 -2 68.42 2.55 4 -6 -1 221.59 2.92 4 -6 0 5.16 2.43 4 -6 1 2122.92 6.89 4 -6 2 32.55 2.46 4 -6 3 57.94 2.69 4 -6 4 25.33 2.69 4 -6 5 93.89 3.78 4 -6 6 9.22 3.69 4 -6 7 123.43 4.37 4 -6 8 12.36 4.62 4 -6 9 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567.41 3.75 4 -3 -4 1310.51 4.81 4 -3 -3 1732.82 5.52 4 -3 -2 2324.79 6.20 4 -3 -1 63.38 2.28 4 -3 0 217.57 2.93 4 -3 1 628.93 3.75 4 -3 2 26.52 2.17 4 -3 3 343.44 3.31 4 -3 4 191.29 3.07 4 -3 5 173.08 3.61 4 -3 6 278.37 4.20 4 -3 7 15.05 3.43 4 -3 8 21.88 3.97 4 -2 -14 25.02 6.14 4 -2 -11 13.33 4.16 4 -2 -10 20.48 3.60 4 -2 -9 19.94 2.90 4 -2 -8 4.41 2.49 4 -2 -7 694.97 4.51 4 -2 -6 42.30 2.11 4 -2 -5 789.11 4.19 4 -2 -4 66.80 2.26 4 -2 -3 156.83 2.44 4 -2 -2 75.47 2.20 4 -2 -1 576.74 3.41 4 -2 0 206.59 2.76 4 -2 1 742.69 4.52 4 -2 2 182.31 2.83 4 -2 3 991.87 4.93 4 -2 4 147.59 2.90 4 -2 5 3.43 2.69 4 -2 6 14.80 2.68 4 -2 7 232.36 4.01 4 -2 8 10.44 3.61 4 -1 -14 8.70 6.22 4 -1 -11 89.12 4.11 4 -1 -10 102.47 3.37 4 -1 -9 259.01 3.62 4 -1 -8 258.90 3.50 4 -1 -7 15.06 2.74 4 -1 -6 234.78 2.96 4 -1 -5 81.75 2.37 4 -1 -4 668.26 3.71 4 -1 -3 1244.59 4.64 4 -1 -2 1833.05 5.31 4 -1 -1 247.95 2.82 4 -1 0 147.96 2.57 4 -1 1 219.78 3.09 4 -1 2 9.42 2.71 4 -1 3 358.46 3.30 4 -1 4 667.18 4.47 4 -1 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17.61 5.90 5 -12 -5 8.87 5.49 5 -12 -4 40.77 4.28 5 -12 -3 8.00 4.06 5 -12 -2 104.45 4.98 5 -12 -1 7.42 4.40 5 -12 0 8.88 4.44 5 -12 1 13.34 4.68 5 -12 2 3.22 3.31 5 -12 3 10.48 3.98 5 -11 -8 4.93 4.19 5 -11 -7 53.68 5.76 5 -11 -6 61.66 4.98 5 -11 -5 54.30 4.18 5 -11 -4 62.66 4.27 5 -11 -3 6.04 3.79 5 -11 -2 27.33 3.88 5 -11 -1 7.29 3.89 5 -11 0 6.07 3.71 5 -11 1 33.06 4.09 5 -11 2 18.86 4.63 5 -11 3 72.71 5.10 5 -11 4 17.16 3.51 5 -10 -10 6.29 3.79 5 -10 -8 1.04 5.05 5 -10 -7 109.17 4.96 5 -10 -6 7.30 3.84 5 -10 -5 1.95 3.63 5 -10 -4 17.04 3.60 5 -10 -3 25.79 3.50 5 -10 -2 13.98 3.57 5 -10 -1 305.55 4.75 5 -10 0 3.59 3.37 5 -10 1 37.83 3.65 5 -10 2 2.27 3.93 5 -10 3 21.04 4.29 5 -10 4 7.35 4.62 5 -9 -11 32.92 6.09 5 -9 -10 11.30 5.53 5 -9 -9 9.80 5.58 5 -9 -8 12.53 4.64 5 -9 -7 8.62 4.07 5 -9 -6 17.99 3.27 5 -9 -5 53.54 3.41 5 -9 -4 241.48 4.27 5 -9 -3 65.21 3.22 5 -9 -2 107.66 3.46 5 -9 -1 52.99 3.31 5 -9 0 119.01 3.51 5 -9 1 137.60 3.67 5 -9 2 63.27 3.55 5 -9 3 38.97 4.09 5 -9 4 24.53 4.31 5 -9 5 32.53 4.82 5 -9 6 9.62 3.69 5 -8 -12 20.79 6.23 5 -8 -11 5.28 5.39 5 -8 -10 82.42 6.53 5 -8 -9 30.85 4.42 5 -8 -8 236.85 5.04 5 -8 -7 9.76 3.30 5 -8 -6 233.08 4.01 5 -8 -5 53.59 3.30 5 -8 -4 5.59 2.90 5 -8 -3 51.18 2.94 5 -8 -2 734.26 5.14 5 -8 -1 11.64 3.06 5 -8 0 316.25 4.25 5 -8 1 110.48 3.47 5 -8 2 56.07 3.16 5 -8 3 7.56 3.92 5 -8 4 42.87 4.21 5 -8 5 -1.07 3.93 5 -8 6 109.92 5.48 5 -8 7 18.02 5.16 5 -7 -13 26.01 6.25 5 -7 -12 14.14 5.94 5 -7 -11 54.34 5.56 5 -7 -10 18.41 4.83 5 -7 -9 73.75 4.62 5 -7 -8 30.69 3.68 5 -7 -7 14.98 3.39 5 -7 -6 5.18 3.11 5 -7 -5 473.65 4.45 5 -7 -4 206.75 3.48 5 -7 -3 23.02 2.97 5 -7 -2 72.03 2.82 5 -7 -1 30.77 2.61 5 -7 0 25.01 2.86 5 -7 1 10.92 3.03 5 -7 2 411.13 4.40 5 -7 3 8.69 3.23 5 -7 4 172.97 4.67 5 -7 5 38.33 4.48 5 -7 6 13.48 4.49 5 -7 7 12.48 5.08 5 -7 8 18.35 6.27 5 -6 -13 27.72 6.17 5 -6 -12 9.01 5.78 5 -6 -11 13.50 5.58 5 -6 -10 17.69 4.43 5 -6 -9 243.51 4.89 5 -6 -8 133.37 4.39 5 -6 -7 170.11 3.65 5 -6 -6 11.62 2.82 5 -6 -5 8.90 2.70 5 -6 -4 152.64 3.10 5 -6 -3 297.42 3.52 5 -6 -2 17.07 2.68 5 -6 -1 536.73 4.09 5 -6 0 10.03 2.45 5 -6 1 1008.20 5.38 5 -6 2 54.13 3.02 5 -6 3 106.57 3.51 5 -6 4 82.71 3.67 5 -6 5 136.80 4.61 5 -6 6 12.22 4.25 5 -6 7 141.33 5.28 5 -6 8 21.49 5.24 5 -6 9 13.77 5.70 5 -5 -13 25.77 6.21 5 -5 -12 31.80 5.53 5 -5 -11 46.92 5.28 5 -5 -10 131.45 4.50 5 -5 -9 6.21 3.32 5 -5 -8 19.42 3.39 5 -5 -7 158.47 3.50 5 -5 -6 35.05 3.01 5 -5 -5 270.83 3.62 5 -5 -4 417.64 3.90 5 -5 -3 135.33 2.72 5 -5 -2 61.68 2.47 5 -5 -1 64.14 2.56 5 -5 0 20.08 2.51 5 -5 1 850.93 5.02 5 -5 2 543.52 4.28 5 -5 3 544.97 4.71 5 -5 4 16.64 3.09 5 -5 5 120.76 3.97 5 -5 6 7.31 3.98 5 -5 7 12.96 4.49 5 -5 8 34.08 5.11 5 -4 -12 14.73 5.43 5 -4 -11 8.63 4.51 5 -4 -10 56.05 3.80 5 -4 -9 38.06 3.85 5 -4 -8 319.75 4.43 5 -4 -7 127.30 3.37 5 -4 -6 32.32 2.96 5 -4 -5 10.27 2.54 5 -4 -4 12.34 2.16 5 -4 -3 81.43 2.33 5 -4 -2 1121.17 5.15 5 -4 -1 26.28 2.30 5 -4 0 332.93 3.58 5 -4 1 177.39 3.04 5 -4 2 57.54 2.82 5 -4 3 12.45 3.00 5 -4 4 93.87 3.36 5 -4 5 10.56 3.20 5 -4 6 137.72 4.30 5 -4 7 38.98 4.55 5 -4 8 81.27 5.31 5 -3 -12 54.71 5.09 5 -3 -11 93.67 4.75 5 -3 -10 15.27 3.43 5 -3 -9 14.46 3.00 5 -3 -8 77.91 3.30 5 -3 -7 3.13 2.63 5 -3 -6 460.24 4.27 5 -3 -5 1536.15 5.82 5 -3 -4 180.94 2.87 5 -3 -3 411.34 3.53 5 -3 -2 36.89 2.20 5 -3 -1 25.51 2.21 5 -3 0 721.00 4.42 5 -3 1 303.36 3.27 5 -3 2 68.58 2.71 5 -3 3 285.95 3.72 5 -3 4 219.61 3.58 5 -3 5 127.66 3.67 5 -3 6 4.67 3.58 5 -3 7 37.29 4.35 5 -3 8 7.48 4.67 5 -2 -12 14.57 4.29 5 -2 -11 132.03 4.25 5 -2 -10 36.63 3.61 5 -2 -9 181.40 3.54 5 -2 -8 117.64 3.22 5 -2 -7 443.20 4.45 5 -2 -6 8.83 2.28 5 -2 -5 5.70 2.36 5 -2 -4 4.72 2.35 5 -2 -3 535.80 3.69 5 -2 -2 4.31 2.10 5 -2 -1 2252.95 6.81 5 -2 0 144.74 2.60 5 -2 1 656.83 4.58 5 -2 2 7.66 2.84 5 -2 3 13.31 2.75 5 -2 4 6.19 2.76 5 -2 5 358.80 4.45 5 -2 6 22.46 3.55 5 -2 7 97.36 4.50 5 -1 -11 128.83 3.92 5 -1 -10 29.62 3.20 5 -1 -9 3.32 2.92 5 -1 -8 13.47 2.60 5 -1 -7 264.69 3.24 5 -1 -6 76.61 2.66 5 -1 -5 964.16 4.91 5 -1 -4 398.35 3.41 5 -1 -3 342.05 3.25 5 -1 -2 1064.38 4.83 5 -1 -1 155.50 2.63 5 -1 0 742.46 4.38 5 -1 1 258.74 3.16 5 -1 2 919.70 5.23 5 -1 3 366.30 3.86 5 -1 4 76.93 3.27 5 -1 5 11.18 3.15 5 -1 6 45.25 3.50 5 -1 7 31.55 3.51 5 0 -11 6.55 3.25 5 0 -10 221.60 3.73 5 0 -9 9.73 2.68 5 0 -8 1068.17 5.25 5 0 -7 1.75 2.16 5 0 -6 10.22 2.23 5 0 -5 5.19 2.41 5 0 -4 239.59 3.28 5 0 -3 6.70 1.92 5 0 -2 1285.41 5.10 5 0 -1 1.11 1.98 5 0 0 1811.18 6.08 5 0 1 2.26 2.25 5 0 2 582.85 4.42 5 0 3 8.69 2.57 5 0 4 299.95 3.68 5 0 5 5.58 2.97 5 0 6 45.04 3.29 5 1 -10 25.51 3.21 5 1 -9 8.48 3.27 5 1 -8 25.05 2.81 5 1 -7 293.24 3.59 5 1 -6 74.13 2.88 5 1 -5 973.14 4.88 5 1 -4 447.25 3.84 5 1 0 744.39 4.35 5 1 1 286.38 3.32 5 1 2 877.51 4.71 5 1 3 413.39 3.94 5 1 4 71.01 2.99 5 1 5 6.75 2.70 5 1 6 27.14 2.87 5 2 -10 33.62 3.13 5 2 -9 232.69 3.99 5 2 -8 110.49 3.02 5 2 -7 400.01 3.74 5 2 -6 7.62 2.65 5 2 -5 8.95 2.56 5 2 2 4.33 2.13 5 2 3 12.82 2.62 5 2 4 6.38 2.39 5 2 5 317.44 3.60 5 3 -9 24.56 2.71 5 3 -8 87.73 2.98 5 3 -7 14.73 2.63 5 3 -6 445.37 3.85 5 4 -9 25.65 2.54 5 4 -8 294.04 3.52 5 4 -7 128.48 3.07 5 4 -6 24.62 2.61 5 5 -8 11.80 2.55 5 5 -7 137.45 2.99 5 6 -8 109.22 2.68 5 7 -12 6.93 4.54 5 9 -11 19.52 4.50 5 9 -10 25.21 5.28 5 10 -10 7.78 5.32 5 10 -9 52.00 5.15 5 11 -9 5.37 4.88 5 11 -8 6.69 4.63 5 11 -7 57.25 5.01 5 11 -6 56.72 4.28 5 12 -9 3.80 6.18 5 12 -8 61.09 5.42 5 12 -7 15.06 4.86 5 12 -6 7.27 3.88 5 13 -8 19.18 5.55 6 -14 -3 19.06 6.30 6 -14 -2 14.17 6.36 6 -13 -5 18.26 4.59 6 -13 -4 13.31 5.19 6 -13 -3 11.37 5.12 6 -13 -2 14.40 5.43 6 -13 -1 16.50 5.38 6 -13 0 4.44 3.88 6 -12 -7 4.11 4.56 6 -12 -6 1.51 3.40 6 -12 -5 12.31 4.79 6 -12 -4 35.61 4.84 6 -12 -3 14.12 4.71 6 -12 -2 22.63 4.74 6 -12 -1 6.13 4.68 6 -12 0 11.45 4.72 6 -12 1 5.79 3.96 6 -11 -8 25.15 4.10 6 -11 -7 31.58 5.86 6 -11 -6 42.88 5.00 6 -11 -5 19.13 4.25 6 -11 -4 12.38 4.09 6 -11 -3 16.36 4.19 6 -11 -2 11.35 4.14 6 -11 -1 47.51 4.48 6 -11 0 12.53 4.41 6 -11 1 63.96 4.87 6 -11 2 40.87 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851.61 5.03 6 1 -4 1086.94 5.61 6 1 0 614.91 4.50 6 1 1 407.61 4.03 6 1 2 178.93 3.55 6 1 3 337.44 4.04 6 1 4 16.21 3.12 6 1 5 11.97 3.13 6 2 -10 6.79 3.26 6 2 -9 307.10 3.67 6 2 -8 87.00 3.23 6 2 -7 104.97 2.94 6 2 -6 71.71 2.82 6 2 -5 522.19 4.45 6 2 3 94.75 3.26 6 2 4 14.39 3.04 6 2 5 358.77 4.37 6 3 -10 3.75 2.74 6 3 -9 6.01 3.03 6 3 -8 388.29 4.16 6 3 -7 198.58 3.53 6 3 -6 163.70 3.31 6 4 -9 73.54 2.94 6 4 -8 14.63 2.92 6 4 -7 57.55 2.91 6 5 -8 17.48 2.72 6 5 -7 89.98 3.04 6 6 -8 128.66 3.17 6 11 -9 14.55 5.79 6 12 -9 10.84 5.91 6 12 -8 29.15 5.39 7 -13 -4 15.83 5.89 7 -13 -3 9.99 5.63 7 -13 -2 18.12 5.69 7 -12 -5 7.94 5.17 7 -12 -4 17.29 5.19 7 -12 -3 9.75 4.83 7 -12 -2 20.64 5.12 7 -12 -1 5.66 5.20 7 -11 -7 7.17 3.61 7 -11 -6 15.34 4.60 7 -11 -5 10.26 4.78 7 -11 -4 9.44 4.90 7 -11 -3 15.53 4.59 7 -11 -2 13.77 4.69 7 -11 -1 31.76 4.86 7 -11 0 21.30 4.23 7 -10 -8 16.53 3.58 7 -10 -7 20.24 4.82 7 -10 -6 11.33 4.59 7 -10 -5 16.69 4.25 7 -10 -4 10.94 4.35 7 -10 -3 69.04 4.39 7 -10 -2 4.40 4.15 7 -10 -1 11.56 4.42 7 -10 0 25.24 4.83 7 -10 1 3.71 3.17 7 -10 2 7.61 3.78 7 -9 -10 4.35 4.46 7 -9 -8 147.71 5.43 7 -9 -7 8.84 4.08 7 -9 -6 17.86 4.22 7 -9 -5 9.20 3.91 7 -9 -4 40.55 4.04 7 -9 -3 44.27 4.25 7 -9 -2 56.80 4.09 7 -9 -1 147.21 4.70 7 -9 0 30.93 4.44 7 -9 0 14.90 4.74 7 -9 1 60.55 5.01 7 -9 2 41.34 3.20 7 -8 -11 22.17 4.79 7 -8 -10 33.68 5.31 7 -8 -8 2.90 4.24 7 -8 -7 24.37 3.82 7 -8 -6 185.22 4.65 7 -8 -5 6.23 3.76 7 -8 -4 248.15 4.42 7 -8 -3 43.04 3.88 7 -8 -2 26.24 3.52 7 -8 -1 2.77 3.85 7 -8 0 22.77 4.09 7 -8 1 43.48 4.03 7 -8 2 275.33 5.68 7 -8 4 33.33 3.65 7 -7 -12 22.93 6.62 7 -7 -11 23.92 5.35 7 -7 -10 7.09 4.95 7 -7 -9 54.54 5.05 7 -7 -8 6.38 4.03 7 -7 -7 50.44 3.87 7 -7 -6 135.02 4.09 7 -7 -5 19.12 3.54 7 -7 -4 126.53 3.82 7 -7 -3 21.90 3.63 7 -7 -2 39.43 3.51 7 -7 -1 59.64 3.51 7 -7 0 165.62 4.13 7 -7 1 114.63 4.38 7 -7 2 22.83 3.97 7 -7 3 8.65 4.53 7 -7 5 20.82 4.17 7 -6 -13 27.92 6.81 7 -6 -12 5.04 5.78 7 -6 -11 87.89 5.38 7 -6 -10 6.07 4.65 7 -6 -9 11.62 4.16 7 -6 -8 49.08 4.10 7 -6 -7 23.20 3.51 7 -6 -6 11.02 3.41 7 -6 -5 426.72 5.08 7 -6 -4 7.20 3.27 7 -6 -3 346.00 4.55 7 -6 -2 8.27 3.12 7 -6 -1 7.25 3.43 7 -6 0 27.84 3.68 7 -6 1 254.44 4.55 7 -6 2 18.77 3.84 7 -6 3 98.60 4.56 7 -6 4 23.49 6.56 7 -6 6 18.87 5.48 7 -5 -13 16.20 6.89 7 -5 -12 15.18 5.79 7 -5 -11 16.10 4.80 7 -5 -10 134.60 4.85 7 -5 -9 128.22 4.27 7 -5 -8 85.02 4.28 7 -5 -7 23.01 3.27 7 -5 -6 312.71 4.65 7 -5 -5 23.85 3.17 7 -5 -4 5.21 3.08 7 -5 -3 65.15 3.26 7 -5 -2 105.35 3.62 7 -5 -1 300.93 4.25 7 -5 0 519.85 5.20 7 -5 1 24.12 3.46 7 -5 2 8.99 3.77 7 -5 3 10.04 4.09 7 -5 4 14.99 5.08 7 -5 5 15.50 4.79 7 -4 -13 65.97 5.96 7 -4 -12 104.49 5.51 7 -4 -11 10.20 4.67 7 -4 -10 45.28 4.42 7 -4 -9 12.90 4.08 7 -4 -8 3.13 3.64 7 -4 -7 1.33 3.85 7 -4 -6 20.54 3.25 7 -4 -5 194.85 3.63 7 -4 -4 302.39 4.13 7 -4 -3 192.55 3.56 7 -4 -2 249.09 4.00 7 -4 -1 8.96 3.04 7 -4 0 49.26 3.43 7 -4 1 22.78 3.74 7 -4 1 33.71 4.35 7 -4 2 242.20 4.43 7 -4 2 270.80 5.06 7 -4 3 8.02 3.74 7 -4 4 56.07 4.30 7 -4 5 9.24 4.80 7 -4 6 15.28 5.53 7 -4 7 26.42 5.68 7 -3 -12 25.76 5.21 7 -3 -11 6.96 4.46 7 -3 -10 35.56 4.11 7 -3 -9 77.25 4.17 7 -3 -8 29.02 4.21 7 -3 -7 389.11 4.71 7 -3 -6 9.91 2.91 7 -3 -5 61.14 3.05 7 -3 -4 6.14 2.89 7 -3 -3 97.54 3.34 7 -3 -2 51.36 3.00 7 -3 -1 87.26 3.66 7 -3 0 172.56 3.75 7 -3 1 135.45 3.83 7 -3 2 60.58 3.75 7 -3 3 79.87 4.25 7 -3 4 47.63 4.15 7 -3 5 129.50 5.03 7 -3 6 30.75 5.38 7 -2 -12 4.54 4.61 7 -2 -11 49.92 4.36 7 -2 -10 41.75 4.14 7 -2 -9 65.84 4.22 7 -2 -8 10.69 3.34 7 -2 -7 418.20 4.67 7 -2 -6 8.52 3.11 7 -2 -5 567.90 5.05 7 -2 -4 4.01 2.78 7 -2 -3 597.21 4.96 7 -2 -2 16.75 3.00 7 -2 -1 26.33 3.17 7 -2 0 14.87 3.15 7 -2 1 13.26 3.22 7 -2 2 5.15 3.22 7 -2 3 747.94 6.24 7 -2 4 10.07 3.99 7 -2 5 50.87 4.95 7 -2 6 10.37 5.11 7 -1 -12 20.29 4.23 7 -1 -11 19.63 4.13 7 -1 -10 79.60 4.14 7 -1 -9 20.03 3.40 7 -1 -8 138.92 3.76 7 -1 -7 122.07 3.79 7 -1 -6 104.42 3.75 7 -1 -5 109.74 3.49 7 -1 -4 22.89 3.24 7 -1 -3 47.77 3.17 7 -1 -2 414.72 4.44 7 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7.21 5.39 8 -12 -3 7.98 6.16 8 -12 -2 23.00 5.69 8 -11 -6 20.54 5.60 8 -11 -5 12.75 4.32 8 -11 -4 27.79 5.09 8 -11 -3 34.40 5.28 8 -11 -2 11.58 4.47 8 -11 -1 12.91 5.08 8 -10 -7 20.41 3.93 8 -10 -6 12.47 4.21 8 -10 -5 72.23 4.96 8 -10 -4 5.11 4.50 8 -10 -3 9.52 4.58 8 -10 -2 11.41 4.92 8 -10 -1 16.79 4.65 8 -10 0 11.93 5.20 8 -9 -8 9.13 3.82 8 -9 -7 10.52 3.89 8 -9 -6 19.70 4.70 8 -9 -5 17.36 4.68 8 -9 -4 52.78 4.52 8 -9 -3 75.90 4.68 8 -9 -2 29.72 4.66 8 -9 -1 19.20 4.79 8 -9 0 6.99 4.34 8 -9 1 2.86 3.86 8 -8 -10 10.73 4.02 8 -8 -8 19.20 5.03 8 -8 -7 9.21 4.19 8 -8 -6 115.93 4.72 8 -8 -5 11.81 4.22 8 -8 -4 14.43 3.98 8 -8 -3 8.42 4.28 8 -8 -3 16.72 4.95 8 -8 -2 5.50 3.99 8 -8 -1 16.25 4.36 8 -8 0 65.65 4.75 8 -8 1 13.39 4.47 8 -8 2 17.33 4.26 8 -7 -11 22.91 4.66 8 -7 -10 38.07 5.41 8 -7 -8 87.41 4.94 8 -7 -7 27.11 4.49 8 -7 -6 85.42 4.28 8 -7 -5 45.10 4.00 8 -7 -4 22.63 4.18 8 -7 -3 162.43 4.81 8 -7 -2 17.16 3.74 8 -7 -1 72.15 4.25 8 -7 0 60.55 4.28 8 -7 1 6.90 4.21 8 -6 -12 14.63 5.84 8 -6 -11 29.16 5.61 8 -6 -10 16.17 5.11 8 -6 -9 19.95 4.42 8 -6 -8 28.93 4.53 8 -6 -7 73.81 4.53 8 -6 -6 11.68 4.20 8 -6 -5 71.31 3.90 8 -6 -4 24.11 3.63 8 -6 -3 26.55 3.61 8 -6 -2 24.02 3.97 8 -6 -1 6.94 4.07 8 -6 0 25.53 4.09 8 -6 1 188.65 4.83 8 -6 2 10.66 4.25 8 -6 4 9.04 4.12 8 -5 -13 15.34 6.75 8 -5 -12 18.09 6.06 8 -5 -11 43.87 5.14 8 -5 -10 30.30 4.94 8 -5 -9 63.53 4.91 8 -5 -8 14.95 4.38 8 -5 -7 10.25 4.25 8 -5 -6 4.45 3.41 8 -5 -5 9.07 3.48 8 -5 -4 7.63 3.52 8 -5 -3 69.13 4.11 8 -5 -2 274.32 4.87 8 -5 -1 11.37 3.65 8 -5 0 50.96 4.17 8 -5 1 22.52 4.05 8 -5 2 15.08 4.55 8 -5 3 16.32 4.60 8 -5 4 81.56 5.03 8 -4 -13 25.66 5.88 8 -4 -12 28.65 5.73 8 -4 -11 13.45 4.62 8 -4 -10 9.77 4.94 8 -4 -9 17.42 4.28 8 -4 -8 92.93 4.66 8 -4 -7 24.86 3.40 8 -4 -6 344.82 4.52 8 -4 -5 55.29 3.82 8 -4 -4 253.96 4.39 8 -4 -3 8.70 3.51 8 -4 -2 8.33 3.44 8 -4 -1 18.78 3.45 8 -4 0 199.00 4.34 8 -4 1 20.62 4.22 8 -4 2 137.76 5.00 8 -4 3 9.25 4.57 8 -4 4 46.08 5.26 8 -4 5 22.50 5.99 8 -3 -13 18.41 6.13 8 -3 -12 27.56 5.49 8 -3 -11 22.29 4.42 8 -3 -10 53.92 4.62 8 -3 -9 205.02 5.66 8 -3 -8 67.81 3.81 8 -3 -7 267.58 4.65 8 -3 -6 13.26 4.13 8 -3 -5 14.67 3.65 8 -3 -4 67.18 3.51 8 -3 -3 60.16 3.78 8 -3 -2 226.31 4.35 8 -3 -1 153.38 3.88 8 -3 -1 175.14 4.94 8 -3 0 25.41 3.53 8 -3 1 85.67 4.39 8 -3 2 25.82 4.30 8 -3 3 15.28 4.37 8 -3 4 45.42 5.26 8 -3 5 11.88 5.54 8 -3 6 15.14 6.45 8 -2 -12 14.03 4.98 8 -2 -11 38.32 5.35 8 -2 -10 10.75 4.14 8 -2 -9 54.09 3.98 8 -2 -8 4.97 3.85 8 -2 -7 361.26 5.60 8 -2 -6 0.99 3.63 8 -2 -5 184.06 4.44 8 -2 -4 6.97 3.61 8 -2 -3 47.18 3.67 8 -2 -2 28.50 4.91 8 -2 -2 13.76 3.47 8 -2 -1 55.33 3.48 8 -2 0 12.67 3.54 8 -2 0 14.73 4.64 8 -2 1 480.33 5.49 8 -2 2 59.76 4.18 8 -2 3 78.49 4.65 8 -2 4 12.07 4.84 8 -2 5 14.49 5.01 8 -1 -12 12.30 5.12 8 -1 -11 28.21 4.92 8 -1 -10 94.69 4.16 8 -1 -9 174.49 4.58 8 -1 -8 45.22 4.18 8 -1 -7 12.14 3.64 8 -1 -6 13.23 3.78 8 -1 -5 236.22 4.70 8 -1 -4 62.92 3.55 8 -1 -3 71.63 3.69 8 -1 -2 294.02 4.70 8 -1 -1 10.04 3.61 8 -1 0 9.12 3.63 8 -1 2 18.78 3.59 8 -1 3 110.26 4.40 8 -1 4 50.30 4.77 8 -1 5 60.71 5.16 8 0 -11 8.58 3.86 8 0 -10 1.07 4.03 8 0 -9 10.25 3.76 8 0 -8 659.03 5.98 8 0 -7 2.53 3.41 8 0 -6 576.53 5.83 8 0 -5 4.04 3.55 8 0 -4 101.28 4.10 8 0 -3 0.26 3.23 8 0 -2 103.27 3.99 8 0 -1 5.31 3.60 8 0 0 212.07 4.60 8 0 1 4.74 3.77 8 0 2 210.17 4.63 8 0 3 18.54 4.49 8 0 4 202.47 5.49 8 0 5 6.74 4.98 8 1 -11 28.58 3.79 8 1 -10 92.75 4.30 8 1 -9 178.15 4.63 8 1 -8 38.19 3.67 8 1 -7 15.50 3.78 8 1 -6 11.79 3.81 8 1 -5 260.21 4.64 8 1 -4 59.20 3.69 8 1 2 13.59 3.93 8 1 3 116.11 4.81 8 1 4 54.57 4.61 8 2 -11 17.19 3.81 8 2 -10 8.48 3.84 8 2 -9 61.22 3.94 8 2 -8 8.33 3.68 8 2 -7 311.54 4.83 8 2 -6 9.97 3.89 8 2 -5 207.09 4.58 8 3 -10 52.34 3.91 8 3 -9 145.38 4.42 8 3 -8 56.44 4.17 8 3 -7 288.06 4.94 8 3 -6 4.83 3.48 8 4 -10 16.10 3.47 8 4 -9 12.65 3.93 8 4 -8 81.72 3.90 8 4 -7 16.73 3.68 8 5 -9 64.28 4.08 8 5 -8 14.15 3.95 8 5 -7 11.39 3.79 8 6 -9 17.15 3.52 8 6 -8 24.36 3.87 8 7 -8 70.67 4.04 9 -10 -6 15.11 5.74 9 -10 -5 19.76 5.49 9 -10 -4 15.11 5.23 9 -10 -3 27.10 5.72 9 -10 -2 7.72 5.74 9 -10 -1 6.58 5.69 9 -9 -7 13.52 5.13 9 -9 -6 8.57 4.17 9 -9 -5 41.67 4.45 9 -9 -4 38.82 5.09 9 -9 -3 16.33 5.07 9 -9 -2 22.66 5.16 9 -9 -1 9.81 4.81 9 -8 -8 16.68 3.43 9 -8 -7 10.88 4.65 9 -8 -6 15.70 4.04 9 -8 -5 11.37 4.64 9 -8 -4 9.08 4.37 9 -8 -3 4.54 4.93 9 -8 -2 9.58 4.16 9 -8 -1 11.88 4.56 9 -8 0 37.07 5.11 9 -7 -8 9.81 4.11 9 -7 -7 14.27 4.59 9 -7 -6 94.40 4.66 9 -7 -5 87.42 6.23 9 -7 -5 70.19 4.68 9 -7 -4 5.20 4.41 9 -7 -3 15.42 4.58 9 -7 -2 6.81 4.63 9 -7 -1 7.86 3.78 9 -7 0 5.56 4.21 9 -7 1 20.73 5.14 9 -6 -10 15.16 4.13 9 -6 -7 157.57 4.92 9 -6 -6 34.01 6.58 9 -6 -6 7.03 4.37 9 -6 -5 5.12 3.94 9 -6 -4 12.07 4.41 9 -6 -3 16.46 4.35 9 -6 -2 16.57 4.68 9 -6 -1 84.49 5.19 9 -6 0 5.22 3.98 9 -6 1 19.34 5.25 9 -5 -11 45.92 5.56 9 -5 -10 29.78 5.73 9 -5 -9 9.58 4.95 9 -5 -8 20.23 5.50 9 -5 -7 7.48 4.45 9 -5 -6 30.91 4.32 9 -5 -5 122.86 4.50 9 -5 -4 104.12 4.61 9 -5 -3 73.08 4.70 9 -5 -2 43.67 4.25 9 -5 -1 4.77 4.66 9 -5 0 15.63 4.66 9 -5 1 13.05 4.90 9 -5 2 6.18 4.39 9 -4 -12 14.66 5.94 9 -4 -11 7.19 5.77 9 -4 -10 40.47 5.30 9 -4 -9 11.62 5.17 9 -4 -8 117.73 5.10 9 -4 -7 7.78 4.16 9 -4 -6 104.46 4.48 9 -4 -5 103.32 4.60 9 -4 -4 7.32 4.12 9 -4 -3 20.46 4.25 9 -4 -2 250.94 5.01 9 -4 -1 12.35 4.64 9 -4 0 168.02 5.26 9 -4 1 7.90 4.91 9 -4 2 19.74 5.46 9 -4 3 10.54 5.84 9 -3 -13 39.69 6.24 9 -3 -12 1.91 5.87 9 -3 -11 51.82 5.62 9 -3 -10 23.07 4.41 9 -3 -9 4.47 4.44 9 -3 -8 5.99 4.25 9 -3 -7 28.33 4.59 9 -3 -6 14.84 4.34 9 -3 -5 140.96 4.53 9 -3 -4 293.15 5.22 9 -3 -3 16.86 3.72 9 -3 -2 42.19 5.17 9 -3 -2 28.87 4.28 9 -3 -1 90.14 4.63 9 -3 0 30.80 4.73 9 -3 1 66.96 5.28 9 -3 2 23.99 5.18 9 -3 3 15.91 5.37 9 -3 4 21.95 6.17 9 -2 -12 14.72 5.77 9 -2 -11 13.72 5.33 9 -2 -10 28.35 4.44 9 -2 -9 67.83 4.56 9 -2 -8 13.74 4.24 9 -2 -7 281.68 5.19 9 -2 -6 13.63 4.37 9 -2 -5 47.02 4.01 9 -2 -4 17.92 4.51 9 -2 -3 80.80 4.45 9 -2 -2 12.62 3.94 9 -2 -1 342.85 5.42 9 -2 0 8.53 4.43 9 -2 1 121.47 5.22 9 -2 2 11.92 4.95 9 -2 3 11.65 5.42 9 -2 4 17.42 5.70 9 -1 -12 49.50 5.56 9 -1 -11 34.91 5.99 9 -1 -10 27.73 4.60 9 -1 -9 102.42 4.43 9 -1 -8 10.57 4.15 9 -1 -7 25.52 4.54 9 -1 -6 22.58 4.46 9 -1 -5 64.04 3.86 9 -1 -3 101.29 4.27 9 -1 -2 37.53 4.12 9 -1 -1 36.05 4.31 9 -1 0 13.54 4.18 9 -1 1 6.27 4.41 9 -1 2 16.27 4.83 9 -1 3 102.28 5.62 9 -1 4 21.94 5.81 9 0 -12 10.61 5.29 9 0 -11 19.90 4.56 9 0 -10 37.89 4.65 9 0 -9 12.91 4.56 9 0 -8 152.98 5.05 9 0 -7 18.22 3.87 9 0 -6 5.68 4.01 9 0 -5 9.14 3.74 9 0 -4 19.53 3.80 9 0 -3 1.62 4.30 9 0 -2 557.56 6.15 9 0 -1 12.77 4.22 9 0 1 15.59 4.40 9 0 2 212.74 5.77 9 0 3 12.56 5.28 9 0 4 28.13 5.48 9 1 -11 36.45 4.61 9 1 -10 18.02 4.86 9 1 -9 102.84 5.04 9 1 -8 15.08 4.29 9 1 -7 12.89 3.84 9 1 -6 7.40 4.16 9 1 -5 77.73 4.14 9 1 -4 243.77 4.68 9 1 -3 104.30 4.70 9 2 -11 13.16 4.29 9 2 -10 27.39 4.99 9 2 -9 90.26 4.98 9 2 -8 5.46 4.16 9 2 -7 303.57 5.51 9 2 -6 12.14 4.25 9 2 -5 59.98 4.06 9 2 -4 11.86 4.13 9 3 -10 20.98 4.63 9 3 -9 3.59 4.87 9 3 -8 4.92 4.93 9 3 -7 41.04 4.53 9 3 -6 13.97 4.15 9 3 -5 138.84 4.72 9 4 -10 42.04 4.73 9 4 -9 12.55 4.58 9 4 -8 116.59 5.13 9 4 -7 20.38 4.58 9 4 -6 106.42 4.67 9 5 -9 6.50 4.45 9 5 -8 12.95 4.66 9 5 -7 15.54 4.57 9 6 -9 19.90 4.52 9 6 -8 10.30 4.68 9 7 -8 16.33 4.64 10 -9 -7 27.09 6.25 10 -8 -7 16.69 5.65 10 -8 -6 19.13 5.47 10 -8 -5 14.72 5.43 10 -8 -4 3.02 3.89 10 -8 -3 2.53 6.18 10 -8 -2 13.54 5.37 10 -8 -1 15.42 5.55 10 -7 -6 8.97 4.71 10 -7 -5 18.44 4.21 10 -7 -4 23.06 4.45 10 -7 -3 5.36 4.36 10 -7 -2 7.06 5.19 10 -7 -1 9.45 5.32 10 -7 0 18.94 5.43 10 -6 -8 24.15 5.93 10 -6 -6 10.27 4.23 10 -6 -5 12.25 3.99 10 -6 -4 11.23 4.88 10 -6 -3 73.11 4.61 10 -6 -2 6.89 4.28 10 -6 -1 37.03 5.95 10 -6 0 20.83 6.12 10 -5 -7 67.39 4.21 10 -5 -6 117.07 5.03 10 -5 -5 27.65 4.65 10 -5 -4 68.51 5.17 10 -5 -3 13.69 4.85 10 -5 -2 14.39 4.34 10 -5 -1 5.75 4.61 10 -5 0 27.27 5.58 10 -5 1 17.14 5.83 10 -4 -10 87.79 4.33 10 -4 -9 7.42 3.85 10 -4 -7 5.82 4.97 10 -4 -6 10.95 5.01 10 -4 -5 0.75 4.47 10 -4 -4 107.00 5.06 10 -4 -3 17.29 4.90 10 -4 -2 111.48 4.57 10 -4 -1 26.81 4.86 10 -4 0 23.99 4.57 10 -4 1 14.69 5.95 10 -3 -11 29.62 5.91 10 -3 -10 24.02 6.41 10 -3 -9 17.11 5.27 10 -3 -6 94.48 5.35 10 -3 -5 36.23 5.00 10 -3 -4 23.64 5.07 10 -3 -3 52.35 4.99 10 -3 -2 5.25 5.10 10 -3 -1 3.31 4.51 10 -3 0 5.10 4.75 10 -3 1 47.00 5.34 10 -3 2 19.31 6.28 10 -2 -12 13.67 6.59 10 -2 -11 45.04 6.50 10 -2 -10 9.07 5.15 10 -2 -9 109.58 5.24 10 -2 -8 12.61 5.61 10 -2 -7 11.51 4.58 10 -2 -6 4.35 4.54 10 -2 -5 109.25 5.40 10 -2 -4 14.93 4.99 10 -2 -3 79.71 5.04 10 -2 -2 6.87 4.81 10 -2 -1 94.13 5.13 10 -2 0 11.61 5.19 10 -2 1 15.01 5.45 10 -2 2 5.95 5.81 10 -1 -12 27.62 5.66 10 -1 -11 21.91 5.71 10 -1 -10 0.00 5.31 10 -1 -9 16.61 5.27 10 -1 -8 21.13 5.02 10 -1 -5 13.92 4.62 10 -1 -4 53.35 5.01 10 -1 -3 35.12 4.67 10 -1 -2 10.44 4.84 10 -1 -1 11.17 4.58 10 -1 0 8.44 4.98 10 -1 1 14.20 5.18 10 -1 2 48.38 6.03 10 0 -12 21.85 6.53 10 0 -11 11.13 5.49 10 0 -10 51.94 5.60 10 0 -9 9.05 5.20 10 0 -8 9.39 5.11 10 0 -7 14.91 6.21 10 0 -6 29.46 4.99 10 0 -5 14.43 4.69 10 0 -4 57.79 4.65 10 0 -3 11.77 4.63 10 0 -2 130.20 4.97 10 0 -1 8.21 4.81 10 0 0 46.09 5.00 10 0 1 10.36 4.95 10 1 -11 10.80 5.21 10 1 -10 16.92 5.83 10 1 -9 4.37 5.08 10 1 -8 33.85 5.22 10 1 -7 3.87 4.69 10 1 -6 73.70 5.54 10 1 -5 13.24 4.99 10 1 -4 61.33 5.32 10 1 -3 26.25 4.71 10 1 -2 20.19 4.73 10 2 -11 26.04 5.52 10 2 -10 22.31 5.60 10 2 -9 96.11 5.85 10 2 -8 2.18 5.18 10 2 -7 15.51 5.18 10 2 -6 -2.11 5.24 10 2 -5 115.67 5.34 10 2 -4 4.98 5.03 10 3 -10 27.65 5.43 10 3 -9 18.98 5.41 10 3 -8 50.72 5.64 10 3 -7 107.27 5.64 10 3 -6 89.04 5.63 10 3 -5 34.28 4.92 10 4 -10 81.60 5.70 10 4 -9 20.40 5.51 10 4 -8 26.67 5.34 10 4 -7 1.71 5.28 10 4 -6 5.61 4.57 10 5 -9 24.96 5.26 10 5 -8 24.35 5.67 10 5 -7 79.39 5.27 10 6 -9 79.90 5.52 10 6 -8 19.56 5.49 10 6 -7 35.48 5.37 10 7 -8 18.99 5.17 10 8 -8 29.10 5.39 11 -4 -4 70.09 4.01 11 -3 -7 48.93 4.36 11 -3 -6 27.62 3.90 11 -3 -5 12.89 3.79 11 -3 -4 10.07 4.17 11 -3 -3 5.78 4.31 11 -2 -8 5.93 4.82 11 -2 -6 9.35 4.32 11 -2 -5 70.51 4.18 11 -2 -4 7.57 3.96 11 -2 -3 45.70 4.36 11 -2 -2 7.49 3.92 11 -1 -9 77.31 5.22 11 -1 -8 22.60 4.18 11 -1 -5 91.42 4.77 11 -1 -4 4.03 3.84 11 -1 -3 8.83 4.13 11 -1 -2 7.24 3.63 11 0 -9 21.17 7.03 11 0 -7 5.00 3.93 11 0 -5 10.40 3.96 11 0 -4 208.27 4.69 11 0 -3 2.87 4.05 11 0 -2 11.16 4.06 11 1 -9 67.03 5.77 11 1 -8 36.03 6.03 11 1 -7 37.66 4.57 11 1 -4 5.81 4.12 11 1 -3 17.64 4.16 11 2 -11 43.21 6.63 11 2 -10 2.00 6.40 11 2 -9 32.29 6.53 11 2 -8 16.75 5.74 11 2 -7 34.74 6.45 11 2 -6 15.79 4.30 11 2 -4 9.60 4.04 11 2 -3 30.51 4.14 11 3 -11 15.21 5.78 11 3 -10 27.00 6.45 11 3 -9 6.65 6.09 11 3 -8 72.14 6.18 11 3 -7 61.83 5.79 11 3 -6 35.84 4.45 11 3 -4 14.30 3.69 11 4 -10 21.24 6.36 11 4 -9 4.55 6.17 11 4 -8 18.95 6.08 11 4 -7 7.47 5.66 11 4 -6 66.17 4.07 11 4 -5 10.55 4.33 11 5 -9 26.29 6.71 11 5 -7 56.59 7.96 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 28921 _shelx_SHELXL_version_number '2014/7' _olex2_submission_special_instructions 'No special instructions were received'