data_ham_vof_2 _audit_creation_date 2015-03-02 _audit_creation_method ; Olex2 1.2 (compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998) ; _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_requested_journal 'Acta Chimica Slovenica' _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Palatinus, L. & Chapuis, G. (2007). J. Appl. Cryst., 40, 786-790; Palatinus, L. & van der Lee, A. (2008). J. Appl. Cryst. 41, 975-984; Palatinus, L., Prathapa, S. J. & van Smaalen, S. (2012). J. Appl. Cryst. 45, 575-580. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'F4 O V, H4 N O' _chemical_formula_sum 'F4 H4 N O2 V' _chemical_formula_weight 176.98 _chemical_melting_point ? _chemical_oxdiff_formula 'V F4 O2 N H4 ' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'V' 'V' 0.3005 0.5294 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 7.2349(2) _cell_length_b 5.03513(16) _cell_length_c 12.8322(4) _cell_angle_alpha 90 _cell_angle_beta 94.843(3) _cell_angle_gamma 90 _cell_volume 465.79(3) _cell_formula_units_Z 4 _cell_measurement_reflns_used 2346 _cell_measurement_temperature 150.00(10) _cell_measurement_theta_max 29.3140 _cell_measurement_theta_min 4.1320 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 2.141 _exptl_absorpt_correction_T_max 0.957 _exptl_absorpt_correction_T_min 0.791 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET) (compiled Aug 2 2013,16:46:58) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 2.524 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description '' _exptl_crystal_F_000 344 _exptl_crystal_size_max 0.1621 _exptl_crystal_size_mid 0.0768 _exptl_crystal_size_min 0.0205 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0180 _diffrn_reflns_av_unetI/netI 0.0218 _diffrn_reflns_Laue_measured_fraction_full 0.988 _diffrn_reflns_Laue_measured_fraction_max 0.873 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 5 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 3232 _diffrn_reflns_point_group_measured_fraction_full 0.988 _diffrn_reflns_point_group_measured_fraction_max 0.873 _diffrn_reflns_theta_full 25.000 _diffrn_reflns_theta_max 29.655 _diffrn_reflns_theta_min 3.359 _diffrn_ambient_temperature 150.00(10) _diffrn_detector_area_resol_mean 10.6426 _diffrn_measured_fraction_theta_full 0.988 _diffrn_measured_fraction_theta_max 0.873 _diffrn_measurement_details ; #__ type_ start__ end____ width___ exp.time_ 1 omega -56.00 36.00 1.0000 11.8150 omega____ theta____ kappa____ phi______ frames - 11.3380 -57.0000 -180.0000 92 #__ type_ start__ end____ width___ exp.time_ 2 omega -15.00 75.00 1.0000 11.8150 omega____ theta____ kappa____ phi______ frames - 11.3380 77.0000 90.0000 90 #__ type_ start__ end____ width___ exp.time_ 3 omega -11.00 82.00 1.0000 11.8150 omega____ theta____ kappa____ phi______ frames - 11.3380 57.0000 -30.0000 93 ; _diffrn_measurement_device_type 'New Gemini, Dual, Cu at zero, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_UB_11 0.0195484000 _diffrn_orient_matrix_UB_12 0.0242535000 _diffrn_orient_matrix_UB_13 0.0542699000 _diffrn_orient_matrix_UB_21 0.0542267000 _diffrn_orient_matrix_UB_22 -0.1173754000 _diffrn_orient_matrix_UB_23 0.0045032000 _diffrn_orient_matrix_UB_31 0.0797427000 _diffrn_orient_matrix_UB_32 0.0739756000 _diffrn_orient_matrix_UB_33 -0.0106004000 _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'Enhance (Mo) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 1066 _reflns_number_total 1139 _reflns_odcompleteness_completeness 99.62 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET) (compiled Aug 2 2013,16:46:58) ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET) (compiled Aug 2 2013,16:46:58) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET) (compiled Aug 2 2013,16:46:58) ; _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2008)' _computing_structure_solution ; Superflip (Palatinus & Chapuis, 2007;Palatinus & van der Lee, 2008; Palatinus et al., 2012) ; _refine_diff_density_max 0.273 _refine_diff_density_min -0.327 _refine_diff_density_rms 0.062 _refine_ls_extinction_coef 0.0111(17) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick 2014' _refine_ls_goodness_of_fit_ref 1.063 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 90 _refine_ls_number_reflns 1139 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0197 _refine_ls_R_factor_gt 0.0180 _refine_ls_restrained_S_all 1.066 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0235P)^2^+0.0585P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0436 _refine_ls_wR_factor_ref 0.0444 _refine_special_details ? _olex2_refinement_description ; 1. Restrained distances H4-N1 0.91 with sigma of 0.02 ; _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary iterative _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group V1 V 0.25400(3) 0.43049(4) 0.12649(2) 0.00800(9) Uani 1 1 d . . . . . F1 F 0.01334(10) 0.51980(16) 0.13436(6) 0.01335(17) Uani 1 1 d . . . . . F2 F 0.17738(11) 0.12187(15) 0.06474(6) 0.01513(18) Uani 1 1 d . . . . . F3 F 0.48141(10) 0.28269(15) 0.16351(6) 0.01370(17) Uani 1 1 d . . . . . F4 F 0.31664(10) 0.68268(15) 0.22869(6) 0.01209(17) Uani 1 1 d . . . . . O1 O 0.30102(13) 0.59185(19) 0.02779(8) 0.0150(2) Uani 1 1 d . . . . . O2 O 0.82430(13) 0.3504(2) 0.32838(8) 0.0165(2) Uani 1 1 d . . . . . N1 N 0.66801(15) 0.4968(2) 0.35385(10) 0.0121(2) Uani 1 1 d D . . . . H1 H 0.901(3) 0.474(5) 0.3291(18) 0.040(6) Uiso 1 1 d . . . . . H2 H 0.569(3) 0.394(5) 0.3324(19) 0.047(6) Uiso 1 1 d . . . . . H3 H 0.674(2) 0.525(4) 0.4211(17) 0.027(5) Uiso 1 1 d . . . . . H4 H 0.668(3) 0.648(4) 0.323(2) 0.065(8) Uiso 1 1 d D . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 V1 0.00892(13) 0.00750(13) 0.00745(14) -0.00089(7) 0.00000(8) 0.00116(7) F1 0.0102(4) 0.0140(4) 0.0157(4) -0.0006(3) -0.0004(3) 0.0027(3) F2 0.0216(4) 0.0114(4) 0.0122(4) -0.0036(3) 0.0009(3) -0.0016(3) F3 0.0109(4) 0.0143(4) 0.0161(4) 0.0023(3) 0.0020(3) 0.0035(3) F4 0.0135(4) 0.0112(4) 0.0116(4) -0.0030(3) 0.0012(3) -0.0015(3) O1 0.0188(5) 0.0145(5) 0.0119(5) 0.0016(4) 0.0024(3) 0.0016(4) O2 0.0113(5) 0.0139(5) 0.0249(6) -0.0034(4) 0.0057(4) -0.0005(4) N1 0.0130(6) 0.0112(6) 0.0123(6) -0.0014(5) 0.0019(4) 0.0013(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag V1 F1 1.8094(7) . ? V1 F2 1.8100(8) . ? V1 F3 1.8315(7) . ? V1 F4 1.8540(8) . ? V1 F4 2.3306(7) 2_545 ? V1 O1 1.5662(10) . ? F4 V1 2.3306(7) 2 ? O2 N1 1.4111(14) . ? O2 H1 0.83(2) . ? N1 H2 0.90(2) . ? N1 H3 0.87(2) . ? N1 H4 0.857(17) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F1 V1 F2 88.69(4) . . ? F1 V1 F3 159.09(4) . . ? F1 V1 F4 79.15(3) . 2_545 ? F1 V1 F4 88.24(3) . . ? F2 V1 F3 89.99(4) . . ? F2 V1 F4 79.03(3) . 2_545 ? F2 V1 F4 160.96(4) . . ? F3 V1 F4 80.12(3) . 2_545 ? F3 V1 F4 86.23(3) . . ? F4 V1 F4 81.932(14) . 2_545 ? O1 V1 F1 101.07(4) . . ? O1 V1 F2 99.83(5) . . ? O1 V1 F3 99.72(4) . . ? O1 V1 F4 178.84(4) . 2_545 ? O1 V1 F4 99.20(4) . . ? V1 F4 V1 150.89(4) . 2 ? N1 O2 H1 98.7(16) . . ? O2 N1 H2 105.0(14) . . ? O2 N1 H3 109.7(12) . . ? O2 N1 H4 108.9(17) . . ? H2 N1 H3 111.6(19) . . ? H2 N1 H4 113(2) . . ? H3 N1 H4 108(2) . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O2 H1 F3 0.83(2) 1.77(2) 2.5884(13) 167(2) 2_655 N1 H2 F1 0.90(2) 2.03(2) 2.7471(15) 135(2) 2_545 N1 H2 F3 0.90(2) 2.28(2) 2.8973(15) 125.5(19) . N1 H3 F2 0.87(2) 1.98(2) 2.7665(15) 148.7(18) 4_666 N1 H3 O1 0.87(2) 2.50(2) 3.1360(16) 130.9(16) 4_676 N1 H4 F1 0.857(17) 2.38(2) 2.9516(14) 125(2) 2 N1 H4 O2 0.857(17) 2.20(2) 2.9433(16) 145(3) 2_655 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag F1 V1 F4 V1 28.44(8) . . . 2 ? F2 V1 F4 V1 -52.40(15) . . . 2 ? F3 V1 F4 V1 -131.38(8) . . . 2 ? F4 V1 F4 V1 -50.84(8) 2_545 . . 2 ? O1 V1 F4 V1 129.37(9) . . . 2 ? _shelx_SHELXL_version_number '2014/7' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -10 0 7 0.0073 -10.0000 0.0000 7.0000 0.1844 -0.5107 -0.8716 -5 1 16 0.0227 -5.0000 1.0000 16.0000 0.7948 -0.3165 -0.4943 -8 -4 6 0.0405 -8.0000 -4.0000 6.0000 0.0722 0.0627 -0.9974 7 -1 11 0.0455 7.0000 -1.0000 11.0000 0.7096 0.5465 0.3676 2 7 -1 0.0708 2.0000 7.0000 -1.0000 0.1546 -0.7177 0.6879 -1 -7 1 0.0810 -1.0000 -7.0000 1.0000 -0.1351 0.7719 -0.6082 4 -5 -10 0.0648 4.0000 -5.0000 -10.0000 -0.5858 0.7588 0.0551 3 6 6 0.0644 3.0000 6.0000 6.0000 0.5298 -0.5146 0.6195 6 4 -11 0.0475 6.0000 4.0000 -11.0000 -0.3827 -0.1937 0.8910 10 1 1 0.0246 10.0000 1.0000 1.0000 0.2740 0.4294 0.8608 -1 6 -8 0.0700 -1.0000 6.0000 -8.0000 -0.3082 -0.7945 0.4489 -2 1 -17 0.0390 -2.0000 1.0000 -17.0000 -0.9374 -0.3024 0.0947 -1 -4 -14 0.0476 -1.0000 -4.0000 -14.0000 -0.8763 0.3522 -0.2272 1 0 -18 0.0276 1.0000 -0.0000 -18.0000 -0.9573 -0.0268 0.2705 -4 -2 -15 0.0364 -4.0000 -2.0000 -15.0000 -0.9407 -0.0497 -0.3079 10 0 -7 0.0133 10.0000 -0.0000 -7.0000 -0.1844 0.5107 0.8716 _iucr_refine_instructions_details ; ham_vof_2.res created by SHELXL-2014/7 TITL HAM_VOF_2 in P2(1)/n CELL 0.71073 7.234931 5.035133 12.832197 90 94.8432 90 ZERR 4 0.000226 0.000157 0.000422 0 0.0026 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC F H N O V UNIT 16 16 4 8 4 EQIV $1 1.5-X,0.5+Y,0.5-Z EQIV $2 0.5-X,-0.5+Y,0.5-Z EQIV $3 0.5+X,0.5-Y,0.5+Z EQIV $4 0.5+X,1.5-Y,0.5+Z EQIV $5 0.5-X,0.5+Y,0.5-Z DFIX 0.91 H4 N1 L.S. 20 PLAN 10 TEMP -123.15 HTAB O2 F3_$1 HTAB N1 F1_$2 HTAB N1 F3 HTAB N1 F2_$3 HTAB N1 O1_$4 HTAB N1 F1_$5 HTAB N1 O2_$1 BOND $H CONF fmap 2 53 acta 50 more -3 OMIT -2 1 3 OMIT 2 0 4 OMIT 1 2 0 OMIT 2 1 2 OMIT -2 1 5 OMIT 1 0 3 OMIT 0 0 4 OMIT -2 2 3 REM REM REM WGHT 0.023500 0.058500 EXTI 0.011149 FVAR 7.83134 V1 5 0.254004 0.430489 0.126494 11.00000 0.00892 0.00750 = 0.00745 -0.00089 0.00000 0.00116 F1 1 0.013336 0.519803 0.134361 11.00000 0.01015 0.01399 = 0.01565 -0.00061 -0.00043 0.00268 F2 1 0.177383 0.121865 0.064735 11.00000 0.02162 0.01145 = 0.01224 -0.00365 0.00094 -0.00164 F3 1 0.481408 0.282691 0.163508 11.00000 0.01088 0.01427 = 0.01610 0.00226 0.00196 0.00347 F4 1 0.316643 0.682679 0.228692 11.00000 0.01347 0.01122 = 0.01161 -0.00300 0.00124 -0.00149 O1 4 0.301019 0.591850 0.027786 11.00000 0.01880 0.01446 = 0.01188 0.00164 0.00238 0.00157 O2 4 0.824300 0.350399 0.328384 11.00000 0.01134 0.01389 = 0.02487 -0.00339 0.00569 -0.00048 N1 3 0.668010 0.496816 0.353852 11.00000 0.01295 0.01118 = 0.01233 -0.00140 0.00187 0.00134 H1 2 0.900535 0.473684 0.329061 11.00000 0.04024 H2 2 0.569421 0.394372 0.332400 11.00000 0.04707 H3 2 0.674487 0.524860 0.421102 11.00000 0.02710 H4 2 0.668283 0.647894 0.323098 11.00000 0.06514 HKLF 4 REM HAM_VOF_2 in P2(1)/n REM R1 = 0.0180 for 1066 Fo > 4sig(Fo) and 0.0197 for all 1139 data REM 90 parameters refined using 1 restraints END WGHT 0.0235 0.0585 REM Highest difference peak 0.273, deepest hole -0.327, 1-sigma level 0.062 Q1 1 0.2889 0.4729 0.0588 11.00000 0.05 0.27 Q2 1 0.1846 0.2792 0.0650 11.00000 0.05 0.25 Q3 1 0.1067 0.4435 0.1293 11.00000 0.05 0.22 Q4 1 0.3594 0.4110 0.1412 11.00000 0.05 0.21 Q5 1 0.4422 0.2344 0.1820 11.00000 0.05 0.21 Q6 1 0.3834 0.2595 0.1561 11.00000 0.05 0.20 Q7 1 0.3668 0.0089 0.0558 11.00000 0.05 0.19 Q8 1 0.2563 0.1957 0.0405 11.00000 0.05 0.18 Q9 1 0.2332 0.6401 0.0620 11.00000 0.05 0.18 Q10 1 0.4374 0.3023 0.1208 11.00000 0.05 0.17 REM The information below was added by Olex2. REM REM R1 = 0.0180 for 1066 Fo > 4sig(Fo) and 0.0197 for all 3494 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.27, deepest hole -0.33 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0197 REM R1_gt = 0.0180 REM wR_ref = 0.0444 REM GOOF = 1.063 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 3494 REM Reflections_gt = 1066 REM Parameters = n/a REM Hole = -0.33 REM Peak = 0.27 REM Flack = n/a ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_scale_group_code 0 0 -3 20.0058 105.377 1 0 0 -4 540576 8168.99 1 0 0 -5 160.106 133.219 1 0 0 -6 99072.4 2115.16 1 0 0 -7 51.0842 163.29 1 0 0 -8 140093 2942.99 1 0 0 9 -110.506 158.837 3 0 0 -9 364.075 224.643 1 0 0 -10 115960 2073.81 2 0 0 -10 116808 2766.25 1 0 0 -11 -286.309 213.777 1 0 0 -11 161.114 91.5435 2 0 0 -12 57973 1925.83 1 0 0 -12 57352.9 1253.92 2 0 0 -13 -139.519 226.693 1 0 0 -14 9811.65 827.405 1 0 0 -15 682.599 296.815 1 0 0 -16 28190.9 1505.5 1 0 -1 0 570.751 115.446 3 0 1 -1 163547 2613.11 1 0 -1 -1 169030 2608.87 3 0 -1 -2 101487 1755.21 3 0 -1 2 102588 1562.9 2 0 1 -2 100266 1761.41 1 0 1 -3 67360 1359.01 1 0 -1 -3 69967.4 1352.1 3 0 1 -4 21214.7 676.643 1 0 -1 -4 23879.2 715.129 3 0 -1 -5 58436.7 1344.05 3 0 1 -5 54102.7 1319.75 1 0 1 -6 99946.8 2101.98 1 0 -1 -6 99816.6 2090.19 3 0 -1 -7 177422 3363.54 1 0 1 -7 172785 3331 1 0 -1 -8 11783.7 677.902 1 0 1 -8 11796.8 666.087 1 0 -1 9 177071 3606.59 1 0 1 -9 166562 3531.37 1 0 1 9 177004 3510.33 3 0 -1 -9 174862 3587.72 1 0 -1 -10 5490.57 545.195 1 0 1 -10 4902 502.559 1 0 -1 -10 5543.41 374.56 2 0 -1 -11 100794 2111.86 2 0 1 -11 96363.5 2591.55 1 0 -1 -12 2174.08 257.938 2 0 -1 -12 1932.93 381.244 1 0 1 -12 1890.43 392.717 1 0 -1 -13 44427.1 1754.06 1 0 1 -13 44153.2 1719.48 1 0 -1 -13 40940.8 1206.59 2 0 -1 -14 26217.4 1375.49 1 0 1 -14 23560.6 1284.55 1 0 1 -15 12902.6 985.295 1 0 -1 -15 12011.9 968.841 1 0 -2 0 158725 2719.68 3 0 -2 1 40649.2 911.647 2 0 -2 -1 42154.3 1008.07 3 0 -2 1 41775.7 1000.05 3 0 -2 2 55628.2 1110.06 2 0 -2 -2 59352.5 1283.92 3 0 2 -2 56401.9 1273.8 1 0 -2 3 10624.7 354.744 2 0 2 -3 11481.6 498.679 1 0 -2 -3 11063.5 494.242 3 0 2 -4 252881 4293.97 1 0 -2 -4 264353 4328.06 3 0 -2 4 258493 3896.93 2 0 2 -5 470936 7330.89 1 0 -2 -5 480857 7351.74 3 0 -2 5 459822 6756.59 2 0 2 -6 2047.45 272.424 1 0 -2 -6 2072.29 264.494 3 0 -2 -7 15232.3 735.827 3 0 -2 7 15390.6 758.821 1 0 2 -7 14918.9 724.713 1 0 2 -8 135739 2904.58 1 0 -2 8 140348 3013.02 1 0 -2 -8 135771 2930.57 3 0 2 -9 14248.1 792.1 1 0 -2 -9 13078.6 759.76 3 0 -2 -10 2235.39 367.844 1 0 2 -10 2537.4 380.376 1 0 -2 -10 2559.35 366.472 3 0 2 -11 10298.6 750.266 1 0 -2 -11 10122 766.438 1 0 -2 -12 81046.2 2458.34 1 0 2 -12 80804.1 2399.1 1 0 -2 -13 4309.72 556.275 1 0 2 -13 3940.69 524.915 1 0 -2 -14 7534.34 753.797 1 0 2 -14 7761.79 755.476 1 0 2 -15 17145 1160.06 1 0 -2 -15 17850.7 1220.72 1 0 -3 0 -17.0771 112.935 2 0 -3 0 -49.6118 113.033 3 0 -3 1 27923.6 926.337 3 0 -3 -1 29224.5 906.635 2 0 -3 -1 29109.5 936.983 3 0 -3 1 28512.3 840.004 2 0 -3 2 65092.4 1426.09 2 0 -3 -2 68134.5 1570.95 2 0 -3 2 67395.3 1606.89 3 0 -3 -2 65802.2 1593.79 3 0 -3 3 2655.06 300.46 3 0 -3 3 2499.94 227.535 2 0 -3 -3 2663.53 294.267 3 0 3 4 16429.3 718.925 3 0 -3 4 15850.2 547.667 2 0 -3 4 15998.9 720.714 1 0 3 -4 15791.5 712.915 1 0 -3 -4 16676.5 735.404 3 0 3 -5 36276.4 1186.56 1 0 3 5 39867.7 1216.2 3 0 -3 -5 39295.4 1231.05 3 0 -3 5 39651.3 1255.75 1 0 -3 5 38106.6 902.056 2 0 -3 -6 86215.8 2091.51 3 0 -3 6 87101.2 1577.16 2 0 3 -6 85712.6 2074.06 1 0 3 -7 7465.59 546.405 1 0 -3 -7 6919.42 535.882 3 0 -3 7 7246.9 268.131 2 0 3 -8 32857.9 1239.42 1 0 -3 -8 32744.6 1259.13 3 0 3 -9 905.22 244.163 1 0 -3 -9 1131.06 276.327 3 0 -3 -10 49385.1 1715.77 3 0 3 -10 49553.2 1701.79 1 0 -3 -11 -111.51 192.634 3 0 3 -11 100.51 185.621 1 0 -3 -12 12873.2 944.736 1 0 3 -12 12806.7 898.076 1 0 -3 -12 12561.6 891.893 3 0 -3 -13 13259.2 1001.73 1 0 3 -13 14025.6 986.607 1 0 3 -14 67281.9 2386.34 1 0 -3 -14 70406.1 2506.8 1 0 -4 0 5338.24 413.375 2 0 -4 0 5339.29 446.893 3 0 -4 1 38519.2 1168.64 2 0 -4 1 38476.1 1261.19 3 0 -4 -1 40078.1 1286.68 3 0 -4 2 14766.6 658.739 2 0 -4 -2 16468.6 785.552 3 0 -4 2 13909 728.362 3 0 -4 3 5557.55 470.332 3 0 -4 3 5334.69 380.306 2 0 -4 -3 5262.94 474.577 3 0 -4 -4 16169.7 824.223 3 0 -4 4 16574 664.452 2 0 -4 4 16466.1 812.238 3 0 -4 -5 7138.66 561.731 3 0 -4 5 7569.7 560.538 3 0 -4 5 7111.36 410.052 2 0 4 -6 11298.1 715.319 1 0 -4 -6 12562.6 755.55 3 0 -4 6 10870.4 497.499 2 0 -4 7 104489 1955.62 2 0 4 -7 102543 2584.18 1 0 -4 -7 100239 2586.94 3 0 4 -8 9995.82 707.966 1 0 -4 -8 10319.6 739.853 3 0 4 -9 23795.2 1164.42 1 0 -4 -9 24899.9 1215.47 3 0 -4 -10 1195.56 323.036 3 0 4 -10 678.978 277.676 1 0 4 -11 24692.8 1274.56 1 0 -4 -11 28464.6 1390.62 3 0 -4 -12 50.2915 223.539 3 0 4 -12 626.383 272.437 1 0 -5 0 534.897 238.732 3 0 -5 1 3901.32 451.177 3 0 -5 -1 4175.66 462.682 3 0 -5 -2 52445.9 1698.51 3 0 -5 2 51461.4 1673.27 3 0 -5 -3 332.495 219.887 3 0 -5 3 43.5959 200.389 3 0 -5 4 16200.2 908.746 3 0 -5 -4 16845.1 947.094 3 0 -5 -5 7191.71 628.343 3 0 -5 5 8132.24 661.747 3 0 -5 6 33341.9 1374.94 3 0 -5 -6 31823.2 1379.98 3 0 -5 7 33363.4 1408.31 3 0 -5 -7 31193.6 1406.7 3 0 -5 8 266.057 199.458 3 0 -5 -8 426.22 339.509 3 0 -5 9 7028.2 685.062 3 0 -5 -9 7095.69 699.982 3 0 -6 0 11428.2 844.892 3 0 -6 -1 4180.82 513.365 3 0 -6 1 5210.23 565.073 3 0 -6 2 11110.4 833.142 3 0 -6 -2 11063.1 824.132 3 0 -6 3 22435 1193.13 3 0 -6 -3 23549.3 1231 3 0 -6 4 17178.9 1043.79 3 0 -6 -4 16653.3 1048.12 3 0 -6 5 1903.84 395.249 3 0 -6 -5 2357.7 451.044 3 1 0 -16 341.729 255.652 1 1 0 -15 2671.03 453.541 1 1 0 -14 143.286 237.714 1 1 0 -13 79144.9 2411.96 1 1 0 -12 15.8057 71.7421 2 1 0 -12 -74.4966 233.539 1 1 0 -11 17936.9 958.562 1 1 0 -11 16972.8 545.536 2 1 0 -10 59.2528 90.0989 2 1 0 -10 209.252 198.254 1 1 0 -9 166411 2735.58 2 1 0 -9 167554 3437.28 1 -1 0 9 169415 3408.71 3 1 0 -8 62.7757 175.225 1 1 0 -8 -62.9617 72.4466 2 1 0 -7 83432.4 1485.41 2 1 0 -7 86643.2 1977.11 1 1 0 -6 -21.7826 150.857 1 1 0 -6 22.4435 55.813 2 1 0 -5 8189.12 275.916 2 1 0 -5 8949.2 463.964 1 1 0 -4 118.734 124.795 1 1 0 -4 249.176 63.4181 2 -1 0 4 22.4701 66.8686 2 1 0 -3 290181 4625.81 1 1 0 -3 298295 4418.62 2 -1 0 3 305807 4408.95 2 -1 0 2 73.6143 56.527 2 1 0 -2 -22.5837 80.4123 1 -1 0 -1 186834 2798.27 1 -1 0 -1 194962 2874.72 2 -1 0 -2 0.46933 74.4747 1 -1 0 -3 126008 2172.52 1 -1 0 -4 229.205 141.374 1 -1 0 -5 296574 4881.09 1 -1 0 -6 76.7985 149.676 1 -1 0 -7 128786 2697.6 1 1 0 8 -269.147 166.378 3 -1 0 -8 35.6599 167.92 1 1 0 9 70132 1869.36 3 -1 0 -9 71444.7 1963.08 1 -1 0 -10 -109.477 243.034 1 -1 0 -11 114323 2893.26 1 -1 0 -12 -80.0225 195.544 1 -1 0 -13 50667.4 1896.85 1 -1 0 -14 349.113 288.281 1 -1 0 -15 77124.9 2607.43 1 -1 0 -16 -327.633 232.482 1 1 1 -15 22055.8 1268.42 1 1 -1 -15 22645.9 1317.81 1 1 1 -14 15138.3 1002.94 1 1 -1 -14 16309.6 1075.92 1 1 1 -13 1788.12 357.405 1 1 -1 -13 1623.44 226.103 2 1 -1 -13 1580.38 350.621 1 1 1 -12 2552.55 393.844 1 1 -1 -12 3280.93 461.88 1 1 -1 -12 2541.56 268.767 2 1 -1 -11 2600.65 420.529 1 1 1 -11 2177.18 371.131 1 1 -1 -11 1712.63 229.888 2 1 -1 -10 199092 3993.93 1 1 1 -10 186228 3899.68 1 -1 1 9 9093.43 604.005 3 1 -1 -9 9323.54 635.523 1 1 1 -9 8153.04 589.18 1 -1 -1 9 8286.69 613.503 1 1 1 -8 83042.9 2041.17 1 -1 1 8 83267.5 2030.41 3 1 -1 -8 84786.2 2074.73 1 1 -1 -7 54271.4 1482.99 1 1 -1 -7 55027.9 1236.98 2 1 1 -7 55097.1 1480.83 1 1 -1 -6 114868 2097.01 2 1 1 -6 113574 2333.61 1 1 -1 -6 117225 2300.41 3 1 1 -5 293743 4803.04 1 1 -1 -5 293738 4752.57 3 1 -1 -5 291931 4580.11 2 1 -1 -4 198745 3284.36 3 1 -1 -4 196666 3196.05 2 1 1 -4 197950 3338.88 1 -1 1 3 66565.1 1288.32 2 1 1 -3 65520.5 1328.34 1 1 -1 -3 64996.2 1289.6 3 -1 1 2 468983 6848.96 2 1 1 -2 460721 6851.77 1 1 -1 -2 455166 6794.11 3 1 1 -1 94461.9 1620.12 1 1 -1 -1 93480.8 1561.09 3 -1 1 1 96186.9 1645.72 2 -1 1 0 1783.06 160.862 2 -1 -1 0 1922.37 159.848 3 1 -1 0 1864.61 132.045 3 -1 1 -1 53536.1 980.943 2 -1 -1 -1 49864.3 998.497 3 -1 1 -1 50608.9 956.978 1 -1 1 -2 648322 8670.53 2 -1 1 -2 653436 8725.31 1 1 -1 2 660194 8743.67 1 -1 -1 -2 660554 8778.15 3 1 -1 3 102745 1718.35 2 -1 -1 -3 101936 1873.81 3 -1 1 -3 101170 1707.61 2 1 -1 3 106296 1867.34 1 -1 1 -3 103783 1835.07 1 1 -1 4 5055.1 215.692 2 1 -1 4 5978.89 338.26 1 -1 -1 -4 6284.97 355.034 3 -1 1 -4 6003.98 325.867 1 -1 1 -4 5595.59 238.027 2 -1 1 -5 139.589 73.4589 2 -1 -1 -5 9.69818 143.927 3 1 -1 5 303.685 127.831 1 -1 1 -5 -71.629 129.779 1 -1 -1 -6 208335 3653.38 3 -1 1 -6 199196 3158.33 2 -1 1 -6 205808 3600.91 1 -1 -1 -7 11114.1 604.096 1 -1 -1 -7 10832.8 586.73 3 -1 1 -7 10813 370.397 2 1 -1 7 11203.3 615.131 1 -1 1 -7 10327 572.279 1 -1 1 -8 5862.63 278.707 2 1 -1 8 5410.65 469.396 1 -1 1 -8 6335.19 486.328 1 1 1 8 5918.28 449.165 3 -1 -1 -8 5984.89 494.454 1 -1 1 -9 21515.5 594.435 2 1 -1 9 21789.1 984.394 1 -1 -1 -9 22307.2 1009.51 1 -1 1 -9 21682.6 966.057 1 -1 1 -10 157227 3475.3 1 -1 -1 -10 162058 3546.79 1 -1 1 -10 163774 2677.53 2 -1 -1 -11 1975.35 374.596 1 -1 1 -11 1634.31 149.495 2 -1 1 -11 1464.59 324.226 1 -1 -1 -12 1836.11 374.897 1 -1 1 -12 1322.32 325.596 1 -1 1 -12 1989.58 164.252 2 -1 -1 -13 10302.8 834.54 1 -1 1 -13 10736.4 832.663 1 -1 1 -14 19313.7 1164.58 1 -1 -1 -14 17098.2 1115.23 1 -1 -1 -15 17541.9 1179.75 1 -1 1 -15 16344.9 1120.84 1 1 2 -15 14717.7 1056.62 1 1 -2 -15 13713.9 1048.9 1 1 2 -14 -322.66 220.995 1 1 -2 -14 -468.694 332.665 1 1 -2 -13 38.8749 239.96 1 1 2 -13 471.127 268.777 1 1 2 -12 58246.5 1998.39 1 1 -2 -12 64553 2103.64 1 1 2 -11 7163.9 634.585 1 1 -2 -11 8970.95 717.827 1 1 -2 -10 1793.15 339.222 1 1 2 -10 2658.09 387.023 1 1 -2 -9 3874.41 425.721 3 1 2 -9 3829.61 428.014 1 1 -2 -9 4419.55 378.497 2 1 2 -8 188818 3695.1 1 -1 2 8 189236 3664.5 3 1 -2 -8 185432 3422.3 2 1 -2 -8 186815 3645.37 3 -1 2 7 10301.4 582.476 3 1 2 -7 8960.53 566.14 1 1 -2 -7 8812.98 541.966 3 1 -2 -7 8486.62 481.822 2 -1 2 6 -60.4397 146.901 3 1 2 -6 141.998 163.838 1 1 -2 -6 201.654 137.102 2 1 -2 -6 -66.232 121.238 3 1 -2 -5 29628.5 922.64 3 1 2 -5 30540.6 961.682 1 -1 2 5 29506.7 926.058 3 -1 -2 5 28458.5 569.44 2 1 -2 -4 281331 4624.7 3 1 2 -4 287253 4687.49 1 -1 2 4 280074 4625.53 3 1 2 -3 9142.68 452.746 1 1 -2 -3 9833.08 445.214 3 -1 2 3 10089.3 451.927 3 1 2 -2 22265.8 713.553 1 1 -2 -2 22294.1 677.365 3 -1 2 2 22644.2 681.843 3 -1 -2 1 96794.2 1904.62 3 -1 2 1 99620.6 1855.77 3 1 -2 -1 101587 1854.74 3 1 -2 0 47092.1 1050.28 3 -1 -2 0 46073.5 1090.28 3 1 -2 0 44736.8 1039.61 2 -1 2 0 47448.1 1064.88 2 1 -2 1 40180.1 946.824 3 -1 -2 -1 38691 977.935 3 1 -2 1 38347 949.52 1 -1 2 -1 39479.7 916.902 2 1 -2 1 36452 900.874 2 1 -2 2 67053.6 1426.85 1 -1 2 -2 65844.7 1312.36 2 1 -2 2 68624.6 1348.27 2 -1 -2 -2 68711.3 1458.95 3 -1 2 -2 66563.3 1401.83 1 -1 -2 -3 480462 7398.71 3 1 -2 3 474009 7178.08 2 1 -2 3 487494 7363.99 1 -1 2 -3 485786 7137.85 2 -1 2 -3 472527 7337.92 1 1 -2 4 184055 3020.69 2 -1 2 -4 186587 2981.98 2 -1 2 -4 190875 3268.15 1 -1 -2 -4 187929 3330.65 3 1 -2 5 31812.6 751.962 2 -1 -2 -5 31504.2 1000.61 3 -1 2 -5 33021.7 726.548 2 -1 2 -5 32328.5 974.574 1 -1 2 -6 9614.71 532.118 1 -1 2 -6 9607.28 328.781 2 1 -2 6 10258.3 564.814 1 1 -2 6 10233.3 341.12 2 -1 -2 -6 9791.54 558.43 3 -1 2 -7 67480.8 1732.63 1 1 -2 7 70596.7 1820.19 1 -1 -2 -7 69724.5 1806.29 3 1 2 7 73359.5 1780.61 3 -1 2 -7 68972.2 1218.43 2 -1 -2 -8 79356.2 2054.9 3 1 -2 8 82826.3 2107.4 1 -1 2 -8 79568.5 1329.74 2 -1 2 -8 80230 1988.9 1 -1 -2 -9 33157.1 1250.12 3 -1 2 -9 30673.8 1179.15 1 -1 2 -9 30824.1 569.296 2 -1 2 -10 26221.5 1144.47 1 -1 -2 -10 25684.1 1148.14 3 -1 -2 -10 27326 1211.13 1 -1 -2 -11 55927 1932.34 1 -1 2 -11 59282.2 1892.43 1 -1 2 -12 34862.6 1473.96 1 -1 -2 -12 37240.3 1581.16 1 -1 -2 -13 25411.4 1344.82 1 -1 2 -13 23153.5 1239.65 1 -1 -2 -14 2496.91 459.112 1 -1 2 -14 2641.84 481.71 1 -1 -2 -15 13710.5 1071.21 1 -1 2 -15 13015 1004.56 1 1 -3 -14 11182.6 948.351 1 1 3 -14 10750.3 905.251 1 1 3 -13 15635.6 1038.74 1 1 -3 -13 18459.9 1164.91 1 1 -3 -12 4488.66 548.701 1 1 3 -12 3640.66 514.693 1 1 3 -11 17224.5 1008.78 1 1 -3 -11 16511.6 972.172 3 1 -3 -10 940.56 243.55 3 1 3 -10 753.429 262.271 1 1 -3 -9 29202.9 1204.97 3 1 3 -9 29779.6 1232.49 1 1 3 -8 10606.3 694.038 1 1 -3 -8 9953.71 662.712 3 1 3 -7 216.127 157.793 1 -1 -3 7 123.294 44.0559 2 1 -3 -7 212.648 182.742 3 1 -3 -6 39093 1257.86 3 1 3 -6 40811.4 1311.21 1 -1 -3 6 38487.7 830.968 2 -1 3 6 39353 1258.26 3 -1 -3 5 83819.1 1569.39 2 1 3 -5 85993 2036.73 1 1 -3 -5 82843.7 1970.27 3 -1 -3 5 85249 2040.53 1 1 -3 -5 84305.4 1947.32 2 -1 3 5 85634 1990.51 3 -1 3 4 14505.4 664.138 3 -1 -3 4 13943.2 671.692 1 1 3 -4 13784.6 678.109 1 -1 -3 4 13559.3 497.135 2 1 -3 -4 14400.9 660.889 3 -1 -3 3 173146 3255.23 3 1 -3 -3 168566 3167.76 3 -1 3 3 173910 3187.92 3 -1 -3 2 8297.31 496.725 3 1 -3 -2 7671.17 457.187 3 1 -3 -2 7606.77 458.315 2 -1 3 2 8110.24 468.424 3 -1 -3 1 41061.4 1184.92 3 -1 3 1 42021.1 1145.73 3 1 -3 -1 39599.5 1126.71 2 1 -3 -1 43582.8 1162.12 3 -1 -3 0 52781.4 1359.71 3 1 -3 0 51642.7 1317.67 3 1 -3 0 50332.3 1284.93 2 1 -3 0 53794.3 1345.32 1 1 -3 1 117860 2293.97 2 1 -3 1 123588 2386.67 1 -1 -3 -1 116236 2401.32 3 1 -3 1 119133 2358.72 3 1 -3 2 28047.7 911.663 3 1 -3 2 28335.9 923.154 1 1 -3 2 28156 841.904 2 -1 -3 -2 26908.9 940.091 3 1 -3 3 106402 2227.01 3 1 -3 3 110244 2275.93 1 -1 -3 -3 108039 2287.19 3 1 -3 3 105543 2069.54 2 -1 3 -4 47943.3 1342.43 1 1 -3 4 48325.2 1171.77 2 1 -3 4 51781.2 1394.33 1 -1 -3 -4 48461.1 1383.01 3 1 3 4 50447.6 1368.82 3 1 -3 5 82137.6 1673.84 2 1 -3 5 85307.3 2014.72 1 -1 3 -5 82646.8 1955.24 1 1 3 5 85646 1983.68 3 -1 -3 -5 83632.1 2012.86 3 1 -3 6 30708.3 1120.14 1 -1 3 -6 29721.4 1067.17 1 -1 -3 -6 28369.4 1098.21 3 1 -3 6 29761.9 804.163 2 1 -3 7 64065.5 1282.56 2 -1 3 -7 64478.8 1749.82 1 -1 -3 -7 62573.4 1799.34 3 -1 -3 -8 275.714 223.35 3 -1 3 -8 163.441 158.972 1 -1 3 -9 15204.9 833.086 1 -1 -3 -9 14586.4 861.033 3 -1 -3 -10 5784.79 579.708 3 -1 3 -10 5681.15 537.605 1 -1 3 -11 65124.5 2050.47 1 -1 -3 -11 63434.5 2092.31 3 -1 -3 -12 291.829 199.125 1 -1 3 -12 497.278 235.151 1 -1 -3 -12 197.957 201.798 3 -1 -3 -13 -68.027 279.865 1 -1 3 -13 329.518 220.748 1 -1 3 -14 22643.3 1293.84 1 1 4 -12 52505.1 2016.32 1 1 -4 -12 52451.6 1983.93 3 1 4 -11 2003.25 406.437 1 1 -4 -11 3337.64 475.513 3 1 4 -10 2348.3 386.632 1 1 -4 -10 1342.05 299.059 3 1 4 -9 987.181 294.021 1 1 -4 -9 726.495 259.047 3 1 4 -8 35339.9 1407.83 1 1 -4 -8 36655.7 1423.81 3 1 4 -7 11821.9 761.258 1 -1 -4 7 11698.4 450.842 2 1 -4 -7 11586.7 753.957 3 1 4 -6 3044.15 405.037 1 1 -4 -6 3339.71 406.701 3 -1 -4 6 3370.41 265.397 2 1 -4 -5 8374.98 597.009 3 -1 -4 5 8010.6 598.673 3 -1 -4 5 8371.6 436.816 2 -1 -4 4 55420.9 1359.76 2 1 -4 -4 58426.4 1656.36 3 -1 -4 4 54671.9 1650.59 3 -1 -4 3 44153.2 1211.66 2 -1 -4 3 45827.8 1452.7 3 1 -4 -3 44588.7 1383.41 3 -1 -4 2 30852.2 1006.86 2 -1 -4 2 33943.4 1195.49 3 1 -4 -2 31741.1 1125.74 3 -1 -4 1 2441.61 333.159 3 1 -4 -1 2242.67 304.099 3 1 -4 0 143882 2912.03 3 -1 -4 0 140834 2964.51 3 1 -4 0 139415 2836.21 2 1 -4 1 12402.3 660.779 3 -1 -4 -1 11623.3 669.714 3 1 -4 1 11493.5 612.233 2 1 -4 2 20307.5 800.867 2 1 -4 2 19259.3 848.842 3 -1 -4 -2 19167.7 884.771 3 1 -4 3 9826.69 537.226 2 -1 -4 -3 9043.83 604.946 3 1 -4 3 8113.24 560.119 3 1 -4 4 94518 2234.3 3 1 -4 4 92215.3 2031.47 2 -1 -4 -4 92752.9 2308.43 3 1 -4 5 2654.73 271.296 2 1 -4 5 2797.15 358.681 3 -1 -4 -5 3015.24 386.391 3 -1 4 -6 141.361 181.541 1 1 -4 6 414.79 140.643 2 -1 4 -7 5057.05 494.317 1 1 -4 7 5122.81 342.471 2 -1 -4 -7 4634.56 498.672 3 -1 4 -8 122527 2914.31 1 -1 -4 -8 117589 2973.03 3 -1 4 -9 19848.9 1038.61 1 -1 -4 -9 19829.2 1086.91 3 -1 4 -10 10611.4 784.122 1 -1 -4 -10 11917.4 879.804 3 -1 4 -11 3595.78 473.505 1 -1 -4 -11 3506.49 509.453 3 -1 -4 -12 22140.5 1282.97 3 -1 4 -12 21061.8 1192.2 1 1 -5 -10 19192.9 1174.7 3 1 -5 -9 49230.3 1877.15 3 -1 -5 9 45673.5 1797.15 3 1 -5 -8 1519.48 348.938 3 -1 -5 8 2095.64 411.823 3 -1 -5 7 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