#\#CIF_1.1
 
#  CIF produced by WinGX routine CIF_UPDATE
#  Created on 2005-11-07 at 10:44:42
#  Using CIFtbx version 2.6.2 16 Jun 1998
 
#  Dictionary name : cif_core.dic
#  Dictionary vers : 2.3
#  Request file    : c:\wingx\files\cifdoc.dat
#  CIF files read  : shelxl cif _Template_texray.inf
 
#------------------ SECTION 1. GLOBAL INFORMATION ---------------------------#
 
data_global
 
#------------------ AUDIT DETAILS -------------------------------------------#
 
_audit_creation_date            2005-11-07
_audit_creation_method          'WinGX routine CIF_UPDATE'
_audit_conform_dict_name        cif_core.dic
_audit_conform_dict_version     2.3
_audit_conform_dict_location    ftp://ftp.iucr.org/pub/cif_core.dic
_audit_update_record            ?
 
#------------------ SUBMISSION DETAILS --------------------------------------#
 
# Name and address of author for correspondence
 
_publ_contact_author_name      'Tram\^sek, Melita'
_publ_contact_author_address

;
Department of Inorganic Chemistry and Technology
Jozef Stefan Institute
Jamova 39 1000 Ljubljana
SLOVENIA
;

_publ_contact_author_email       'melita.tramsek@ijs.si'
_publ_contact_author_fax         '386(1)4773645'
_publ_contact_author_phone       '386(1)4773155'
 
_publ_requested_journal          'Acta Crystallographica C'
_publ_requested_coeditor_name    ?
_publ_contact_letter            # Include date of submission
;
Date of submission ?

Please consider this CIF submission for publication as a
Regular Structural Paper in Acta Crystallographica C.
;
_publ_requested_category        ?
 
#------------------ PROCESSING SUMMARY (JOURNAL OFFICE ONLY) ----------------#
 
_journal_date_recd_electronic    ?
_journal_date_to_coeditor        ?
_journal_date_from_coeditor      ?
_journal_date_accepted           ?
_journal_date_printers_first     ?
_journal_date_printers_final     ?
_journal_date_proofs_out         ?
_journal_date_proofs_in          ?
_journal_coeditor_name           ?
_journal_coeditor_code           ?
_journal_coeditor_notes          ?
_journal_techeditor_code         ?
_journal_techeditor_notes        ?
_journal_coden_ASTM              ?
_journal_name_full               'Acta Chimica Slovenica'
_journal_year                    ?
_journal_volume                  ?
_journal_issue                   ?
_journal_page_first              ?
_journal_page_last               ?
_journal_suppl_publ_number       ?
_journal_suppl_publ_pages        ?
 
#------------------ TITLE AND AUTHOR LIST------------------------------------#
 
_publ_section_title
;
Oxidation of ruthenium and iridium metal by XeF2 and crystal structure
determination of [Xe~2~F~3~][RuF~6~]?XeF~2~ and [Xe~2~F~3~][MF~6~] (M = Ru,
Ir)
;

 
_publ_section_title_footnote
.
 
loop_
_publ_author_name
_publ_author_address
_publ_author_footnote
_publ_author_email
'Tram\^sek, Melita'
;
Department of Inorganic Chemistry and Technology
Jozef Stefan Institute
Jamova 39 1000 Ljubljana
SLOVENIA
;
.
;
melita.tramsek@ijs.si
;
'Goreshnik, Evgeny'
;
Department of Inorganic Chemistry and Technology
Jozef Stefan Institute
Jamova 39 1000 Ljubljana
SLOVENIA
;
.
;
evgeny.goreshnik@ijs.si
;
'Tav\<car, Ga\<sper'
;
Department of Inorganic Chemistry and Technology
Jozef Stefan Institute
Jamova 39 1000 Ljubljana
SLOVENIA
;
.
;
gasper.tavcar@ijs.si
;

 
#------------------ TEXT ----------------------------------------------------#

 
_publ_section_synopsis
;
# Insert blank lines between paragraphs
?
;
_publ_section_abstract
;
# Insert blank lines between paragraphs
 ?
;
 
_publ_section_comment
;
# Insert blank lines between paragraphs
 ?
;
 
_publ_section_exptl_prep
;
 ?
;
 
_publ_section_exptl_refinement
;
 ?
;
 
# Insert blank lines between references
 
_publ_section_references
;
F. H. Allen, O. Johnson, G. P. Shields, B. R. Smith, M. Towler, J. Applied 
Cryst., 37, 331-334, 2004 

Rigaku Corporation (1999). CrystalClear.

Sheldrick, G.M. (1997) SHELXL97. Program for crystal structure 
refinement. University of G\"ottingen, Germany.

Zachariasen, W. H. (1967). Acta Cryst. 23, 558-564.

Altomare, A., Cascarano, M., 
Giacovazzo, C., Guagliardi, A. (1994). 
J. Appl. Cryst., 26, 343. 

Blessing, R. H. (1995) Acta Cryst., A51, 33-38.

;
_publ_section_figure_captions
;
 Figure 1. View of (I) (50% probability displacement ellipsoids)
;
_publ_section_acknowledgements
;
 ?
;
_publ_section_table_legends
;
Table 1. Fractional atomic coordinates and equivalent
         isotropic displacement parameters (\%A^2^)
 
Table 2. Selected geometric parameters (\%A ,\% )
;
 
#------------------  SECTION 2. COMPOUND(S) DETAILS -------------------------#
 
data_shelxl
 
_audit_creation_date                    2006-11-20T16:38:35-00:00
_audit_creation_method                  'WinGX routine CIF_UPDATE'
 
#------------------ CHEMICAL INFORMATION ------------------------------------#
 
_chemical_formula_moiety                'F6 Ru, F3 Xe2, F2 Xe '
_chemical_formula_sum                   'F11 Ru Xe3'
_chemical_formula_weight                703.94
 
#------------------ UNIT CELL INFORMATION -----------------------------------#
 
_symmetry_cell_setting                  'triclinic'
_symmetry_space_group_name_H-M          'P -1'
_symmetry_space_group_name_Hall          '-P 1'

loop_
    _symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
 
_cell_length_a                          8.33620(10)
_cell_length_b                          8.8197(2)
_cell_length_c                          9.3026(4)
_cell_angle_alpha                       68.277(13)
_cell_angle_beta                        63.451(12)
_cell_angle_gamma                       82.020(16)
_cell_volume                            568.09(9)
_cell_formula_units_Z                   2
_cell_measurement_temperature           200
_cell_measurement_reflns_used           1262
_cell_measurement_theta_min             2.487
_cell_measurement_theta_max             28.6986
 
#------------------ CRYSTAL INFORMATION -------------------------------------#
 
_exptl_crystal_description              Chunk
_exptl_crystal_colour                   Colorless
_exptl_crystal_size_max                 0.08
_exptl_crystal_size_mid                 0.06
_exptl_crystal_size_min                 0.04
_exptl_crystal_density_diffrn           4.115
_exptl_crystal_density_method           'not measured'
_exptl_crystal_F_000                    610
_exptl_absorpt_coefficient_mu           10.289
_exptl_absorpt_correction_type          Multi-scan
_exptl_absorpt_correction_T_min         0.478
_exptl_absorpt_correction_T_max         0.657
_exptl_absorpt_process_details  'Blessing R.H., 1995'
 
#------------------ DATA COLLECTION INFORMATION -----------------------------#
 
_diffrn_ambient_temperature             200
_diffrn_radiation_wavelength            0.71069
_diffrn_radiation_type                  MoK\a
_diffrn_measurement_device
;
        Mercury CCD (2x2 bin mode)
;
_diffrn_measurement_method              dtprofit.ref
_diffrn_reflns_number                   2878
_diffrn_reflns_av_R_equivalents         0.0367
_diffrn_reflns_limit_h_min              -8
_diffrn_reflns_limit_h_max              11
_diffrn_reflns_limit_k_min              -10
_diffrn_reflns_limit_k_max              11
_diffrn_reflns_limit_l_min              -11
_diffrn_reflns_limit_l_max              12
_diffrn_reflns_theta_min                2.49
_diffrn_reflns_theta_max                28.87
_diffrn_reflns_theta_full               25
_diffrn_measured_fraction_theta_max
                                        0.754
_diffrn_measured_fraction_theta_full
                                        0.918
_reflns_number_total                    2259
_reflns_number_gt                       1837
_reflns_threshold_expression            I>2\s(I)
 
#------------------ COMPUTER PROGRAMS USED ----------------------------------#
 
_computing_data_collection
                                       'CrystalClear (Rigaku Corporation, 1999)'
_computing_cell_refinement
                                       'CrystalClear (Rigaku Corporation, 1999)'
_computing_data_reduction
                                       'CrystalClear (Rigaku Corporation, 1999)'
_computing_structure_solution
;
        SIR92 (Altomare, et. al. 1994)
;
_computing_structure_refinement         'SHELXL-97 (Sheldrick, 1997)'
_computing_publication_material   'enCIFer 1.2 (F. H. Allen et al, 2004)'

 
#------------------ REFINEMENT INFORMATION ----------------------------------#
 
_refine_ls_structure_factor_coef        Fsqd
_refine_ls_matrix_type                  full
_refine_ls_weighting_scheme             calc
_refine_ls_weighting_details
         'calc w=1/[\s^2^(Fo^2^)+(0.0964P)^2^+2.0781P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_extinction_method            SHELXL
_refine_ls_extinction_expression
                                    Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_coef              0.0099(11)
_refine_ls_number_reflns                2259
_refine_ls_number_parameters            137
_refine_ls_number_restraints            0
_refine_ls_R_factor_gt                  0.0608
_refine_ls_wR_factor_ref                0.1775
_refine_ls_goodness_of_fit_ref          1.134
_refine_ls_restrained_S_all             1.134
_refine_ls_shift/su_max                 0
_refine_diff_density_max                1.758
_refine_diff_density_min                -3.063
_iucr_refine_instructions_details
;
TITL Template texray.inf
CELL  0.71069   8.3362   8.8197   9.3026   68.277   63.451   82.020
ZERR     2.00   0.0001   0.0002   0.0004    0.013    0.012    0.016
LATT   1
SFAC  XE   RU   F
UNIT  6    2    22
MERG   2
OMIT     3  -8   1
OMIT     3  -5   3
OMIT     7  -4   7
OMIT    10   1   8
OMIT    -2   9   1
OMIT     6  -8   1
OMIT     1   0   0
OMIT    -5   3   0
CONN  12 3 XE2 XE2 XE3
FMAP   2
PLAN   20
ACTA    50.00
L.S.  22
WGHT    0.096600    2.063400
EXTI    0.009917
FVAR       0.52899
XE1   1    0.702929    0.335373    0.227906    11.00000    0.02433    0.03997 =
         0.03532   -0.01521   -0.01152    0.00237
XE2   1    0.227140    0.170360    0.278499    11.00000    0.02153    0.03735 =
         0.02723   -0.01029   -0.00746   -0.00298
XE3   1    0.206282    0.163459    0.786430    11.00000    0.02520    0.04223 =
         0.02904   -0.00906   -0.00962   -0.00372
RU1   2    0.285760    0.681642    0.275837    11.00000    0.02128    0.03135 =
         0.02627   -0.00901   -0.00736   -0.00219
F1    3    0.498061    0.242799    0.200714    11.00000    0.02346    0.11479 =
         0.04578   -0.03035   -0.01098   -0.01358
F2    3    0.891160    0.421203    0.243046    11.00000    0.05160    0.06619 =
         0.08472   -0.03235   -0.03462   -0.00882
F3    3   -0.009286    0.093170    0.346948    11.00000    0.02363    0.05775 =
         0.04088   -0.00305   -0.00434   -0.02174
F4    3    0.258149    0.876945    0.125971    11.00000    0.04951    0.04897 =
         0.04825   -0.01022   -0.02344    0.00186
F5    3    0.219760    0.574027    0.173426    11.00000    0.05918    0.06319 =
         0.04822   -0.02493   -0.01578   -0.01896
F6    3    0.050221    0.686243    0.427952    11.00000    0.01778    0.05747 =
         0.04565   -0.01861   -0.00939    0.00761
F7    3    0.317429    0.484964    0.424208    11.00000    0.03732    0.04120 =
         0.05051   -0.00437   -0.00971    0.00670
F8    3    0.353679    0.792578    0.376445    11.00000    0.04002    0.05396 =
         0.04184   -0.02157   -0.02016    0.00045
F9    3    0.525333    0.682745    0.123405    11.00000    0.02954    0.05301 =
         0.03057   -0.00763   -0.00536   -0.00244
F10   3    0.073892    0.227124    0.991747    11.00000    0.03971    0.09355 =
         0.03452   -0.02340   -0.01100    0.01757
F11   3    0.337327    0.095271    0.582412    11.00000    0.05234    0.07591 =
         0.04816   -0.03262   -0.01350   -0.00177
HKLF    4
 
REM  Template texray.inf
REM R1 =  0.0608 for   1837 Fo > 4sig(Fo)  and  0.0728 for all   2259 data
REM    137 parameters refined using      0 restraints
 
END
;
 
#------------------ ATOMIC TYPES, COORDINATES AND THERMAL PARAMETERS --------#
 
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
Xe Xe -0.4205 1.9578 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_symmetry_multiplicity
 _atom_site_calc_flag
 _atom_site_refinement_flags
 _atom_site_disorder_assembly
 _atom_site_disorder_group
Xe1 Xe 0.70293(10) 0.33537(10) 0.22791(10) 0.0332(3) Uani 1 1 d . . .
Xe2 Xe 0.22714(9) 0.17036(9) 0.27850(9) 0.0298(3) Uani 1 1 d . . .
Xe3 Xe 0.20628(10) 0.16346(10) 0.78643(10) 0.0335(3) Uani 1 1 d . . .
Ru1 Ru 0.28576(12) 0.68164(12) 0.27584(12) 0.0274(3) Uani 1 1 d . . .
F1 F 0.4981(10) 0.2428(12) 0.2007(10) 0.060(2) Uani 1 1 d . . .
F2 F 0.8912(12) 0.4212(11) 0.2430(12) 0.062(2) Uani 1 1 d . . .
F3 F -0.0093(9) 0.0932(10) 0.3469(9) 0.0464(19) Uani 1 1 d . . .
F4 F 0.2581(11) 0.8769(9) 0.1260(10) 0.0501(19) Uani 1 1 d . . .
F5 F 0.2198(12) 0.5740(10) 0.1734(10) 0.056(2) Uani 1 1 d . . .
F6 F 0.0502(9) 0.6862(9) 0.4280(9) 0.0425(17) Uani 1 1 d . . .
F7 F 0.3174(10) 0.4850(9) 0.4242(10) 0.051(2) Uani 1 1 d . . .
F8 F 0.3537(10) 0.7926(9) 0.3764(9) 0.0426(17) Uani 1 1 d . . .
F9 F 0.5253(9) 0.6827(9) 0.1234(8) 0.0425(17) Uani 1 1 d . . .
F10 F 0.0739(10) 0.2271(12) 0.9917(9) 0.059(2) Uani 1 1 d . . .
F11 F 0.3373(11) 0.0953(11) 0.5824(10) 0.058(2) Uani 1 1 d . . .
 
loop_
 _atom_site_aniso_label
 _atom_site_aniso_U_11
 _atom_site_aniso_U_22
 _atom_site_aniso_U_33
 _atom_site_aniso_U_23
 _atom_site_aniso_U_13
 _atom_site_aniso_U_12
Xe1 0.0243(5) 0.0400(5) 0.0353(5) -0.0152(4) -0.0115(3) 0.0024(3)
Xe2 0.0215(4) 0.0374(5) 0.0272(5) -0.0103(4) -0.0075(3) -0.0030(3)
Xe3 0.0252(5) 0.0422(5) 0.0290(5) -0.0091(4) -0.0096(3) -0.0037(3)
Ru1 0.0213(5) 0.0313(6) 0.0263(5) -0.0090(4) -0.0074(4) -0.0022(4)
F1 0.023(4) 0.115(8) 0.046(5) -0.030(5) -0.011(3) -0.014(4)
F2 0.052(5) 0.066(6) 0.085(7) -0.032(5) -0.035(5) -0.009(4)
F3 0.024(3) 0.058(5) 0.041(4) -0.003(4) -0.004(3) -0.022(3)
F4 0.050(5) 0.049(5) 0.048(5) -0.010(4) -0.023(4) 0.002(4)
F5 0.059(5) 0.063(5) 0.048(5) -0.025(4) -0.016(4) -0.019(4)
F6 0.018(3) 0.057(5) 0.046(4) -0.019(4) -0.009(3) 0.008(3)
F7 0.037(4) 0.041(4) 0.051(5) -0.004(4) -0.010(3) 0.007(3)
F8 0.040(4) 0.054(5) 0.042(4) -0.022(4) -0.020(3) 0.000(3)
F9 0.030(4) 0.053(5) 0.031(4) -0.008(3) -0.005(3) -0.002(3)
F10 0.040(5) 0.094(7) 0.035(4) -0.023(4) -0.011(3) 0.018(5)
F11 0.052(5) 0.076(6) 0.048(5) -0.033(5) -0.014(4) -0.002(4)
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
Xe1 F2 1.913(8) . ?
Xe1 F1 2.139(7) . ?
Xe1 Xe2 4.1831(11) . ?
Xe1 Xe3 4.4007(11) 2_656 ?
Xe1 Xe3 4.5311(11) 2_666 ?
Xe1 Xe2 4.5827(12) 1_655 ?
Xe1 Xe3 4.8081(14) . ?
Xe1 Xe3 4.9204(13) 1_654 ?
Xe1 Xe2 4.9583(14) 2_665 ?
Xe2 F3 1.919(6) . ?
Xe2 F1 2.152(7) . ?
Xe2 F11 3.169(8) . ?
Xe2 F9 3.190(7) 2_665 ?
Xe2 F3 3.219(7) 2_556 ?
Xe2 F6 3.241(7) 2_566 ?
Xe2 F8 3.268(7) 1_545 ?
Xe2 F10 3.298(8) 1_554 ?
Xe2 F4 3.314(8) 1_545 ?
Xe2 F5 3.324(8) . ?
Xe2 F2 3.378(9) 1_455 ?
Xe2 F7 3.792(8) . ?
Xe3 F10 1.980(7) . ?
Xe3 F11 1.992(7) . ?
Xe3 F8 3.301(7) 2_666 ?
Xe3 F9 3.303(7) 2_666 ?
Xe3 F7 3.335(7) . ?
Xe3 F6 3.373(7) 2_566 ?
Xe3 F4 3.400(8) 1_546 ?
Xe3 F2 3.575(9) 2_666 ?
Xe3 F4 3.623(8) 2_566 ?
Xe3 F10 3.774(10) 2_557 ?
Xe3 F3 3.780(7) 2_556 ?
Xe3 F5 3.910(9) 2_566 ?
Ru1 F4 1.834(8) . ?
Ru1 F5 1.842(7) . ?
Ru1 F6 1.843(6) . ?
Ru1 F7 1.847(7) . ?
Ru1 F8 1.860(7) . ?
Ru1 F9 1.861(7) . ?
Ru1 Xe2 4.2781(12) 1_565 ?
Ru1 Xe3 4.3543(12) 2_666 ?
Ru1 Xe3 4.3599(13) 2_566 ?
Ru1 Xe2 4.7492(15) 2_665 ?
F1 Xe3 4.052(10) 2_656 ?
F2 Xe2 3.378(9) 1_655 ?
F2 Xe3 3.575(9) 2_666 ?
F3 Xe2 3.219(7) 2_556 ?
F3 Xe3 3.780(7) 2_556 ?
F4 Xe2 3.314(8) 1_565 ?
F4 Xe3 3.400(8) 1_564 ?
F4 Xe3 3.623(8) 2_566 ?
F5 Xe3 3.910(9) 2_566 ?
F6 Xe2 3.241(7) 2_566 ?
F6 Xe3 3.373(7) 2_566 ?
F8 Xe2 3.268(7) 1_565 ?
F8 Xe3 3.301(7) 2_666 ?
F9 Xe2 3.190(7) 2_665 ?
F9 Xe3 3.303(7) 2_666 ?
F10 Xe2 3.298(8) 1_556 ?
F10 Xe3 3.774(10) 2_557 ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
F2 Xe1 F1 177.8(4) . . ?
F2 Xe1 Xe2 169.0(3) . . ?
F1 Xe1 Xe2 12.9(2) . . ?
F2 Xe1 Xe3 113.5(3) . 2_656 ?
F1 Xe1 Xe3 66.5(3) . 2_656 ?
Xe2 Xe1 Xe3 73.24(2) . 2_656 ?
F2 Xe1 Xe3 48.9(3) . 2_666 ?
F1 Xe1 Xe3 131.0(3) . 2_666 ?
Xe2 Xe1 Xe3 124.91(3) . 2_666 ?
Xe3 Xe1 Xe3 161.83(3) 2_656 2_666 ?
F2 Xe1 Xe2 40.9(3) . 1_655 ?
F1 Xe1 Xe2 139.1(3) . 1_655 ?
Xe2 Xe1 Xe2 143.94(3) . 1_655 ?
Xe3 Xe1 Xe2 72.60(2) 2_656 1_655 ?
Xe3 Xe1 Xe2 89.78(2) 2_666 1_655 ?
F2 Xe1 Xe3 108.5(3) . . ?
F1 Xe1 Xe3 73.6(2) . . ?
Xe2 Xe1 Xe3 61.490(19) . . ?
Xe3 Xe1 Xe3 93.16(3) 2_656 . ?
Xe3 Xe1 Xe3 96.98(3) 2_666 . ?
Xe2 Xe1 Xe3 109.37(2) 1_655 . ?
F2 Xe1 Xe3 83.2(3) . 1_654 ?
F1 Xe1 Xe3 95.2(2) . 1_654 ?
Xe2 Xe1 Xe3 107.74(2) . 1_654 ?
Xe3 Xe1 Xe3 53.78(3) 2_656 1_654 ?
Xe3 Xe1 Xe3 113.38(3) 2_666 1_654 ?
Xe2 Xe1 Xe3 58.887(16) 1_655 1_654 ?
Xe3 Xe1 Xe3 146.33(3) . 1_654 ?
F2 Xe1 Xe2 88.8(3) . 2_665 ?
F1 Xe1 Xe2 89.6(2) . 2_665 ?
Xe2 Xe1 Xe2 94.48(3) . 2_665 ?
Xe3 Xe1 Xe2 123.93(2) 2_656 2_665 ?
Xe3 Xe1 Xe2 58.904(17) 2_666 2_665 ?
Xe2 Xe1 Xe2 114.07(2) 1_655 2_665 ?
Xe3 Xe1 Xe2 129.08(2) . 2_665 ?
Xe3 Xe1 Xe2 81.25(2) 1_654 2_665 ?
F3 Xe2 F1 176.6(4) . . ?
F3 Xe2 F11 114.9(3) . . ?
F1 Xe2 F11 65.0(3) . . ?
F3 Xe2 F9 116.7(2) . 2_665 ?
F1 Xe2 F9 63.1(2) . 2_665 ?
F11 Xe2 F9 127.9(2) . 2_665 ?
F3 Xe2 F3 59.1(3) . 2_556 ?
F1 Xe2 F3 119.8(3) . 2_556 ?
F11 Xe2 F3 57.8(2) . 2_556 ?
F9 Xe2 F3 159.9(2) 2_665 2_556 ?
F3 Xe2 F6 72.7(3) . 2_566 ?
F1 Xe2 F6 110.0(3) . 2_566 ?
F11 Xe2 F6 67.16(19) . 2_566 ?
F9 Xe2 F6 136.14(19) 2_665 2_566 ?
F3 Xe2 F6 63.4(2) 2_556 2_566 ?
F3 Xe2 F8 89.4(3) . 1_545 ?
F1 Xe2 F8 87.3(3) . 1_545 ?
F11 Xe2 F8 71.85(19) . 1_545 ?
F9 Xe2 F8 102.11(19) 2_665 1_545 ?
F3 Xe2 F8 59.59(19) 2_556 1_545 ?
F6 Xe2 F8 121.32(18) 2_566 1_545 ?
F3 Xe2 F10 59.2(3) . 1_554 ?
F1 Xe2 F10 120.8(3) . 1_554 ?
F11 Xe2 F10 174.1(2) . 1_554 ?
F9 Xe2 F10 57.83(19) 2_665 1_554 ?
F3 Xe2 F10 116.5(2) 2_556 1_554 ?
F6 Xe2 F10 109.84(18) 2_566 1_554 ?
F8 Xe2 F10 106.7(2) 1_545 1_554 ?
F3 Xe2 F4 70.7(3) . 1_545 ?
F1 Xe2 F4 106.2(3) . 1_545 ?
F11 Xe2 F4 118.6(2) . 1_545 ?
F9 Xe2 F4 73.79(19) 2_665 1_545 ?
F3 Xe2 F4 86.7(2) 2_556 1_545 ?
F6 Xe2 F4 141.18(19) 2_566 1_545 ?
F8 Xe2 F4 46.77(17) 1_545 1_545 ?
F10 Xe2 F4 60.2(2) 1_554 1_545 ?
F3 Xe2 F5 107.9(3) . . ?
F1 Xe2 F5 75.4(3) . . ?
F11 Xe2 F5 96.7(2) . . ?
F9 Xe2 F5 73.82(19) 2_665 . ?
F3 Xe2 F5 126.2(2) 2_556 . ?
F6 Xe2 F5 62.96(19) 2_566 . ?
F8 Xe2 F5 162.3(2) 1_545 . ?
F10 Xe2 F5 86.0(2) 1_554 . ?
F4 Xe2 F5 142.16(19) 1_545 . ?
F3 Xe2 F2 56.7(3) . 1_455 ?
F1 Xe2 F2 126.5(3) . 1_455 ?
F11 Xe2 F2 122.2(2) . 1_455 ?
F9 Xe2 F2 92.1(2) 2_665 1_455 ?
F3 Xe2 F2 99.6(2) 2_556 1_455 ?
F6 Xe2 F2 55.7(2) 2_566 1_455 ?
F8 Xe2 F2 145.97(19) 1_545 1_455 ?
F10 Xe2 F2 55.8(2) 1_554 1_455 ?
F4 Xe2 F2 110.95(19) 1_545 1_455 ?
F5 Xe2 F2 51.7(2) . 1_455 ?
F3 Xe2 F7 123.4(3) . . ?
F1 Xe2 F7 59.6(3) . . ?
F11 Xe2 F7 54.08(19) . . ?
F9 Xe2 F7 100.42(18) 2_665 . ?
F3 Xe2 F7 97.30(18) 2_556 . ?
F6 Xe2 F7 51.39(17) 2_566 . ?
F8 Xe2 F7 124.10(16) 1_545 . ?
F10 Xe2 F7 128.5(2) 1_554 . ?
F4 Xe2 F7 165.33(18) 1_545 . ?
F5 Xe2 F7 42.65(17) . . ?
F2 Xe2 F7 82.38(18) 1_455 . ?
F10 Xe3 F11 178.9(4) . . ?
F10 Xe3 F8 114.0(3) . 2_666 ?
F11 Xe3 F8 66.6(3) . 2_666 ?
F10 Xe3 F9 67.6(3) . 2_666 ?
F11 Xe3 F9 113.0(3) . 2_666 ?
F8 Xe3 F9 46.58(16) 2_666 2_666 ?
F10 Xe3 F7 112.0(3) . . ?
F11 Xe3 F7 69.0(3) . . ?
F8 Xe3 F7 74.87(19) 2_666 . ?
F9 Xe3 F7 88.36(19) 2_666 . ?
F10 Xe3 F6 102.0(3) . 2_566 ?
F11 Xe3 F6 78.1(3) . 2_566 ?
F8 Xe3 F6 126.36(17) 2_666 2_566 ?
F9 Xe3 F6 136.16(18) 2_666 2_566 ?
F7 Xe3 F6 54.85(19) . 2_566 ?
F10 Xe3 F4 70.6(3) . 1_546 ?
F11 Xe3 F4 108.7(3) . 1_546 ?
F8 Xe3 F4 83.28(19) 2_666 1_546 ?
F9 Xe3 F4 71.26(18) 2_666 1_546 ?
F7 Xe3 F4 157.1(2) . 1_546 ?
F6 Xe3 F4 148.09(19) 2_566 1_546 ?
F10 Xe3 F2 57.7(3) . 2_666 ?
F11 Xe3 F2 123.2(3) . 2_666 ?
F8 Xe3 F2 96.40(19) 2_666 2_666 ?
F9 Xe3 F2 68.51(18) 2_666 2_666 ?
F7 Xe3 F2 54.3(2) . 2_666 ?
F6 Xe3 F2 70.37(18) 2_566 2_666 ?
F4 Xe3 F2 123.05(19) 1_546 2_666 ?
F10 Xe3 F4 77.2(3) . 2_566 ?
F11 Xe3 F4 102.3(3) . 2_566 ?
F8 Xe3 F4 167.83(17) 2_666 2_566 ?
F9 Xe3 F4 143.65(17) 2_666 2_566 ?
F7 Xe3 F4 96.87(18) . 2_566 ?
F6 Xe3 F4 43.19(17) 2_566 2_566 ?
F4 Xe3 F4 105.78(16) 1_546 2_566 ?
F2 Xe3 F4 85.54(18) 2_666 2_566 ?
F10 Xe3 F10 90.7(3) . 2_557 ?
F11 Xe3 F10 88.3(3) . 2_557 ?
F8 Xe3 F10 128.28(17) 2_666 2_557 ?
F9 Xe3 F10 133.13(17) 2_666 2_557 ?
F7 Xe3 F10 138.42(19) . 2_557 ?
F6 Xe3 F10 87.43(17) 2_566 2_557 ?
F4 Xe3 F10 62.27(18) 1_546 2_557 ?
F2 Xe3 F10 134.17(19) 2_666 2_557 ?
F4 Xe3 F10 53.23(17) 2_566 2_557 ?
F10 Xe3 F3 124.7(3) . 2_556 ?
F11 Xe3 F3 54.5(3) . 2_556 ?
F8 Xe3 F3 119.23(16) 2_666 2_556 ?
F9 Xe3 F3 163.59(17) 2_666 2_556 ?
F7 Xe3 F3 95.54(18) . 2_556 ?
F6 Xe3 F3 56.34(18) 2_566 2_556 ?
F4 Xe3 F3 101.28(18) 1_546 2_556 ?
F2 Xe3 F3 126.28(18) 2_666 2_556 ?
F4 Xe3 F3 51.74(17) 2_566 2_556 ?
F10 Xe3 F3 44.22(15) 2_557 2_556 ?
F10 Xe3 F5 60.6(3) . 2_566 ?
F11 Xe3 F5 119.6(3) . 2_566 ?
F8 Xe3 F5 140.35(18) 2_666 2_566 ?
F9 Xe3 F5 110.36(17) 2_666 2_566 ?
F7 Xe3 F5 72.48(17) . 2_566 ?
F6 Xe3 F5 41.60(16) 2_566 2_566 ?
F4 Xe3 F5 123.86(18) 1_546 2_566 ?
F2 Xe3 F5 45.67(18) 2_666 2_566 ?
F4 Xe3 F5 39.88(17) 2_566 2_566 ?
F10 Xe3 F5 91.30(17) 2_557 2_566 ?
F3 Xe3 F5 85.98(16) 2_556 2_566 ?
F4 Ru1 F5 89.3(4) . . ?
F4 Ru1 F6 89.4(4) . . ?
F5 Ru1 F6 91.2(4) . . ?
F4 Ru1 F7 179.1(4) . . ?
F5 Ru1 F7 90.7(4) . . ?
F6 Ru1 F7 91.6(3) . . ?
F4 Ru1 F8 90.0(3) . . ?
F5 Ru1 F8 179.2(4) . . ?
F6 Ru1 F8 89.1(3) . . ?
F7 Ru1 F8 90.0(4) . . ?
F4 Ru1 F9 89.9(3) . . ?
F5 Ru1 F9 90.5(4) . . ?
F6 Ru1 F9 178.1(3) . . ?
F7 Ru1 F9 89.1(3) . . ?
F8 Ru1 F9 89.1(3) . . ?
F4 Ru1 Xe2 47.1(2) . 1_565 ?
F5 Ru1 Xe2 133.6(3) . 1_565 ?
F6 Ru1 Xe2 75.9(2) . 1_565 ?
F7 Ru1 Xe2 133.2(3) . 1_565 ?
F8 Ru1 Xe2 45.9(2) . 1_565 ?
F9 Ru1 Xe2 102.4(2) . 1_565 ?
F4 Ru1 Xe3 93.6(3) . 2_666 ?
F5 Ru1 Xe3 135.0(3) . 2_666 ?
F6 Ru1 Xe3 133.6(2) . 2_666 ?
F7 Ru1 Xe3 85.8(3) . 2_666 ?
F8 Ru1 Xe3 44.6(2) . 2_666 ?
F9 Ru1 Xe3 44.7(2) . 2_666 ?
Xe2 Ru1 Xe3 72.80(2) 1_565 2_666 ?
F4 Ru1 Xe3 54.7(3) . 2_566 ?
F5 Ru1 Xe3 63.7(3) . 2_566 ?
F6 Ru1 Xe3 46.7(2) . 2_566 ?
F7 Ru1 Xe3 126.1(3) . 2_566 ?
F8 Ru1 Xe3 116.2(2) . 2_566 ?
F9 Ru1 Xe3 133.8(2) . 2_566 ?
Xe2 Ru1 Xe3 76.04(3) 1_565 2_566 ?
Xe3 Ru1 Xe3 146.12(3) 2_666 2_566 ?
F4 Ru1 Xe2 126.6(2) . . ?
F5 Ru1 Xe2 37.4(3) . . ?
F6 Ru1 Xe2 94.4(2) . . ?
F7 Ru1 Xe2 53.4(3) . . ?
F8 Ru1 Xe2 143.2(2) . . ?
F9 Ru1 Xe2 87.4(2) . . ?
Xe2 Ru1 Xe2 167.70(3) 1_565 . ?
Xe3 Ru1 Xe2 119.46(3) 2_666 . ?
Xe3 Ru1 Xe2 91.82(3) 2_566 . ?
F4 Ru1 Xe2 66.5(3) . 2_665 ?
F5 Ru1 Xe2 78.8(3) . 2_665 ?
F6 Ru1 Xe2 153.8(2) . 2_665 ?
F7 Ru1 Xe2 112.6(2) . 2_665 ?
F8 Ru1 Xe2 100.6(2) . 2_665 ?
F9 Ru1 Xe2 26.3(2) . 2_665 ?
Xe2 Ru1 Xe2 93.35(3) 1_565 2_665 ?
Xe3 Ru1 Xe2 61.70(2) 2_666 2_665 ?
Xe3 Ru1 Xe2 107.84(3) 2_566 2_665 ?
Xe2 Ru1 Xe2 92.20(3) . 2_665 ?
Xe1 F1 Xe2 154.3(4) . . ?
Xe1 F1 Xe3 84.6(2) . 2_656 ?
Xe2 F1 Xe3 107.3(3) . 2_656 ?
Xe1 F2 Xe2 117.3(4) . 1_655 ?
Xe1 F2 Xe3 107.4(3) . 2_666 ?
Xe2 F2 Xe3 135.3(2) 1_655 2_666 ?
Xe2 F3 Xe2 120.9(3) . 2_556 ?
Xe2 F3 Xe3 135.4(3) . 2_556 ?
Xe2 F3 Xe3 82.36(15) 2_556 2_556 ?
Ru1 F4 Xe2 109.0(3) . 1_565 ?
Ru1 F4 Xe3 162.6(4) . 1_564 ?
Xe2 F4 Xe3 88.39(18) 1_565 1_564 ?
Ru1 F4 Xe3 100.9(3) . 2_566 ?
Xe2 F4 Xe3 100.1(2) 1_565 2_566 ?
Xe3 F4 Xe3 74.22(15) 1_564 2_566 ?
Ru1 F5 Xe2 122.9(4) . . ?
Ru1 F5 Xe3 91.3(3) . 2_566 ?
Xe2 F5 Xe3 125.3(2) . 2_566 ?
Ru1 F6 Xe2 145.8(3) . 2_566 ?
Ru1 F6 Xe3 109.9(3) . 2_566 ?
Xe2 F6 Xe3 88.79(16) 2_566 2_566 ?
Ru1 F7 Xe3 156.8(3) . . ?
Ru1 F7 Xe2 103.6(3) . . ?
Xe3 F7 Xe2 80.71(16) . . ?
Ru1 F8 Xe2 110.0(3) . 1_565 ?
Ru1 F8 Xe3 112.0(3) . 2_666 ?
Xe2 F8 Xe3 102.5(2) 1_565 2_666 ?
Ru1 F9 Xe2 138.7(3) . 2_665 ?
Ru1 F9 Xe3 111.9(3) . 2_666 ?
Xe2 F9 Xe3 92.24(18) 2_665 2_666 ?
Xe3 F10 Xe2 123.0(3) . 1_556 ?
Xe3 F10 Xe3 89.3(3) . 2_557 ?
Xe2 F10 Xe3 97.4(2) 1_556 2_557 ?
Xe3 F11 Xe2 125.9(4) . . ?

# start Validation Reply Form
_vrf_PLAT029_I
;
PROBLEM: _diffrn_measured_fraction_theta_full Low .......      0.918      
RESPONSE: The data were obtained from twinned crystal. Excluding of overlapped 
reflections from the final refinement has led to smaller completeness. 
;
# end Validation Reply Form